An economical synthesis of the major sex attractant of the oak leaf roller—cis-10-tetradecenyl acetate

The major sex attractant of the oak leaf roller (Archips semiferanus Walker),cis-10-tetradecenyl acetate (I), was synthesized in 55–62% overall yield by a highly economical route from inexpensive azelaic acid (II).Authorized as Paper No. 4779 in the Journal Series of the Pennsylvania Agricultural Experiment Station.     

Electroantennogram responses ofCampoletis sonorensis (hymenoptera: Ichneumonidae) to chemicals in cotton (Gossypium hirsutum L.)

Combined gas chromatography-electroantennogram (GC-EAG) recording ofCampoletis sonorensis (Cameron) responses to cotton plant volatile chemicals was performed.C. sonorensis antennal olfactory receptors respond differentially to green leaf, mono-, and sesquiterpene chemicals that have been identified previously in cotton. EAG depolarizations to green leaf chemicals were greater than to terpenes.     

混酸冲洗滤盘的可行性

湿法磷酸生产中，均以水为介质冲洗倾覆盘式真空过滤机的滤盘，为实现系统的污水零排放，提高倾覆盘式真空过滤机的生产能力，提出以回磷酸和硫酸配制成混酸去冲洗滤盘的方法。分析了采用该方法的诸多优点及注意事项，指出安全生产问题须认真落实。     

基于WinCC的卷烟贮叶时间动态监控系统设计

为有效控制卷烟贮叶时间,保障制丝线产品内在质量,通过WinCC开发平台,设计贮叶时间动态监控系统,集中显示各贮柜当前状态,自动计算贮存时间,对超时贮存发出报警提示.系统能够为批次化的生产调度提供科学的时间依据,避免贮叶时间不足或超时现象,有利于平衡物料温度和含水率,改善卷烟香气特性,同时减轻操作人员工作压力,实现贮叶控制的自动化、智能化.     

高纯竹叶碳苷黄酮复合纳米生物材料的制备及其结构表征（急）

采用离子交联法，以高纯竹叶碳苷黄酮制剂（碳苷总质量分数﹥90%，记为H-BLF）和芫根阴离子多糖（TP）为原料，通过ε-聚赖氨酸（ε-PL）的阳离子桥键合而成竹叶碳苷黄酮纳米混悬液（H-BLFnd），进一步在混悬液中添加8%（w/v）的γ-环糊精、经真空冷冻干燥得到纳米冻干粉（H-BLFnp），采用粒径分析、TEM、UV、FTIR、TG和DSC对其外观、性能、结构进行表征。结果表明： H-BLFnp外观为白色粉状，表面光洁平整，色泽均匀，平均粒径为（679±10.2）nm，分散系数为（0.349±0.004），包埋率为（92.39±0.34）%。     

Orientation ofMicroplitis croceipes (Hymenoptera: Braconidae) to green leaf volatiles: Dose-response curves

FemaleMicroplitis croceipes wasps were tested in a wind tunnel for their ability to orient to various concentrations of eight different green leaf volatile (GLV) substances [hexanal, (E)-2-hexenal, (E)-2-hexen-1-ol, (Z)-3-hexen-1-ol, (E)-2-hexenyl acetate, (Z)-3-hexenyl acetate, (Z)-3-hexenyl propionate, and (Z)-3-hexenyl butyrate]. Overall, the esters elicited the greatest percentage of successful orientation flights, the alcohols elicited an intermediate response, and the aldehydes elicited a low response. The semilog dose-response curves were generally hill-shaped with high responses at medium release rates and low responses at high or low release rates. For the aldehydes, positive responses occurred at all GLV release rates between 0.01 and 100 nl/min. For some alcohols and esters, positive responses occurred at release rates as low as 1 pl/min and as high as 1μl/min. These data show thatM. croceipes wasps are strongly attracted to GLVs and are capable of orienting to GLV concentrations that would occur in nature when a caterpillar feeds on a green leaf. Hence, in nature, GLVs may be important clues, enablingM. croceipes to locate their hosts.     

Physical properties and morphology of polycaprolactone/starch/pine‐leaf composites

Polycaprolactone (PCL)/starch and PCL/starch/pine‐leaf composites, which can be possibly applied as biodegradable food packaging materials with natural pine flavor, were prepared and characterized in this study. The effect of incorporating a silane coupling agent at different content levels on the physical properties and morphology of the composites was studied. To investigate the melting behavior of the composites, a differential scanning calorimetry was employed. A universal testing machine was used to investigate the tensile properties of the composites and the water absorption properties of the composites were also investigated. Scanning electron microscope was used to investigate the morphology of the composites. The physical properties and morphology of the PCL/starch and PCL/starch/pine‐leaf composites were largely affected by the composition, especially the content of the silane coupling agent. The silane coupling agent led to a much better interfacial compatibility between the PCL matrix and the fillers and resulted in better physical properties of the composites. The PCL/starch/pine‐leaf composite with the silane coupling agent showed a morphology, indicating a good interfacial adhesion between the PCL matrix and the fillers. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 928–934, 2007     

东北红豆杉中紫杉醇的含量分析

以抗癌活性成分紫杉醇作为标准物,利用高压液相色谱法分析了东北红豆杉树叶和树干的水提取物中抗癌活性成分紫杉醇的含量,确定最佳色谱条件为：色谱柱：C18,Φ4.6×250 mm;流动相：甲醇︰水︰乙腈=45︰35︰20;检测波长：225 nm;柱温：室温;流速：1.0 mL/min。结果表明：东北红豆杉树干中紫杉醇含量高于树叶。     

马铃薯叶片外植体再生系统的建立

选用马铃薯的叶片作为外植体,MS为基本培养基,采用不同浓度组合的BA和NAA对马铃薯再生系统的影响进行了研究.结果表明：最佳培养基为MS＋1.5 mg/L BA＋0.3 mg/L NAA,分化率为75%.采用该培养基研究了不同着生位置的叶片、同一着生位置叶片的不同切断以及叶片在培养基上的放置方式对马铃薯叶片再生的影响.结果表明：带有叶柄的下切断比其余叶片切断不定芽再生率高,幼嫩叶片比老化叶片再生率高.叶片再生系统的建立为马铃薯的遗传转化和工厂化育苗奠定了基础.     

天然染料银杏叶上染棉织物的媒染工艺研究

对棉织物进行银杏叶天然染料媒染染色,同时考察银杏叶媒染后织物的色牢度.探讨了明矾、硫酸铜两种媒染剂对棉织物银杏叶染色性能的影响;通过正交设计试验,确定了媒染最佳工艺条件.试验结果表明,明矾媒染最佳工艺为染色温度70℃、媒染时间25 min、媒染剂质量浓度10 g/L;硫酸铜媒染最佳工艺为染色温度60℃、媒染时间25 m...