花生粕曲奇饼的加工工艺研究

以花生粕、低筋面粉为基料,研究了花生粕与面粉的比例、黄油、白砂糖、泡打粉对花生粕曲奇饼干品质的影响。在单因素试验的基础上,通过正交试验得出产品的最佳配方为:低筋面粉与花生粕(1∶1)41.6%、黄油40%、白砂糖18%、泡打粉0.4%、鸡蛋60 g。最佳烘烤工艺为:面火温度180℃、底火温度100℃、时间为7 min。     

Utilization of protein concentrates from ungerminated and germinated fluted pumpkin (Telfairia occidentalis Hook) seeds in cookie formulations

Cookies (soft type biscuits) were produced from blends of wheat flour containing graded levels (0–25%) of protein concentrates prepared from ungerminated and germinated fluted pumpkin (Telfairia occidentalis Hook) seeds and evaluated for nutritional, baking and sensory properties. Protein quality was investigated using weanling albino rats fed diets that were formulated to supply 10% protein using cookie samples, with casein as a control. Cookies produced from blends containing protein concentrates from germinated seeds had higher contents of crude protein and lower levels of polyphenol and phytic acid, compared with cookies supplemented with concentrates from ungerminated seeds. The use of up to 15% concentrate from ungerminated seeds in the blends produced cookies with spread ratio, hardness, colour and flavour similar to the 100% wheat flour (control) cookies. Cookies supplemented with concentrates from germinated seeds at 15–25% levels were nutritionally comparable to diets based on casein, but at the expense of acceptability. Copyright © 2004 Society of Chemical Industry     

Geometric and statistical techniques for projective mapping of chocolate chip cookies with a large number of consumers

The so-called rapid sensory methods have proved to be useful for the sensory study of foods by different types of panels, from trained assessors to unexperienced consumers. Data from these methods have been traditionally analyzed using statistical techniques, with some recent works proposing the use of geometric techniques and graph theory. The present work aims to deepen this line of research introducing a new method, mixing tools from statistics and graph theory, for the analysis of data from Projective Mapping. In addition, a large number of n = 349 unexperienced consumers is considered for the first time in Projective Mapping, evaluating nine commercial chocolate chips cookies which include a blind duplicate of a multinational best-selling brand and seven private labels. The data obtained are processed using the standard statistical technique Multiple Factor Analysis (MFA), the recently appeared geometric method SensoGraph using Gabriel clustering, and the novel variant introduced here which is based on the pairwise distances between samples. All methods provide the same groups of samples, with the blind duplicates appearing close together. Finally, the stability of the results is studied using bootstrapping and the RV and Mantel coefficients. The results suggest that, even for unexperienced consumers, highly stable results can be achieved for MFA and SensoGraph when considering a large enough number of assessors, around 200 for the consensus map of MFA or the global similarity matrix of SensoGraph.     

杨梅提取物抑制二羰基化合物活性研究

目的 分离纯化杨梅果实提取物并考察不同组分对模型及饼干中甲基乙二醛(methylglyoxal, MGO)、乙二醛(glyoxal, GO)的抑制效果。方法 乙醇浸提制备杨梅果实粗提物(crude extract, CE),采用AB-8大孔吸附树脂,以不同体积分数的乙醇(20%、40%、60%)洗脱,得到三种杨梅提取物;采用NaNO₂- Al(NO₃)₃-NaOH比色法、pH示差法、液相色谱-质谱法测定提取物中花色苷、总黄酮含量和主要成分,并用气相色谱法考察其对模型和曲奇中MGO/GO的抑制活性。结果 40%乙醇组分F₁得率最高,活性最好,主要成分为矢车菊素-3-O-葡萄糖苷(cyanidin-3-O-glucoside, C-3-Glu)和杨梅素-3-O-鼠李糖苷(myricetin-3-O-rhamnoside, M-3-Rha);60%乙醇洗脱组分F₂成分主要为槲皮素-3-O-鼠李糖苷(quercetin-3-O-rhamnoside, Q-3-Rha);当曲奇中提取物添加量为0.4%时,F_1、F₂对MGO和GO均有抑制活性,其中F₁效果最佳,分别为61.5%和40.4%。结论 杨梅果实提取物具有良好清除MGO/GO的能力,为其作为添加剂应用于抑制食品加工中的MGO和GO提供了一定的理论基础。     

Inhibition of lipid oxidation in fried chips and cookies by Majorana syriaca

This study evaluates the antioxidant effectiveness of a natural extract obtained from Majorana syriaca in fried and baked foods. Majorana syriaca was extracted with ethyl acetate (yield 129 g kg^?1, dry basis) and the extract was added to refined corn oil at a concentration of 500 ppm. The oil was used in deep frying of potato chips at 185 °C and in making baked cookies. Potato chips and cookies were further subjected to accelerated oxidation at 70 °C. The protection of the frying oil was moderate as indicated by the polar content and conjugated dienes (CD) measurements, however, a remarkable improvement of the oxidative stability of the fried chips was observed through the decrease of peroxide value (PV) and CD by 59–72% and 51–79%, respectively, compared to samples with no additive. Also, the PV and CD of cookies decreased by 79% and 72%, respectively.     

Extraction of polycyclic aromatic hydrocarbons from cookies: A comparative study of ultrasound and microwave-assisted procedures

The chromatographic determination of 15 polycyclic aromatic hydrocarbons (PAHs) in cookies has been improved in order to obtain a fast method with a low limit of detection through the combination of microwave-assisted extraction (MAE), oil saponification and solid-phase extraction clean-up before the injection of purified extracts in a C18 201TP52 (5 µm, 250 ×?2.1 mm) column. Using acetonitrile–water as mobile phase, with a 50% to 95% w/w acetonitrile gradient for a fixed flow of 0.250 ml min^?1, 15 PAHs were separated in 45 min. The column temperature was maintained at 15°C; and fluorimetric detection was made at a fixed excitation wavelength of 264 nm and emission measurements at the best wavelength for each analyte, from 352 nm for 11H-benzo[b]fluorene to 500 nm for indeno[1,2,3-c,d]pyrene. Recoveries for all 15 PAHs varied between 96 ±?4 and 105% ±?4%; and the limits of detection ranged from 0.015 ng g^?1 for chrysene to 0.7 ng g^?1 for phenantrene. Results were compared with those obtained by conventional Soxhlet extraction during 8-h refluxing with toluene, demonstrating that the methodology proposed is appropriate to quantify PAHs in cookies. Furthermore, the microwave-assisted method was faster and used less solvent than the conventional and ultrasound-assisted methods. The extraction time was reduced to 9 min compared with the 8 h required for Soxhlet extraction and 60 min required for ultrasound-assisted treatment, and the solvent consumption has been reduced to 25 ml compared with the 155 and 90 ml required using Soxhlet and ultrasound, respectively.