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121.
122.
Dynamic light scattering is a suitable method for the investigation of transport properties such as the thermal diffusivity of optically transparent fluids. The main advantages of the method are its quickness, the fact of the thermodynamic state of equilibrium of the sample (gradients are not required), and the relatively simple evaluation of data without the necessity of calibration. However, an insufficient production of intensity of scattered light may be a limiting effect. For that reason the vicinity of the gas-liquid critical point represents the classical range of application. In this paper, it is shown that by means of an appropriate choice of experimental apparatus, measurements are also feasible in an extended range of states. Broad regions around critical points of three pure fluids (sulfur hexafluoride, SF6; ethane, C2H6; nitrous oxide, N2O) over temperature ranges ¦T-T
c¦ of 0.02 to 50 K and density ranges (/c) of 0.2 to 2 were investigated. In this region the thermal diffusivity shows great variations with temperature and density and cannot be described by means of ideal-gas behavior or relations for liquids. The measurements were carried out along the coexistence curve for both phases, along the critical isochore and along some isotherms with TT
c. The measured or calculated density, pressure, and thermal diffusivity data as well as some correlations are presented. 相似文献
123.
X. Q. Ma H. Zhang J. Dai J. Roth R. Hui T. D. Xiao D. E. Reisner 《Journal of Thermal Spray Technology》2005,14(1):61-66
This work addresses the fabrication of membrane-type solid oxide fuel cells (SOFCs) operating at medium temperatures, where
all components are fabricated by plasma spray technology, and the evaluation of the performance of the SOFC single unit in
a temperature range of 500 to 800 °C. Single cells composed of LaSrMgO3 cathodes, LaSrGaMgO3 (LSGM) electrolytes, and Ni/yttria-stabilized zirconia anodes were fabricated in successive atmospheric plasma-spraying processes.
Plasma-spraying processes have been optimized and tailored to each layer to achieve highly porous cathode and anode layers
as well as high-density electrolyte layers. A major effort has been devoted to the production of the LSGM electrolyte that
has a high density and is free of cracks. Electrochemical impedance spectroscopy was used to investigate the conductivity
of the electrode layers, and particularly the resistance of the electrolyte layer. It revealed that the heat treatment had
a great influence on the specific conductivity of the sprayed electrolyte layers and that the specific conductivity of the
heat-treated layers was dramatically increased to the same magnitude as is typical for sintered LSGM pellets. The experimental
results have demonstrated that the plasma-spraying process has a great potential for the integrated fabrication of medium-temperature
SOFC units.
The original version of this article was published as part of the ASM Proceedings, Thermal Spray 2003: Advancing the Science and Applying the Technology, International Thermal Spray Conference (Orlando, FL), May 5–8, 2003, Basil R. Marple and Christian Moreau, Ed., ASM International,
2003. 相似文献
124.
介绍铝及铝合金阳极氧化膜颜色的概念和描写,对颜色的儿种测量方法进行了比较,重点分析观察法及其在各国标准中的异同。在此基础上,提出了GB8013中的对颜色进行观察的条件和理论根据。 相似文献
125.
Francisco J. Corpas Salvador Gonzlez-Gordo Jos M. Palma 《International journal of molecular sciences》2021,22(5)
The peroxisome is a single-membrane subcellular compartment present in almost all eukaryotic cells from simple protists and fungi to complex organisms such as higher plants and animals. Historically, the name of the peroxisome came from a subcellular structure that contained high levels of hydrogen peroxide (H2O2) and the antioxidant enzyme catalase, which indicated that this organelle had basically an oxidative metabolism. During the last 20 years, it has been shown that plant peroxisomes also contain nitric oxide (NO), a radical molecule than leads to a family of derived molecules designated as reactive nitrogen species (RNS). These reactive species can mediate post-translational modifications (PTMs) of proteins, such as S-nitrosation and tyrosine nitration, thus affecting their function. This review aims to provide a comprehensive overview of how NO could affect peroxisomal metabolism and its internal protein-protein interactions (PPIs). Remarkably, many of the identified NO-target proteins in plant peroxisomes are involved in the metabolism of reactive oxygen species (ROS), either in its generation or its scavenging. Therefore, it is proposed that NO is a molecule with signaling properties with the capacity to modulate the peroxisomal protein-protein network and consequently the peroxisomal functions, especially under adverse environmental conditions. 相似文献
126.
