Preparations of nanosized TiO2 in reverse microemulsion and their photocatalytic activity

Nanosized titania sol has been produced by the controlled hydrolysis of titanium tetraisopropoxide (TTIP) in sodium bis(2-ethylhexyl)sulfosuccinate (AOT) reverse micelles. The physical properties, such as surface area, crystallite size and crystallinity according to R and W₀ ratio, have been investigated by TEM, XRD, BET, FT–IR, TGA and DTA. In addition, the photocatalytic decomposition of p-nitrophenol has been studied by using a batch reactor in the presence of UV light in order to compare the photocatalytic activity of prepared nanosized titania. It is shown that the anatase structure appears in the 300–600 °C calcination temperature range and the transformation of anatase into rutile starts above 700 °C. The crystallite size increases with increasing R and W₀ ratio but W₀ ratio shows a stronger effect on the crystallite size than R ratio. In the photocatalytic decomposition of p-nitrophenol, the photocatalytic activity is mainly determined by the crystallinity of titania. In addition, the titania calcined at 500 °C shows the highest activity on the photocatalytic decomposition of p-nitrophenol() and the pure anatase structure.     

钢筋混凝土结构内的钢筋腐蚀监测

用钢筋混凝土修建的建筑物和构筑物，因受外界因素的影响，其内部钢筋可能会受到腐蚀而生锈，锈蚀严重者将危及安全。根据钢筋在混凝土内的锈蚀是一个电化学过程的特点，在不损伤钢筋混凝土结构的条件下，利用腐蚀监测仪，测量钢筋混凝的电化学特性值，并以此特性值绘制等值线图，利用该图能正确评估混凝土内钢筋受腐蚀的情况。     

Whey Drying on Porous Carriers

Whey is an undurable product. treated very often as a waste which pollutes the natural environment. Whey which is a valuable source of protein, lactose, vitamins and mineral salts should be utilized completely. The present paper is a proposal of whey drying on porous carriers. It is proved experimentally that the proposed drying method guarantees good product quality.     

高喷煤比操作对焦炭劣化的影响

为考查提高喷煤量对焦炭在炉内劣化的影响,在宝钢高炉上进行了风口取样研究.结果表明,喷煤量达到200 kg/t以上时焦炭劣化严重.高炉生产实绩回归显示,焦炭的热性能对高炉透气性的影响比冷强度显著.分析认为焦炭热性能指标CRI、CSR对高炉高煤比操作更重要.借此还提出了提高喷煤量和改善焦炭质量需加强研究的课题.     

板锥网壳结构的动力特性分析

板锥网壳结构是一种受力性能合理 ,技术经济效益良好的新型空间结构形式。对板锥网壳结构的自振特性及其影响因素进行了系统分析研究 ,并与普通双层网壳结构进行比较 ,得出了可应用于工程实践的重要结论     

CARR水平孔道的设计特点

介绍了中国先进研究堆(CARR)水平孔道的用途、在堆本体的布置、水平孔道结构设计及设计方面的特点。     

苏州园林的色彩

造园者非常重视运用色彩美化景物，刻意创作“以色传神、以色抒情”的作品。苏州园林怡心悦目的色彩引人入胜。苏州园林建筑物常以淡雅宁静的灰色和白色为其基本色调。苏州园林不用大红大绿蓝紫等颜色，更少施彩绘，色彩以淡雅为其独特风格。     

工程结构动态特性智能优化设计研究

本文针对在传统结构优化设计中，优化过程复杂和费时的问题，采用神经网络的智能算法对结构进行动态优化设计，并给出了具体的设计方法。以门座起重机筒型支柱结构为例，应用此方法对其进行了动态优化设计计算，从而证明了该算法的有效性。     

内热式液态合金离子源

本文介绍了一种实用的液态合金离子源结构，我们利用本结构研制成功了Ａｕ－Ｓｉ和Ａｕ－Ｓｉ－Ｂｅ液态合金离子源，测出了它们的发射特性。     

QFD质量职能扩展简介

介绍ＱＦＤ（质量职能扩展）的发展历史及其具体的操作过程。