Use of polymeric nitrosation reagents for the N‐nitrosation of secondary amines under mild and heterogeneous conditions

A combination of crosslinked poly(4‐vinylpyridinium)chloride [P₄‐H]Cl ( I ) and sodium nitrite or quaternized crosslinked poly(N‐methyl‐4‐vinylpyridinium)nitrite [P₄‐Me]NO₂ ( II ) was used as effective nitrosating agents for the N‐nitrosation of secondary amines under mild and heterogeneous conditions in moderate to excellent yields. The spent polymeric reagents can usually be removed quantitatively and regenerated. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 1064–1067, 2007     

石油系二元族烃型橡胶增塑剂

以重油催化裂化装置生产的重组分油为原料，采用二次脱沥青精制工艺，可制备二元族烃型橡胶增塑剂。该增塑剂与国外同类产品的质量相当，仅凝点有一定差距，前者为２９．０℃，后者为－１０．６℃。应用试验表明，该产品替代传统增塑剂，且添充后硫化胶综合胶综合性能良好，耐磨性能优于添加传统增塑剂者。     

以合作学习为导向,探索中职计算机教学

随着我国教育模式的转变,在信息化的背景下,中国教育也逐步进入了信息化网络时代.为了提高计算机网络教学的发展,中职学校在计算机教学中进行了不断的探寻和研究,总结出通过合作学习的教学方式来提升中职计算机教学的教学质量.合作学习在中职计算机教学中的应用,使学生的学习应用能力与社会接轨,并锻炼学生合作意识,加强学生交流、分享能力.本文对合作学习在中职计算机教学中的应用进行研究分析,查找出其存在的问题,并给出了相应的解决策略.     

Pattern-induced multi-sequence alignment (PUMA) algorithm employing secondary structure-dependent gap penalties for use in comparative protein modelling

A multiple sequence alignment algorithm is described that usesa dynamic programming-based pattern construction method to aligna set of homologous sequences based on their common patternof conserved sequence elements. This pattern-induced multi-sequencealignment (PUMA) algorithm can employ secondary-structure dependentgap penalties for use in comparative modelling of new sequenceswhen the three-dimensional structure of one or more membersof the same family is known. We show that the use of secondarystructure information can significantly improve the accuracyof aligning structure boundaries in a set of homologous sequenceseven when the structure of only one member of the family isknown     

基于Bioperl的生物二次数据库的设计与实现

在分子生物学研究中,建立二次数据库可以更深入的进行特色物种的研究。通过分析了构建生物信息二次数据库的复杂性和必要性,在MySQL数据库的基础上利用Bioperl相关技术提出了可行性方案,并给出了关键的构建步骤,最后建立了一个生物信息研究平台。     

浅谈中职计算机课程中如何创设问题情境

在教学中,创设问题情境是一种科学有效的教学手段。通过对一堂计算机基础课《PPT动画路径》的分析,探究如何在中职计算机课程中创设问题情境,提高课堂教学实效性,并对容易出现的问题进行简单的阐述。     

Effects of mite resistance mechanism of geraniums on mortality and behavior of foxglove aphid (Acyrthosiphon solani Kaltenbach)

Geraniums (Pelargonium xhortorum Bailey) possess a pest-resistance mechanism, based on glandular trichomes and the exudate they produce, that has been shown to be effective against the two-spotted spider mite (Tetranychus urticae Koch). Using an intact plant bioassay, the effectiveness of the resistance mechanism was determined for another potential pest, the foxglove aphid (Acyrthosiphon solani Kaltenbach). Comparisons were made between plant lines previously analyzed for their degree of resistance to mites, as well as their glandular trichome density and trichome exudate production. Over 100 aphid adults were bioassayed on each of the five plant lines used in the experiment. In addition to adult aphid survival, the production and survival of nymphs was determined in this bioassay. The results indicate that plant lines that are resistant to the two-spotted spider mite are also resistant to the foxglove aphid, while lines susceptible to mites are susceptible to the aphids. To evaluate the physical impediment features of the trichome exudate, the behavior of foxglove aphid nymphs was compared on two geranium lines, one a resistant line with high trichome densities and large quantities of exudate and the second a susceptible line with few trichomes and reduced exudate. A third leaf surface type was produced by washing the exudate from resistant leaves using a mildly basic buffer solution prior to the bioassay. Aphid behavior was divided into five categories: feeding or probing, resting, wandering, struggling, and immobilized. On both susceptible leaves and resistant leaves from which the exudate had been removed by washing, the aphids settled quickly and were observed with inserted stylets during most of the observation intervals. In contrast, aphids on the unwashed resistant leaf surfaces often became ensnared in the sticky trichome exudate and had difficulty in settling to probe the leaf. Physical entrapment by glandular trichome exudate appears to be an important aspect of aphid resistance in geraniums.     

盐水二次精制工艺流程和生产操作

介绍了盐水二次精制的工艺流程、操作方法以及树脂塔的再生原理和注意问题。通过加强对盐水二次精制生产条件和螯舍树脂再生过程的控制，提高了树脂性能，保证了螯合能力的发挥，生产的合格精制盐水满足了离子膜电解生产的要求。     

Status of research on biogenic coalbed gas generation mechanisms

Biogenic coalbed gas,how it is generated and the geochemical characteristics of the gas are gaining global attention.The ways coalbed gas is generated,the status of research on the generation mechanism and the methods of differentiating between biogenic gasses are discussed.The generation of biogenic coalbed methane is consistent with anaerobic fermentation theory.Commercial biogenic coalbed gas reservoirs are mainly generated by the process of CO2 reduction.The substrates used by the microbes living in the coal include organic compounds,CO2,H2 and acetate.The production ratio and quantity of biogenic coalbed methane depend on the exposed surface area,the solubility and permeability of the coal and the microbial concentration in the coal seam.It is generally believed that biogenic coalbed gas has a value for σ13C1＜-5.5%,C1/C1+＞0.95.The H isotope ratio is controlled by both the environment and the generation mechanism:typically σD1＜-20%.Biogenic methane formed by CO2 reduction has more σD1 than that formed by acetate fermentation.     

基于硼酸溶液处理的GaAs/InP低温晶片键合技术

提出了一种基于硼酸溶液的GaAs/InP低温晶片键合技术,实现了GaAs/InP基材料间简单、无毒性的高质量、低温(290℃)晶片键合。GaAs/InP键合晶片解理截面的扫描电子显微镜(SEM)图显示,键合界面整齐,没有裂缝和气泡。通过键合过程,InP上的In0.53Ga0.47As/InP多量子阱结构转移到了GaAs基底上。X射线衍射及荧光谱显示,键合后的多量子阱晶体质量未变。二次离子质谱(SIMS)和Raman光谱图显示,GaAs/InP键合晶片的中间层厚度约为17 nm,界面处B元素有较高的浓度,键合晶片的中间层很薄,因此可以得到较好的电学、光学特性。