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41.
Calcining of the mixture of BaCO3 and TiO2 with a ratio 1:4 at different temperatures was carried out to synthesize BaTi4O9 powders. Phase evolution of the samples was studied using the differential thermal analysis (DTA) and X-ray diffractometry
(XRD). Both techniques confirmed that the formation of BaTi4O9 started around 1000 °C. The XRD peaks showed that BaTi4O9 was most pronounced at 1250 °C. X-ray line broadening methods were employed to study the variation of particle size and microstrain
of the BaTi4O9 powders. The Voigt function in a single line and the pseudo-Voigt function in the variance methods were used in our case.
We found that both functions resulted in the same trends, i.e., the particle size increased with the temperature with the
biggest size of 180 and 160 nm, whilst the microstrain yielded the opposite trend with the lowest values of 6.2 × 10–3 and 1.1 × 10–3. The scanning electron microscopy (SEM) study revealed the size of the large particles formed, due to agglomeration, to be
about 0.5–1.9 μm. Furthermore, it was shown that irregular shapes of BaTi4O9 powders necked to each other appeared at 1000 °C and grew into ellipse and rod shapes at 1250 °C.
Electronic Publication 相似文献
42.
喻尧全 《石油化工管理干部学院学报》2002,(2):1-3
剖析国有企业党风廉政建设中的突出问题。提出“推进国有企业党风廉政建设运用市场经济原则经营运作是重要途径;加强对企业经营管理者的监督管理是关键;完善法人治理结构、建立企业内部权力制衡机制是重要基础”的观点。 相似文献
43.
加强农村广播电视的发展,提高其覆盖率是关键,针对这一问题,阐述了解决农村广播电视覆盖的手段,对农村广播电视覆盖现状做了详细的分析,并提出建议和措施。 相似文献
44.
提出了一种相似度的新定义,使双极WAT模型的实现更加简洁明了。增加一个阈值使系统能判别非存储模式或因其信息量过低而无法鉴定的输入模式,阈值的大小与要求的容错能力有关。双极相似度及阈值通过光学方法实现。阈值的光学实现使系统仍具有照明不变性。通过电路实现取及WTA网络的迭代运算。 相似文献
45.
考虑Hopfield模型中假态之间的布尔逻辑关系,提出利用IPA模型对神经网络中的假态进行抑制,并和原网络的性能进行了比较,结果表明:改进后的网络性能比Hopfield模型和IPA模型均有较大提高。 相似文献
46.
赵正予 《电子科学学刊(英文版)》1994,11(3):262-267
In this paper, the evaluation by running window smoothing is used for the digital processing of the polarization of geophysical ULF signals. The observed signals are resolved into two orthogonal complex components so that it is no longer necessary to consider the phase and amplitude of the signals simultaneously. 相似文献
47.
48.
A. Palmeri F. Ricciardelli G. Muscolino A. De Luca 《Canadian Metallurgical Quarterly》2004,130(9):1052-1061
The equation of motion of linear dynamic systems with viscoelastic memory is usually expressed in a integrodifferential form, and its numerical solution is computationally heavy. In two recent papers, the writers suggested that the system memory be accounted for through the introduction of a number of additional internal variables. Following this approach, the motion of the system is governed by a set of first-order, linear differential equations, whose solution is quite easy. In this paper, the approach is extended to single-degree-of-freedom systems subjected to random, nonstationary excitation. The equations governing the time variation of the second-order statistics are derived, and an effective step-by-step solution procedure is proposed. Numerical example shows the accuracy of the procedure for white and nonwhite excitations. 相似文献
49.
本文为了克服精馏塔静态仿真不易收敛和初值难以给定等难题,巧妙地利用隐含数值积分方法的特点,将稳态与动态数学模型耦合起来,用以求解高难度的非理想精馏塔静态仿真问题。所得静动态混俣模型大大提高了精馏塔静态仿真的鲁棒性,对于高度非理想精馏塔的仿真尤为有效。通过对某丙烯腈萃取精馏塔的静态仿真,充分证明了这种混合模型化方法的可行性。 相似文献
50.
Y1.94-xMgxO2S:0.06Ti (0≤x≤0.10) phosphors with long afterglow were synthesized by solid state reaction route. The photoluminescence spectra, decay curves, thermoluminescent spectra and chromaticity coordinate curves were investigated. The results show that the luminescence intensity of Y1.94-xMgxO2S:0.06Ti (0≤x≤0.10) phosphors decrease gradually with increasing Mg2 ion content, and the shape of luminescence spectra and chromaticity coordinate change as well. Furthermore, two thermoluminescent peaks in single Ti-doped Y2O2S sample are found at 91.8 and 221.5 ℃, respectively. Nevertheless, significant different spectra were found for the Mg, Ti co-doped Y2O2S samples that three thermoluminescence peaks appear at 52.3, 141.7 and 226.8 ℃, respectively. These results indicate that the co-doped Mg ion changes the inherent trap depth of single Ti-doped Y2O2S:Ti phosphor, and induces simultaneously a new trap level in the Y1.94-xMgxO2S:0.06Ti phosphor. Based on the analysis of thermoluminescent spectra, photoluminescent spectra, decay curve and crystal structure defect, it was proposed that the varied structure defect and introduced new trap level by the doped Mg2 ions should be responsible for reducing luminescence intensity and varying color in the Y1.94-xMgxO2S:0.06Ti phosphor. 相似文献