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41.
42.
Catalytic wet air oxidation of butyric acid solutions using carbon-supported iridium catalysts 总被引:1,自引:0,他引:1
Aqueous solutions of butyric acid were treated by catalytic wet air oxidation using carbon-supported iridium catalysts in a stirred reactor. Under the operating conditions of 6.9 bar of oxygen partial pressure and 200 °C of temperature, conversions up to 52.9% after 2 h were obtained depending on the type of catalyst used. The effects of butyric acid initial concentration, loading of catalyst, oxygen partial pressure and temperature were investigated and the empirical rate law for acid conversion is presented. Oxidation intermediates such as propionic and acetic acid were identified. The heterogeneous catalyzed free-radical oxidation of butyric acid is discussed. 相似文献
43.
In recent years, ultra-precision micromachining technology has been used in a variety of fields such as optical instruments, electronic devices, medical equipments, etc. At present, it is essential to meet the requirement of producing various shapes, one of which is a structure with a high aspect ratio. Such structures are applied, for example, to a shaft of micro robot, a long part of microactuator and micromachine, a microneedle for syringe, etc. However, due to its fragile nature, it is extremely difficult to fabricate the structure with a high aspect ratio since it is easily damaged during cutting. It is intended to produce micro towers with high aspect ratios by applying the ultra-precision milling technology using a single crystal diamond cutting tool. The method enables accurate creation of a variety of microstructures with high aspect ratios. In addition, the study also proposes a new machining method to create microneedle arrays, avoiding the contact of cutting edge with already machined parts again. As a result, it is concluded that the proposed method has the potential of producing a variety of microstructures with high aspect ratios. 相似文献
44.
Transformations in machining. Part 1. enhancement of wavelet transformation neural network (WT-NN) combination with a preprocessor 总被引:2,自引:0,他引:2
X. Wang P. Chen I.N. Tansel Yenilmez A 《International Journal of Machine Tools and Manufacture》2006,46(1):36-42
Properly selected transformation methods obtain the most significant characteristics of metal cutting data efficiently and simplify the classification. Wavelet Transformation (WT) and Neural Networks (NN) combination was used to classify the experimental cutting force data of milling operations previously. Preprocessing (PreP) of the approximation coefficients of the WT is proposed just before the classification by using the Adaptive Resonance Theory (ART2) type NNs. Genetic Algorithm (GA) was used to estimate the weights of each coefficient of the PreP. The WT-PreP-NN (ART2) combination worked at lower vigilances by creating only a few meaningful categories without any errors. The WT-NN (ART2) combination could obtain the same error rate only if very high vigilances are used and many categories are allowed. 相似文献
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介绍龙门铣床的直流调速控制系统的改造方案,根据龙门铣床工作台运动过程及原直流电机的容量来选择交流电机和变频器并对变频器的功能进行设定。 相似文献
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48.
Hybrid precursors were assembled with cerium coordination polymers, polyethyl glycohol (PEG), SrCO3 and other functional components using a modified in-situ chemical polymeric gel technology. The hybrid precursors were calcinated to achieve the Sr2CeO4 phosphors, whose particle sizes were in the range of micrometer by XRD and SEM. The photoluminescence spectra indicate that the phosphors present a strong blue emission. 相似文献
49.
以Y30H-1的SrM预烧料为原料,通过对二次添加剂、二次球磨及烧结曲线的调整,做出了Br≥380mT,Hcb≥240kA穖-1,Hcj≥250kA穖-1,(BH)max≥27.0kJm-3的干压各向异性锶铁氧体产品。 相似文献
50.