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61.
3,5-二羟基苯甲醇的简便合成方法 总被引:1,自引:0,他引:1
以3,5 二羟基苯甲酸为原料,经酯化、酰化、硼氢化锂还原等改进步骤合成了3,5 二羟基苯甲醇,总收率达75%,提供了一条较为简便的适合于工业化生产的合成方法。 相似文献
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Degree of crosslinking and mechanical properties of crosslinked poly(vinyl alcohol) beads for use in solid-phase organic synthesis 总被引:1,自引:0,他引:1
The limited swellability in polar media of the commonly used polystyrene/divinylbenzene (PS-DVB) support materials for solid-phase organic synthesis has led to the development of novel, highly swellable hydrophilic gels designed for use in aqueous or polar media. Poly(vinyl alcohol) beads crosslinked with epichlorohydrin (PVA-EP) were prepared by a two-step inverse-suspension polymerization method. While it is known that the morphology of the resulting beads can be controlled by the ratio of EP versus PVA as well as by the pre-crosslinking time, the actual degree of crosslinking of the beads and their mechanical properties remain unknown. It is therefore the purpose of this study to evaluate the actual degree of crosslinking of beads prepared with different quantities of crosslinker in the feed by spectroscopic (Raman, nuclear magnetic resonance) and chemical (functional group loading) methods. The mechanical properties of these swollen PVA-EP beads will be evaluated by single-bead unconfined compression in solvents such as water, N,N-dimethylformamide (DMF), and tetrahydrofuran (THF) and compared to model PS-DVB beads commonly used for solid phase synthesis. 相似文献
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《Expert systems with applications》2014,41(5):2574-2581
We describe in this paper a new methodology for blood alcohol content (BAC) estimation of a subject. Rather than using external devices to determine the BAC value of a subject, we perform a behaviour analysis of this subject using intelligent systems. We monitor the user’s actions in an ordinary task and label those data to various measured BAC values. The obtained data-set is then used to train learning systems to detect alcoholic consumption and perform BAC estimation. We obtain good results on a mono-user base, and lower results with multiple users. We improve the results by combining multiple classifiers and regression algorithms. 相似文献
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Seon Jeong Kim Seoung Gil Yoon Young Moo Lee Kay Hyeok An Sun I. Kim 《应用聚合物科学杂志》2003,90(5):1389-1392
Temperature‐responsive interpenetrating polymer network (IPN) hydrogels constructed with poly(vinyl alcohol) and poly(diallyldimethylammonium chloride) using the sequential IPN method were studied. The characteristics of IPN hydrogels were investigated using the dynamic vapor sorption system. IPN hydrogels exhibited a relatively high sorption ratio, 180–360% at room temperature. The sorption ratio of hydrogels depended on temperature. Diffusion coefficients were calculated according to the Fickian Law at several temperatures. The apparent activation energy was 5.43 kJ mol?1, which corresponds to typical diffusion processes. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 1389–1392, 2003 相似文献
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Yoshitoshi Nakamura Tatsuro Sawada Akihiro Komatsu 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2002,77(10):1101-1106
In order to develop a method for converting raw starch into ethanol efficiently, direct fermentation of ozonized raw starch using a recombinant yeast was investigated. Ozonolysis was carried out as a pretreatment to convert raw starch into ethanol rapidly and efficiently, and then the effect of the ozone degradation conditions on the degree of polymerization and the amount of amylose in a raw starch was determined. Since the degree of polymerization was low and the amount of amylose was high, raw starch treated with an ozone concentration of 40 gm?3 and an ozonation time of 30 min was the material chosen for alcohol fermentation. Though the recombinant yeast could not convert the untreated raw starch, it converted the soluble starch and the ozonized raw starch at a comparatively high yield into ethanol. About 56% of the ozonized raw starch decomposed, and the ethanol concentration obtained from the ozonized raw starch was markedly greater than that obtained from untreated raw starch. The dynamic behavior of cell growth, substrate degradation, and ethanol production was examined in a continuous culture under various dilution rates, and the optimal dilution rate, ie 0.15 h?1, was determined for maximizing the ethanol productivity (amount of ethanol produced per unit time). © 2002 Society of Chemical Industry 相似文献
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