Low temperature bonding of LD31 aluminum alloys by electric brush plating Ni and Cu coatings

0Introduction Amongavarietyofbondingtechnologies,vacuum brazinghasbeenwidelyadoptedasareliablemethodfor joiningaluminumcomponents[1],whereintheAl Sialloys systemisrecognizedasthemostpopularfillermetals[2,3]. Althoughasoundjointcanbeachievedforcertainalumi…     

(Ni-P)-纳米Si3N4微粒复合刷镀工艺研究

论述了（Ni-P)-纳米Si3N4微粒复合刷镀工艺,设备及（Ni-P)-纳米Si3N4微粒复合刷镀液的组成和配制方法;研究了纳米Si3N4微粒在刷镀液中的含量,刷镀工作电压和刷镀温度对（Ni-P)-纳米Si3N4微粒复合刷镀层的影响;研究了在不同的热处理温度下复合刷镀层的硬度和耐磨性。     

SnCu钎料合金镀层钎焊连接机理及界面反应

通过在LD31铝合金表面电刷镀Ni,Cu后再沉积SnCu钎料合金镀层的钎焊实验,研究了钎料镀层的连接机理及界面反应,改进了可降低Ni层应力的电刷镀镀Ni液的配方,开发出适合镀层钎焊的SnCu钎料合金镀液,钎焊时钎料润湿为附着润湿,研究了在300℃钎焊时焊缝界面金属间化合物的生长规律,结果表明：焊缝中Cu-SnCu界面处生成了球状和棒状的Cu6Sn5金属间化合物;拉伸时焊缝主要沿着SnCu金属间化合物和富Sn相之间的界面断裂。     

The effective hydrodynamic radius of single DNA-grafted colloids as measured by fast Brownian motion analysis

Optical tweezers accomplished with fast position detection enable one to carry out Brownian motion analysis of single DNA-grafted (grafting density: ∼1000 molecules per particle, molecular weight: 4000 bp) colloids in media of varying NaCl concentration. By that the effective hydrodynamic radius of the colloid under study is determined and found to be strongly dependent on the conformation of the grafted DNA chains. Our results compare well both with recent measurements of the pair interaction potential between DNA-grafted colloids (Kegler et al. Phys Rev Lett 2008; 100:118302) and with microfluidic studies (Gutsche et al. Microfluid Nanofluid 2006; 2:381-386). The observed scaling of the brush height with the ion concentration is in full accord with the theoretical predictions by Pincus, Zhulina, Birshtein and Borisov.     

导电滑环大电流电刷成型技术研究

针对电子设备高功率密度发展需求,文中研发了一种基于表带触指式多触点电刷的导电滑环,实现了旋转机构内大电流高可靠传输能力。介绍了表带电刷组件轴向插槽式导电滑环装配新型结构、多触点自润滑电刷成型技术路线及大电流导电滑环性能测试。将银石墨触点集成至表带电刷尖端,实现电刷自润滑、大电流、高寿命性能需求,制备的导电滑环通流能力达到1 kA。该多触点自润滑电刷构件制造技术为大电流导电滑环的工程化应用奠定了基础。     

一个三维计算机水粉笔刷模型

提出一个三维计算机水粉笔刷模型,包括笔刷单元选取、颜料模拟、颜料扩散以及整体控制４部分,该模型结构简单开可以直接应用到传统三维曲面上,给了的结果具有手工绘制水粉画的效果,文中图例表明该模型的模拟效果令人满意。     

基于Bi-Laplacian润饰图像的盲鉴别算法

图像润饰是一种广泛应用的图像篡改手段。为了对润饰的图像实施盲检测,提出了一种图像盲鉴别算法。该算法首先查找图像中每个分块并把其插入到KD树中,搜索到值相同或最近的粗略匹配块,然后使用位置向量的分层聚类法群集块对消除杂散配对,最后应用7-tap拉普拉斯过滤器并统计可疑块的零连通分量来消除误报,从而定位出精确的润饰篡改区域。实验表明,该方法能有效精确地识别出修复刷对非压缩图像和高品质压缩图像等一类图像的润饰篡改技术的使用。当应用到压缩级别较高的图像时,如果润饰的区域足够大,依然会获得准确的结果。     

Synthesis of thermoresponsive poly(N-isopropylacrylamide) brush on silicon wafer surface via atom transfer radical polymerization

Thermoresponsive poly(N-isopropylacrylamide) [poly(NIPAM)] brush on silicon wafer surface was prepared by combining the self-assembled monolayer of initiator and atom transfer radical polymerization (ATRP). The resulting polymer brush was characterized by in situ reflectance Fourier transform infrared spectroscopy, atomic force microscopy and ellipsometry techniques. Gel permeation chromatography determination of the number-average molecular weight and polydispersity index of the brush detached from the silicon wafer surface suggested that the surface-initiated ATRP method can provide relatively homogeneous polymer brush. Contact angle measurements exhibited a two-stage increase upon heating over the board temperature range 25-45 °C, which is in contrast to the fact that free poly(NIPAM) homopolymer in aqueous solution exhibits a phase transition at ca. 34 °C within a narrow temperature range. The first de-wetting transition takes place at 27 °C, which can be tentatively attributed to the n-cluster induced collapse of the inner region of poly(NIPAM) brush close to the silicon surface; the second de-wetting transition occurs at 38 °C, which can be attributed to the outer region of poly(NIPAM) brush, possessing much lower chain density compared to that of the inner part.     

偶联剂处理对树脂碳刷结合性能的影响

在树脂结合碳刷的工艺中,将石墨粉或焦炭粉先用偶联剂预处理后再加入配料中,研究了偶联剂种类(KH550,KH570,NDZ-311,NDZ-131)及用量、热处理温度等对树脂石墨电刷抗压强度的影响,并对试样微观组织进行了观察.结果表明,加入的偶联剂,能使电刷的抗压强度增加,硅烷偶联剂用于水溶性酚醛树脂/沥青焦配料,能得到高抗压强度的电刷制品;并优选出了偶联剂KH570,其最佳加入值为石墨粉含量的0.5%～1.0%.     

Powder coatings technology: new developments at the turn of the century

The growth of the powder coating business is affected by the toxicological effects of the raw materials used in the coating formulation and the saturation of the present market for powder coatings, being limited to general metal applications only. This has a strong influence on the long-term research programmes at both raw materials suppliers and powder paint producers. In the last decade of the 20th century, we witness appearance of several new types of toxicologically-safe powder coating systems on the commercial scale. At the same time, there is strong evidence of efforts to penetrate new market fields where powder coatings are not typically used. This includes the markets for automotive clear top coatings, can and coil coatings, coatings for industrial wood, plastics and paper. The new developments in the chemistry of powder coatings are followed by changes and improvements in the production technology for powder coatings as well as developments of new application techniques. This paper summarises the research work on chemistry, production and application technology of powder coatings and tries to extrapolate the tendencies in the years to come in order to predict the achievements and the impacts on the paint industry.