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71.
Catalytic degradation of high-density polyethylene (HDPE) was carried out under nitrogen using a laboratory fluidised bed reactor operating at 360 °C with catalyst to polymer feed ratio of 2:1 and at 450 °C with catalyst to polymer feed ratio of 6:1 under atmospheric pressure. The catalysts used in this study were ZSM-5, US-Y, ASA, fresh FCC (fluid catalytic cracking) commercial catalyst (Cat-A) and equilibrium FCC catalysts with different levels of metal poisoning were studied. The initial results for polymer degradation at 360 °C (catalyst to polymer ratio of 2:1) in a fluidised bed reactor in terms of the yield of volatile hydrocarbon products were: model catalysts>commercial FCC catalyst>E-Cats. However, when the process conditions more closely resembled to FCC conditions, the fresh commercial FCC catalyst was more favourable in terms of the yield of volatile hydrocarbon products. The degradation of HDPE over E-Cats although reduced was similar to ASA in product selectivity and yield, and the level of metal contamination did not affect the product stream generated. A simple economic evaluation of polymer recycling process is reported showing that a catalytic system based on E-Cats appears comparable in costs to a commercial thermal cracking plant. 相似文献
72.
甲基三氯硅烷(M1)与低沸物(LBR)是工业上"直接法"生产二甲基二氯硅烷单体过程中产生的副产物,两者之间通过再分配反应可转化为高价值的有机硅单体.以活性炭为载体,采用浸渍蒸发煅烧法制备了负载型AlCl3固体酸催化剂,在固定床反应器中进行甲基三氯硅烷与低沸物的再分配反应,制得二甲基二氯硅烷和三甲基氯硅烷.考察了活性炭载体预处理方式及反应条件对再分配反应的影响.结果表明,经过高温扩孔处理的活性炭载体负载的AlCl3催化剂具有较好的反应活性;优化的反应条件为:W(M1/LBR)为2.0~3.0,反应温度为310℃,LHSV为1.5 h-1;该催化剂的制备过程简单,催化反应条件温和且表现出良好的催化稳定性. 相似文献
73.
在对旋转填料床精馏特性研究的基础上,以塑料多孔板为填料,乙醇-水为体系,在全回流操作条件下,进一步研究了气相动能因子F、超重力因子β和回流量L对旋转填料床流体力学特性的影响,证明了旋转填料床的低耗能特性。 相似文献
74.
75.
The vector form of the Ergun equation was used to numerically predict gas phase streamlines, residence time distributions, chemical conversions and pressure drops in the annulus of a side-outlet spouted bed with an internal draft tube. By varying the position of the side-outlet, it was demonstrated that there exists an optimum location for this outlet at which conversion is a maximum and which shows a greatly improved gas phase residence time distribution in the annulus compared with a conventional spouted bed unit. 相似文献
76.
A fractal approach is adopted to describe the dynamic behavior of a circulating fluidized bed. Two times series, differential pressure fluctuations along the riser height and solids momentum fluctuations along the radial direction, are measured and analyzed in terms of fractal dimensions. The influences of operating conditions and axial/radial positions on the fractal dimension are discussed. Attempts are also made to interpret the flow structure in the bed in terms of the fractal dimension. It is found that fractal analysis can provide a useful tool for understanding the characteristics of gas-solids flow in circulating fluidized beds. 相似文献
77.
78.
压力流化床燃烧技术近二十年来在世界上得到很大发展。煤的湿法给料系统具有比干法输送系统更简单,运行调节更可靠等优点。煤水混合物可泵送的水分在25%左右,煤的粒度一般为0~6mm,表现为非牛顿的假塑性流体特性,通过级配来达到一定的稳定性和良好输送性能,且流动阻力低,不用添加剂即可实现泵送,它的应用使压力流化床的燃烧制备和输送系统成本大大降低。 相似文献
79.
The reaction between SO2 and calcined limestone particles has been studied in a fluidized bed combustor. Measurements of sorbent reactivity with SO2 were made for small batches of limestone injected into the combustor. Simultaneous continuous combustion of bituminous coal provided conditions like those of a boiler for study of the sulphation reaction. A semi-empirical rate model of the CaO-SO2 reaction has been developed. External mass transfer of SO2, diffusion within the particles and chemical reaction are taken into account. The limestone reactivity with SO2 is characterized by two parameters which are dependent on the temperature and sorbent particle size. A model for predicting the limestone requirements in a fluidized bed boiler has been developed. Parameters from the batch experiments are included. The predictions for sulfur retention agree with the experimental results. In addition, effects of operating conditions (gas velocity, recycle, limestone particle size) on the retention of SO2 were simulated using the model. 相似文献
80.
The interface area between the bubble and emulsion phases in a fluidized catalyst bed is one of the important parameters used to analyze and design the fluidized bed reactor. We used a fast‐scanning X‐ray CT system to observe the bubble shape and structure. We then obtained the transient 2‐dimensional cross sectional gas‐phase distribution in a fluidized catalyst bed. Using image‐processing techniques, pseudo 3‐dimensional images of the bubbles were reconstructed. The bubble structure was studied based on the 3‐dimensional images and the previously obtained results in a 2‐dimensional fluidized bed. It was found that the bubble shape was not spherical but complicated, and that the bubbles ascending in a fluidized catalyst bed consisted of some smaller bubbles. 相似文献