A three‐dimensional model describing stress‐temperature induced solid phase transformations: solution algorithm and boundary value problems

An always increasing knowledge on material properties as well as a progressively more sophisticated production technology make shape memory alloys (SMA) extremely interesting for the industrial world. At the same time, SMA devices are typically characterized by complex multi‐axial stress states as well as non‐homogeneous and non‐isothermal conditions both in space and time. This aspect suggests the finite element method as a useful tool to help and improve application design and realization. With this aim, we focus on a three‐dimensional macroscopic thermo‐mechanical model able to reproduce the most significant SMA features (Int. J. Numer. Methods Eng. 2002; 55 : 1255–1264), proposing a simple modification of such a model. However, the suggested modification allows the development of a time‐discrete solution algorithm, which is more effective and robust than the one previously discussed in the literature. We verify the computational tool ability to simulate realistic mechanical boundary value problems with prescribed temperature dependence, studying three SMA applications: a spring actuator, a self‐expanding stent, a coupling device for vacuum tightness. The effectiveness of the model to solve thermo‐mechanical coupled problems will be discussed in a forthcoming work. Copyright © 2004 John Wiley & Sons, Ltd.     

Review on testers for measuring flow properties of bulk solids

 The author was asked by the International Fine Particle Research Institue (IFPRI) to write a critical review on shear testers for IFPRI-members. The review was delivered to IFPRI in summer 1999. Following the contract with IFPRI it was not allowed to publish the review elsewhere for at least two years. Granular Matter invited the author to submit the review in the original form; during the refereeing process (besides other changes) it turned out that some remarks should be added here for clarification: - Since 1999, the author is not aware of a really new device for testing bulk solid properties, which could lead to a change of the general comments and conclusions provided in the review. It was argued, that the review is referring too much to the work of Jenike, while the works of Johanson and Peschl were not adequately cited. Both are excellent engineers with a lot of experience, but their basic ideas are not available in published form, and if, they are not set in relation to alternative approaches so that an objective comparison in detail would be a future research issue rather than a topic in this report. A discussion on the influence of electrostatic charges was missing. There hardly is an influence, since the particles are in continuous contact. Only with non-conducting plastic particles electrostatic charges could cause problems. But no relevant experiments and results are known. In closed systems, the effect of electric charges is thus mainly neglected, but it is clear that electrostatic forces are eminent in flows with a free surface – an issue not addressed in this review. Received: 1 November 2002     

钻井液固相化学清洁剂ZSC-201的合成及性能

介绍了钻井液用固相化学清洁剂ZSC－201的室内合成及性能评价，结果表明，固相化学清洁剂ZSC－201具有较强的抑制性，可有效抑制粘土水化分散，保证钻井液清洁，在钻井液体系中与阴、阳离子型钻井液处理剂配伍性好，同时具有较好的抑制增效作用，在有效的加量内对钻井液滤矢量和流变性等影响小，固相化学清洁剂ZSC－201已在中原油田近30口井中应用，具有良好的推广应用前景。     

实炉底节能连续式加热炉

轧钢生产使用实炉底连续式加热炉加热钢坯，炉内双纵滑管用耐热耐高温材料，无水冷，起到节约水、电的作用，达到节能增效的目的。     

An eight‐node hybrid‐stress solid‐shell element for geometric non‐linear analysis of elastic shells

This paper presents eight‐node solid‐shell elements for geometric non‐linear analysis of elastic shells. To subdue shear, trapezoidal and thickness locking, the assumed natural strain method and an ad hoc modified generalized laminate stiffness matrix are employed. A selectively reduced integrated element is formulated with its membrane and bending shear strain components taken to be constant and equal to the ones evaluated at the element centroid. With the generalized stresses arising from the modified generalized laminate stiffness matrix assumed to be independent from the ones obtained from the displacement, an extended Hellinger–Reissner functional can be derived. By choosing the assumed generalized stresses similar to the assumed stresses of a previous solid element, a hybrid‐stress solid‐shell element is formulated. Commonly employed geometric non‐linear homogeneous and laminated shell problems are attempted and our results are close to those of other state‐of‐the‐art elements. Moreover, the hybrid‐stress element converges more readily than the selectively reduced integrated element in all benchmark problems. Copyright © 2002 John Wiley & Sons, Ltd.     

高温润滑涂层设计的系统考虑

航天、航空、核能等尖端技术迫切要求使用耐高温润滑涂层，以保护金属构件的表面，增加发动机、推进器的工作效率和输出功率，８０年代国际摩擦学界根据工业和国防的需要将高温润滑涂层和耐磨材料定为摩擦学学科发展的重要研究方向之一。本文对高温润滑涂层设计中遇到的典型环境、涉及到的关键问题、未来发展的途径等问题作了阐述。     

以废钡渣为原料制取氯化钡的研究

本文研究了以直接耐晒黑Ｇ染料生产中的废钡渣为原料制取氯化钡的方法，氯化钡的得率达到废钡渣量的７０．９９％，产品质量达到一级品的标准。     

KCl与NaCl在低盐固态法酱油发酵中的应用比较

对KCl与NaCl在低盐固态酱油发酵中的应用进行了比较研究。结果表明：用KCl代替NaCl，KCl的浓度要高于NaCl才能抑制发酵期间杂茵的污染，且使用KCl的发酵效果比NaCl要好。     

Analysis of supersaturation and nucleation in a moving solution droplet with flowing supercritical carbon dioxide

A supercritical antisolvent (SAS) process is employed for production of solid nanoparticles from atomized droplets of dilute solution in a flowing supercritical carbon dioxide (SC CO₂) stream by attaining extremely high, very rapid, and uniform supersaturation. This is facilitated by a two‐way mass transfer of CO₂ and solvent, to and from the droplet respectively, rendering rapid reduction in equilibrium solubility of the solid solute in the ternary solution. The present work analyses the degree of supersaturation and nucleation kinetics in a single droplet of cholesterol solution in acetone during its flight in a flowing SC CO₂ stream. Both temperature and composition are assumed to be uniform within the droplet, and their variations with time are calculated by balancing the heat and mass transfer fluxes to and from the droplet. The equilibrium solubility of cholesterol with CO₂ dissolution has been predicted as being directly proportional to the Partial Molar Volume Fraction (PMVF) of acetone in the binary (CO₂–acetone) system. The degree of supersaturation has been simulated up to the time required to attain almost zero cholesterol solubility in the droplet for evaluating the rate of nucleation and the size of the stable critical nuclei formed. The effects of process parameters have been analysed in the pressure range of 7.1–35.0 MPa, temperature range of 313–333 K, SC CO₂ flow rate of 0.1136–1.136 mol s^?1, the ratio of the volumetric flow rates of CO₂‐to‐solution in the range of 100–1000, and the initial mole fraction of cholesterol in acetone solution in the range of 0.0025–0.010. The results confirm an extremely high and rapid increase in degree of supersaturation, very high nucleation rates and stable critical nucleus diameter of the order of a nanometre. Copyright © 2005 Society of Chemical Industry