Ozonation of CI Reactive Black 5 using rotating packed bed and stirred tank reactor

This study investigates the ozonation of CI Reactive Black 5 (RB5) by using the rotating packed bed (RPB) and completely stirred tank reactor (CSTR) as ozone contactors. The RPB, which provides high gravitational force by adjusting the rotational speed, was employed as a novel ozone contactor. The same ozone dosage was separately introduced into either the RPB or the CSTR for the investigation, while the experimental solution was continuously circulated within the apparatus consisting of the RPB and CSTR. The decolorization and mineralization efficiencies of RB5 in the course of ozonation are compared for these two methods. Moreover, the dissolved and off‐gas ozone concentrations were simultaneously monitored for the further analysis. As a result, the ozone mass transfer rate per unit volume of the RPB was significantly higher because of its higher mass transfer coefficient and gas–liquid concentration driving force. Furthermore, ozonation kinetics was found to be independent of the gravitational magnitude of an ozone gas–liquid contactor. Therefore, the results suggest employing RPBs as ozone‐contacting devices with the advantage of volume reduction. The experimental results, which can be used for further modeling of the ozonation process in the RPB, also show the requirement of correct design for the RPB. Consequently, the present study is useful for the understanding of practical application of RPBs. Copyright © 2004 Society of Chemical Industry     

消减空压机气流脉动方法的探讨

根据气流脉动的机理，提出了解决空压机常见的机组枷管过振动问题的一些具体措施。     

输气管道天然气连续取样器的研制及应用

文章针对国内管输天然气气质分析工作中取样环节所存在的问题，结合国外技术发展趋势，全面地介绍了输气管道天然气连续取样器的研制过程。实践证明，该装置较好地解决了天然气密度值偏差问题，满足管输天然气全分析的要求，同时，该装置的推广应用将会提高天然气的计量准确度。     

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凝析气井井筒温度分布是进行气井节点分析和动态分析必不可少的参数。根据传热学原理推出了凝析气井井筒温度分布计算公式，研究了温度计算基础数据求取方法，分析了产气量、产水量、井深及油管直径对井口温度的影响规律。对某一井深为５４００ｍ的凝析气井进行了计算，该气井气油比为３０００，含２３％的Ｈ２Ｓ和４％的Ｎ２；地层温度为１３４℃。计算结果表明：井口实测温度与计算温度的相对误差为０２％～３８％，符合工程精度。气井温度随井深不呈线性分布；气井井口温度随产量、井深增加而增加，随油管直径减少而减少；该公式同时适用于干气井、湿气井和凝析气井的温度分布计算，计算精度符合工程精度要求。     

液相添加剂对PTCR陶瓷电性能的影响

液相添加剂ＡＳＴ（Ａｌ２Ｏ３＋ＳｉＯ２＋ＴｉＯ２）对ＢａＴｉＯ３陶瓷材料电性能的影响很大，随着Ａｌ２Ｏ３含量的增加，材料的电性能降低；ＳｉＯ２、ＴｉＯ２的物理特性对材料电性能影响较大；过量ＴｉＯ２对材料ＰＴＣ效应有重要影响，适当过量ＴｉＯ２含量，可得到性能优良的ＰＴＣＲ陶瓷。     

塑料薄膜透气测试装置及测试方法研究

根据塑料薄膜透气原理，设计了一种简易薄膜透气测试装置，并对测试方法及结果处理进行了探讨。     

混合型表面活性剂液膜法处理含酚废水研究

研究了兰－１１３Ｂ＝Ｓｐａｎ－８０－－煤油ＮａＯＨ液膜体系处理苯酚废水的最佳操作工用于对高浓度含酚废水进行处理，实验结果表明，混合型表面活性剂各项指标均较好，除酚效率可达９９％以上，对内相ＮａＯＨ的最佳浓度的确定给出了估算方法。     

外循环型鼓泡式反应器气含率及循环液速率

对直径２８０ｍｍ、扩大直径５００ｍｍ、外循环管直径６５ｍｍ、总高２９００ｍｍ的外循环型鼓泡式反应器，在气体空塔线速Ｕｇ为０．０４－０．５５ｍ／ｓ时，用静压差法和脉冲示踪法测定了不同部位的气含率Ｅｇ，Ｅｐｇ和循环液速率ｕ１，并获得了它们的关联式：对反应段，Ｅｇ＝０．４５５６Ｕ＾０．３１９８ｇ〔Ｕｇ／（Ｕｇ＋Ｕ１）〕＾０．７３９６；对反应器扩大段，Ｅｕｇ＝０．９３８９Ｕ＾０．４４３１ｕｇ；对循环管，Ｅ