Banendu Sunder Dash Gils Jose Yu-Jen Lu Jyh-Ping Chen 《International journal of molecular sciences》2021,22(6)
Cancer is one of the deadliest diseases in human history with extremely poor prognosis. Although many traditional therapeutic modalities—such as surgery, chemotherapy, and radiation therapy—have proved to be successful in inhibiting the growth of tumor cells, their side effects may vastly limited the actual benefits and patient acceptance. In this context, a nanomedicine approach for cancer therapy using functionalized nanomaterial has been gaining ground recently. Considering the ability to carry various anticancer drugs and to act as a photothermal agent, the use of carbon-based nanomaterials for cancer therapy has advanced rapidly. Within those nanomaterials, reduced graphene oxide (rGO), a graphene family 2D carbon nanomaterial, emerged as a good candidate for cancer photothermal therapy due to its excellent photothermal conversion in the near infrared range, large specific surface area for drug loading, as well as functional groups for functionalization with molecules such as photosensitizers, siRNA, ligands, etc. By unique design, multifunctional nanosystems could be designed based on rGO, which are endowed with promising temperature/pH-dependent drug/gene delivery abilities for multimodal cancer therapy. This could be further augmented by additional advantages offered by functionalized rGO, such as high biocompatibility, targeted delivery, and enhanced photothermal effects. Herewith, we first provide an overview of the most effective reducing agents for rGO synthesis via chemical reduction. This was followed by in-depth review of application of functionalized rGO in different cancer treatment modalities such as chemotherapy, photothermal therapy and/or photodynamic therapy, gene therapy, chemotherapy/phototherapy, and photothermal/immunotherapy. 相似文献
127.
姚成虎 《安徽冶金科技职业学院学报》2021,31(1):9-11
确定了试样以盐酸分解,重铬酸钾滴定法测定金属铁和亚铁合量,再减去金属铁含量,通过换算得到氧化亚铁含量。通过对不同条件下的试验优化,建立了重铬酸钾滴定法测定金属化球团中氧化亚铁含量试验方法,其测定结果的相对标准偏差为0.41%~0.94%,回收率大于96.0%。 相似文献
128.
热处理对制备纳米氧化铟锡(ITO)粉末的影响 总被引:9,自引:0,他引:9
以共沸蒸馏工艺辅助的共沉淀法制备了纳米氧化铟-氧化锡(ITO)粉体,研究了不同热处理温度对制备粉体的影响,结果表明,随着热处理温度的提高,粉体发生从四方结构向体心立方结构转变,晶粒出现长大现象,比表面积变化明显,化学组分保持高纯状态,综合比较,在700~800℃进行热处理可以得到尺寸均匀,晶形完整的纳米级粉体。 相似文献
129.
探索催化剂的制备条件,包括搅拌温度、干燥温度、煅烧温度及煅烧时间对二甲苯氧化效果的影响,结果表明煅烧温度对氧化效果的影响最为明显。在其它制备条件(搅拌温度为60 ℃、干燥温度为60 ℃和煅烧时间为3 h)不变的前提下,通过改变煅烧温度(温度分别350、450和550 ℃),比较3种二甲苯氧化难易以及不同煅烧温度下氧化同一构型二甲苯的差异。整体而言,煅烧温度为350 ℃的催化剂性能最佳。邻、间和对3种二甲苯完全氧化的温度相差约15 ℃,其中,邻二甲苯最难氧化,完全氧化需260 ℃,间二甲苯次之,对二甲苯最易氧化。与此同时,利用XRD、XPS、N2吸附-脱附和H2-TPR等表征手段来分析煅烧温度造成3种不同构型二甲苯氧化程度差异性的原因。 相似文献
130.