X-Ray Measurement of Residual Stress in Plastic Bonded Explosives

The X-ray diffractive technology was adopted for tentative study of plastic bonded explosive. The datum of some new diffractive peaks in standard PDF cards were added. The effects of strain to interplanar distance and crystal size of the explosive were studied. The results show that grain size of plastic bonded explosive is decreasing with the increasing of the pressure, and the residual stress of the explosive is draw stress.     

弱导光纤的标量衍射光束特性分析

仿照罗兰圆光学系统构造罗兰球光学系统 ,在罗兰球中简化电磁波的瑞利 索末菲标量衍射积分公式 ,推导出折射率阶跃分布的弱导光纤LP模衍射场分布和空间频谱的计算公式。提出LP0 1模远场衍射分布存在类似于平面波圆孔夫琅禾费衍射艾里斑的中央亮斑概念 ,并给出中央亮斑角半宽度的计算公式。     

电控平行排列液晶光栅的光衍射特性研究

对电控平行液晶光栅的理论进行了分析,并配以结构原理图。通过对平行排列及90°扭曲排列液晶指向矢的计算,得出液晶盒中相应的折射率、相位差与电压之间的关系图,两者经比较证明平行排列更具适用性,并在实验中观测到了平行排列液晶光栅衍射特性与电压的关系。     

XPS studies of directly fluorinated HDPE: problems and solutions

X-ray photoelectron spectroscopy (XPS) applied to the study of fluorinated polymer surfaces presents several problems related both to peak assignment and to degradation. In this work, we analyse extensively the question of XPS peak assignments in this kind of surfaces. We conclude that in this kind of surfaces using binding energy differences between fluorine and carbon is better than using absolute binding energies. Also a useful relation between fluorine photoelectron energy vs. polymer composition expressed through the atomic ratio fluorine/carbon (F/C) was found. A protocol for data treatment is proposed and applied to a XPS study of the degradation induced by X-ray on high-density polyethylene surfaces modified by direct fluorination. Results obtained for the degradation, namely the atomic ratio F/C obtained by two different methods, combined with angle resolved X-ray photoelectron spectroscopy (ARXPS) were used to study the fluorine concentration profile in depth, producing self-consistent results.     

Possibilities and extension of XRD material response analysis in failure research for the advanced evaluation of the damage level of Hertzian loaded components

Due to clearly distinguishable damage symptoms, it is differentiated between the surface and sub‐surface failure mode of rolling bearings. Material states red out by X‐ray diffraction (XRD) residual stress measurements point to a variety of loading conditions especially at raceway surfaces that are associated with several competing failure mechanisms. The corresponding lifetime reduction can range from the lower fatigue strength region to material ratcheting in extreme cases. Relevant position of the microstructural changes and nature of the failure mechanisms are characterized. The time alteration of the XRD material parameters measured at or near the surface and at the depth of the maximum equivalent stress correlates, in a different manner, with the statistical parameter of the 10 % bearing life. Both failure modes are illustrated by concrete examples. Contaminated lubricant and boundary lubrication, which represent practically important surface‐induced failures, are discussed in more detail. Gray staining, i.e. shallow pitting, often occurs without distinct indication of global material aging by means of XRD characteristics. Here, scanning electron microscopy observations and electron microprobe analyses point to corrosion fatigue as acting surface failure mechanism. The interaction between material and lubricant under complex loading regimes particularly of mixed friction and corrosion opens further failure research areas in the field of tribology.     

Combined PIXE and SEM study of the behaviour of trace elements in gel formed around implant coated with bioactive glass

Bioactive glasses are used as coating biomaterials to facilitate anchorage of metallic prostheses implanted into the body. The aim of this work is to study the behavior of gel formed in contact with alloys and BVA and BVH bioactive glasses implanted. Cylinders of metallic implants composed by Ti, Al and V, are coated with bioactive glass. Three sheep were implanted for different time length: 3, 6 and 12 months in the femoral epiphysis. Results obtained with particle induced X-ray emission and scanning electron microscopy show that BVA coating induces a better contact between the metallic implant and bone. On the other hand, BVH coating prevents corrosion from the metallic implant.     

基于米氏散射及夫朗和费衍射的FAM激光测粒仪

提出了综合运用夫朗和费衍射和米氏散射，即在大粒径范围内采用夫朗和费衍射理论，而在小粒径范围内采用米氏散射理论，来改善小粒径范围内的测量精度，保证激光测粒仪在整个粒径范围内的测量精度。     

部分种子成分的特征X射线在等效生物材料中衰减的测定

用Ｓｉ（Ｌｉ）探测器实现了Ｎａ、Ｍｇ、Ｓ、Ｃｌ的特征Ｘ射线在有机膜中的相对衰减以及与Ｏ、Ｋ元素的特征Ｘ射线能量相当的Ｘ射线或轫致辐射在有机膜中的相对衰减，分别得出了它们减的数学描述，并把实验得到不同能量的Ｘ射线在有机膜中的质量吸收系数与Ｂｅｒｋｅｌｅｙ的ＯＣＧ软件计算出的结果相比，相关都小于３０％。     

Application of Rachinger''s method to separate overlapped doublets in the X-ray photoelectron spectrum

Rachinger's method of separating ₁ and ₂ doublets in X-ray emission spectra is applied for the first time to separate the superimposed doublets due to spin-orbit coupling. This method has been applied to separate closely lying doublets such as (Ag 4p_3/2and Ag 4p_1/2, (Ni 3p_3/2and Ni 3p_1/2) and (Cu 3p_3/2and Cu 3p_1/2). The intensities ratios of the separated peaks are measured and compared with the ratios obtained from a first-order calculation. An excellent agreement between the measured and calculated ratios are obtained. Residual background intensities compared with the estimated values are found to agree within certain uncertainties.     

柱形颗粒群直径分布的激光衍射测量技术

提出了用激光衍射功率谱方法测量柱形颗粒群直径分布的技术方法，解决了长颗粒随机排列时的功率谱探测，及数据快速优化方法等技术难题。此技术已地应用于由羊毛和化纤截成的柱形颗粒群直径分布的测量，实现结果证明了此技术的可行性和实用性。