含丙烯酰基可聚合色素中间体的合成

采用N,N-二羟乙基苯胺(BHEA)与丙烯酸直接酯化法,合成了一类可聚合色素的重要中间体。考察了催化剂种类及用量、反应温度、物料配比等反应参数对酯化反应的影响。对酯化产物分别采用TLC和GC/MS法进行了分析和鉴定。     

基于PLC的电阻炉温度控制系统中模拟量的采集方法

本文以电阻炉温度控制系统为例,介绍了利用三菱FX-2N型PLC通过FX-2N-4AD转换模块实现数据采集的方法。     

注入氮离子的SiC涂层阻氢性能研究

利用离子束混合－离子注入（Ar^ ）和磁控溅射相结合的实验技术在HR－1不锈钢基体上制备了注入N^ 的SiC涂层，并用表面分析手段对所制备涂层的表面形貌，剖面形貌、相结构，表面成分，表面元素的化学态进行了分析，结果表明：制备的涂层结构致密，表面平整、膜层成分均匀；涂层与基体之间形成了一明显的过渡层，增强了涂层和基体之间的结合力，用二次离子质谱（SIMS）对充氘涂层的阻氢性能进行了定性分析，结果表明，涂层元素与氢形成稳定的化学键，抑制了氢的扩散和迁移，使得涂层具有一定的阻氢能力。     

Larke Nahme Huang: Award for Distinguished Senior Career Contributions to Psychology in the Public Interest.

Presents the citation, biography, and selected bibliograpy for Larke Nahme Huang, the 2007 recipient of the American Psychological Association's Award for Distinguished Senior Career Contributions to Psychology in the Public Interest. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Detection of COVID-19 and its pulmonary stage using Bayesian hyperparameter optimization and deep feature selection methods

Since the first case of COVID-19 was reported in December 2019, many studies have been carried out on artificial intelligence for the rapid diagnosis of the disease to support health services. Therefore, in this study, we present a powerful approach to detect COVID-19 and COVID-19 findings from computed tomography images using pre-trained models using two different datasets. COVID-19, influenza A (H1N1) pneumonia, bacterial pneumonia and healthy lung image classes were used in the first dataset. Consolidation, crazy-paving pattern, ground-glass opacity, ground-glass opacity and consolidation, ground-glass opacity and nodule classes were used in the second dataset. The study consists of four steps. In the first two steps, distinctive features were extracted from the final layers of the pre-trained ShuffleNet, GoogLeNet and MobileNetV2 models trained with the datasets. In the next steps, the most relevant features were selected from the models using the Sine–Cosine optimization algorithm. Then, the hyperparameters of the Support Vector Machines were optimized with the Bayesian optimization algorithm and used to reclassify the feature subset that achieved the highest accuracy in the third step. The overall accuracy obtained for the first and second datasets is 99.46% and 99.82%, respectively. Finally, the performance of the results visualized with Occlusion Sensitivity Maps was compared with Gradient-weighted class activation mapping. The approach proposed in this paper outperformed other methods in detecting COVID-19 from multiclass viral pneumonia. Moreover, detecting the stages of COVID-19 in the lungs was an innovative and successful approach.     

金属间化物（Sm_（1－x）Y_x）_2Fe_（17）N_y中N原子占位的点电

通过穆斯堡尔谱等手段研究赝三元金属间化物（Ｓｍ１－ｘＹｘ）２Ｆｅ１７Ｎｙ中的Ｎ原子占位机闭，并通过点电荷模型对Ｎ原子的占泣机制进行理论解释。由试验结果和点电荷模型结果得出以下结论：１）Ｎ原子占据９ｅ（６ｈ）和１８ｇ（３ｂ）两个间隙品位；２）Ｎ原子的双重占位与自旋磁结构密切相关，是单轴各向异性产生的主要原因。     

CO2对钻具的腐蚀及控制

与含CO2油气层接触的钻井液会对钻具造成腐蚀.针对用于钻水平井的PRD钻井液,采用静态挂片失重法,研究了温度、CO2分压和钻井液pH值对N80钢腐蚀的影响,筛选并评价了抑制CO2腐蚀的缓蚀剂.结果表明,PRD钻井液对N80钢的腐蚀速率随CO2分压的增大和温度的升高而增大,随pH值的增大而减小.在CO2分压为0.1～1.5 MPa范围内,温度低于100℃时,N80钢的腐蚀速率较小,温度在100～140 ℃时腐蚀速率明显增大.筛选的咪唑啉硫代磷酸酯类缓蚀剂JLB能有效抑制CO2腐蚀,在CO2分压为1.5MPa和温度120 ℃下,加入量为0.5%时,可使N80钢的腐蚀速率由0.206 mm/a降至0.072 mm/a.调节钻井液的pH值在8以上和添加JLB缓蚀剂是控制CO2对钻具的腐蚀的有效措施.     

GB/T31732-2015《测土配方施肥-配肥服务点技术规范》国家标准解读

测土配方施肥技术是为了达到平衡施肥的目的而开展的土壤测试、肥料试验、专用肥料配制、施肥技术指导等一整套综合性的科学施肥技术,是目前世界上广泛使用的比较先进适用的科学施肥技术。本文通过对新颁布国家标准的解读,阐述测土配方施肥服务点的技术要素,以提高测土配方施肥的质量及施用效果。同时,对标准实施监督也提出了参考建议。     

N,N-二甲基甘氨酸的合成研究

本文报道了合成N,N-二甲基甘氨酸的新方法。以甘氨酸为原料,Pd/C为催化剂,采用常温常压氢化方法,产物收率达95%。     

缓／控释肥料的研究现状及发展趋势

介绍了缓／控释肥料的定义和类型;阐述了国内外缓／控释肥料的发展历程和研究进展;展望了缓／控释肥料的发展趋势。