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71.
X-ray microtomography: Application to microstructure analysis of a cementitious material during leaching process 总被引:4,自引:0,他引:4
Leaching of cementitious materials leads to an increase in porosity, which has important consequences on transport and mechanical properties. The present study outlines the characterization of microstructural evolution in a mortar subjected to a chemical attack, by means of a powerful non-intrusive experimental method, namely synchrotron X-ray computed microtomography. This innovative method is used to measure the variation of porosity in a leached mortar. Having described the effects of leaching in mortar (influences on microstructure and on mechanical properties), we present the accelerated leaching process and the microtomographic analysis that have been used to monitor it. We then investigate the capacity of this method to quantify the evolution of porosity during the leaching process. The method is validated by comparison of the results obtained with data available in the literature. 相似文献
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Bai-Huan Xu Dong-Ya Sun Cong Ding Xue-Zhong Liu Zi-Jing Xiao 《Materials Research Bulletin》2007,42(9):1633-1639
Layered nanocomposite PEG/WS2, intercalating oligomeric poly(ethylene glycol) (PEG6000) into the tungsten disulfide host galleries, was synthesized using the exfoliation-adsorption technique. X-ray diffraction revealed that the intercalated oligomer within the host galleries is in a double-layer arrangement with an interlayer expansion of about 8.8 Å. The optimum conditions were explored to prepare the single-phase product with a composition of Li0.12(PEG)1.51WS2. Thermal analyses suggested that the resulting material shows good thermal stability, with the decomposition of the interacted oligomeric chains within the disulfide galleries occurring at around 258 °C. Despite high conductivity of the host material, those of the PEG/WS2 nanocomposite were found to be high in the order of 1 × 10−2 S cm−1 at ambient temperature, resulted from the host guest-host charge transfers. 相似文献
76.
《Materials and Manufacturing Processes》2007,22(1):5-8
The technological properties of the hot-work tool steels depend on their microstructural quality induced by the production process and the heat treatment. One of the frequently applied methods to improve microstructure is preheat treatment. The treatment of carbonitriding X37CrMoV5-1 steel has been investigated in fluidized bed furnaces. Thickness and phase composition have been conducted using optical microscopy Neophot 32 and scanning microscopy, JEOL 5400, after etching in nital. 相似文献
77.
Fresh niobium hydroxide was first precipitated from NbF5 solution using an aqueous ammonium hydroxide under basic conditions. Then a simple procedure of mixing lithium and niobium hydroxides together and heating at a low temperature (400 °C) produced pure ultrafine single phase LiNbO3 (LN). In the literature, this is the lowest temperature so far reported on the formation of LN. The phase content and lattice parameters are determined by X-ray diffraction (XRD). The average particle size and morphology were studied by transmission electron microscopy (TEM). 相似文献
78.
Y.X. Li 《Materials Letters》2007,61(22):4366-4369
TiC/Al composite was successfully synthesized utilizing laser ignited self-propagating high-temperature synthesis (SHS) of Al-C-Ti system with the different C/Ti molar ratio. When the molar ratio of C to Ti is below 1:1 in the starting materials, in addition to fine TiC particulates, a large amount of Al3Ti phase was found in the composites; however, when the molar ratio of C to Ti is 1:1 in the starting materials, the Al3Ti phase was almost completely eliminated and the distribution of TiC particulates generally appeared to be more homogeneous throughout the products synthesized. 相似文献
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小型微/纳米级三坐标测量机的研制 总被引:11,自引:1,他引:10
介绍一套低成本小型三维坐标测量机的研制过程,作为微/纳米级超精密测量设备,整体机台结构采用花岗岩材料;X/Y轴的移动平台利用压电材料摩擦驱动与挠性变形原理,长短两行程可达25mm范围及5nm的微位移,藉自行研发的衍射干涉激光尺,位置回馈测量系统可具有0.025nm的分辨率;测量探头在一般DVD光读取头的自动聚焦原理基础上改装,最佳分辨率可达2.5nm,该雏形机适于测量微机电组件、微型器件及膜厚等。 相似文献