电场固溶对2091A1-Li合金显微结构的影响

用电子探针及透射电镜研究了２０９１ＡｌＬｉ合金的电场固溶对显微结构的影响。结果发现，电场固溶通过促进含铜相溶解提高铜元素的固溶程度，加剧Ｌｉ原子在晶界上的非平衡偏聚，导致析出相δ′分布不均匀，体积分数减少，晶界上出现粗大的δ平衡相，Ｔ１及Ｓ′相均匀弥散分布，合金的力学性能（Ｔ６）达到了应变时效处理（Ｔ８）的水平。     

ZL114铝合金激光--龟弧的复合焊接

设计了一种激光-电弧复合热源焊接ZL114合金的新工艺，并对焊后的试件进行了X光检测、抗拉强度和全相组织等实验。结果表明，该种新工艺对铝合全有良好的适应性和可行性，是焊接领域的一个趋势。     

Electrochemical corrosion behavior of 2A02 Al alloy under an accelerated simulation marine atmospheric environment

The corrosion behavior of 2A02 Al alloy under simulated marine atmospheric environment has been studied using mass-gain, scanning electron microscope/energy dispersive spectroscopy (SEM/EDS), laser scanning confocal microscopy, X-ray diffraction spectroscopy and localized electrochemical methods. The results demonstrate that the relationship between the corrosion induced mass-gain and the corrosion time is in accordance with the power rule. The mass-gain increases gradually during the corrosion time, while the corrosion rate decreases. With ongoing of the corrosion, corrosion products film changed from a porous to a compact structure. The various spectroscopic data show that the corrosion products films composed mainly of Al(OH)₃, Al₂O₃ and AlCl₃. The electrochemical corrosion behavior of the 2A02 Al alloy was studied by electrochemical impedance spectroscopy (EIS).     

花形氧化锌纳米粒子的制备及其光催化性能

以氯化锌和氢氧化钠为原料,水为反应介质,密闭加热的条件下制备了花形ZnO纳米粒子。借助扫描电镜及X射线粉末衍射仪等仪器,对产物的形貌、结构进行了表征;对产物的生长机理做了研究,同时研究了反应条件对产物的影响,另外对产物进行了光催化测试。结果表明,花形骨架在反应初期就已经产生,反应时间增加,花形粒子变大;改变氯化锌和氢氧化钠的物质的量比,产物形貌产生了较大变化,分别生成了另一种形貌的花形粒子和片状粒子;通过光催化测试表明,所得的产物均有良好的光催化性能。     

Strain rate sensitivity of the commercial aluminum alloy AA5182-O

The mechanical behavior of the commercial aluminum alloy AA5182-O is investigated at temperatures ranging from −120 to 150 °C and strain rates from 10⁻⁶ to 10⁻¹ s⁻¹. The strain rate sensitivity parameter is determined as a function of temperature and plastic strain, and the strain rate and temperature range in which dynamic strain aging leads to negative strain rate sensitivity is mapped. The effect of dynamic strain aging on ductility and strain hardening is investigated. The sensitivity of the measured quantities to the experimental method employed and their dependence on grain shape are discussed. The experimental data are compared with the predictions of a model constructed based on a recently proposed mechanism for dynamic strain ageing. The mechanism is based on the effect solute clustering at forest dislocations has on the strength of dislocation junctions. The model is shown to reproduce qualitatively the experimental trends.     

添加Al2O3和SiO2的大晶粒UO2芯块制备研究

研究了Al2O3和SiO2添加剂对UO2芯块晶粒尺寸的影响.结果表明:加入少量的Al2O3和SiO2,可有效促进烧结过程中UO2芯块的晶粒度长大,过量加入则会阻碍烧结过程中UO2芯块的致密化;在添加量一定的情况下,添加不同比例的Al2O3和SiO2,对芯块晶粒尺寸有较大影响,只添加SiO2,对芯块晶粒尺寸影响不大,Al2O3添加量增加,芯块晶粒尺寸随之增加;添加Al2O3和SiO2促进UO2芯块晶粒长大的机制是在烧结期间发生了液相烧结.     

大型水轮发电机引进灭磁装置存在问题的探讨

本通过对我国近年引进的大型水轮发电机组灭磁装置运行与实验情况的研究，认为有的引进设备无论设计参数的选择还是自身可靠性方面或多或少地存在一些问题，应给以足够重视，在总结的基础上提出解决机组灭磁可靠性的技术方向。