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31.
采用恒定pH 12±0.2,按n(Mg2+)∶n(Al3+)∶n(OH-)∶n(CO2-3)=6∶2∶16∶1配制溶液,采用一步反应液相法,制备纳米层状双金属氢氧化物(LDH)粉体.为了获得无团聚、分散均匀的纳米粉体,探讨了溶剂置换干燥、真空干燥、常压干燥对纳米LDH粉体形成团聚的影响;用X射线衍射仪、透射电镜、红外光谱仪和元素分析仪对样品的物相、形貌、粒径和组成进行了表征.结果表明,溶剂置换干燥能够有效防止纳米粉体形成硬团聚,样品分散性好,呈针状形态,长50 nm,宽5 nm. 相似文献
32.
Electrochemical parameters of the nanoporous carbide-derived carbon|organic electrolyte have been studied by cyclic voltammetry and electrochemical impedance spectroscopy. The gas adsorption measurements have been used for evaluating the specific surface area, pore size distribution and porosity as the essential parameters influencing the double layer performance of carbon. The region of ideal polarizability, values of series and parallel resistance, capacitance and other important electrical double layer parameters were established. It was shown that specific capacitance of typical nanoporous carbon derived from titanium carbide is in the range of 70-90 F cm−3 or 100-130 F g−1 and it depends on the synthesis conditions. The influence of the electrolyte solvent to the capacitance was insignificant, although acetonitrile was advantageous with respect of smaller viscosity. 相似文献
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锌基重防腐双涂层防护技术在高速公路护栏上的应用 总被引:1,自引:0,他引:1
介绍了双涂层防护技术的进展以及锌基重防腐双涂层防护技术在高速公路护栏上的应用。 相似文献
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Abstract. Three linear methods for estimating parameter values of vector auto-regressive moving-average (VARMA) models which are in general at least an order of magnitude faster than maximum likelihood estimation are developed in this paper. Simulation results for different model structures with varying numbers of component series and observations suggest that the accuracy of these procedures is in most cases comparable with maximum likelihood estimation. Procedures for estimating parameter standard error are also discussed and used for identification of nonzero elements in the VARMA polynomial structures. These methods can also be used to establish the order of the VARMA structure. We note, however, that the primary purpose of these estimates is to generate initial estimates for the nonzero parameters in order to reduce subsequent computational time of more efficient estimation procedures such as exact maximum likelihood. 相似文献
37.
Giuseppe Ajroldi Maurizio Pianca Massimiliano Fumagalli Giovanni Moggi 《Polymer》1989,30(12):2180-2187
The dynamic-mechanical properties of some fluoroelastomers were determined as a function of composition at low frequency (≈ 1 Hz), by means of a free oscillation torsion pendulum, between −180°C and the softening point. Vinylidenefluoride (VDF)-hexafluoropropene (HFP) copolymers of molar composition 0–39% HFP and terpolymers of VDF and HFP with up to 30mol% tetrafluoroethylene (TFE) and a constant VDF to HFP molar ratio of 3.4 were considered. Two relaxation processes typical of the amorphous phase were found. The first, located at about −87°C, is related to local motions and the transition temperature was found to be independent of composition for copolymers, while it depends on TFE molar content for terpolymers. The second is related to the glass transition and the transition temperature depends on the composition. However, for semicrystalline copolymers the double glass transition phenomenon was observed. When crystallinity goes to zero at about 20 mol% HFP, only one transition is observed. It was also found that ordered structures can take place for terpolymers when TFE molar concentration exceeds 20%. The crystal disorder transition of pure PVDF (75°C) is observed also for low HFP concentrations but the transition temperature is strongly reduced. Analogies between the VDF-HFP and E-P systems are also discussed. 相似文献
38.
《Electronic Commerce Research and Applications》2014,13(5):355-367
One-sided auctions are used for market clearing in the spot markets for perishable goods because production cost in spot markets is already “sunk.” Moreover, the promptness and simplicity of one-sided auctions are beneficial for trading in perishable goods. However, sellers cannot participate in the price-making process in these auctions. A standard double auction market collects bids from traders and matches the higher bids of buyers and lower bids of sellers to find the most efficient allocation, assuming that the value of unsold items remains unchanged. Nevertheless, in the market for perishable goods, sellers suffer a loss when they fail to sell their goods, because their salvage values are lost when the goods perish. To solve this problem, we investigate the suitable design of an online double auction for perishable goods, where bids arrive dynamically with their time limits. Our market mechanism aims at improving the profitability of traders by reducing trade failures in the face of uncertainty of incoming/departing bids. We develop a heuristic market mechanism with an allocation policy that prioritizes bids of traders based on their time-criticality, and evaluate its performance experimentally using multi-agent simulation. We find out that our market mechanism realizes efficient and fair allocations among traders with approximately truthful behavior in different market situations. 相似文献
39.
扩展双星树(T(n)n1,n2)是 n-1长路径的两端点分别联结 n1条悬挂边和 n2条悬挂边所得到的图。论文根据扩展双星树的结构特征,研究了扩展双星树的类Wiener指数,给出了一般计算公式。 相似文献
40.