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61.
Dennis J. O’Brien Gerard E. Senske 《Journal of the American Oil Chemists' Society》1994,71(9):947-950
Utilization of lipids containing eicosapentaenoic acid (EPA) produced by microorganisms requires processes for their efficient
recovery from microbial cells. Recovery of EPA from mycelia of the fungusPythium irregulare by solvent extraction with hexane-isopropanol (HIP) in a pilot-plant colloid mill was investigated. Extraction efficiencies
of 96% for lipid and EPA were achieved with a 3∶2 (vol/vol) HIP mixture by milling wet, filtered mycelia for 5 min at a solvent/dry
solids ratio of 100 L/kg. The process yielded a crude extract that contained up to 96% lipid and an EPA content as high as
24% (with no selectivity for EPA). 相似文献
62.
Hiromi Yoshida Mikiko Tatsumi Goro Kajimoto 《Journal of the American Oil Chemists' Society》1991,68(8):566-570
Effects of microwave heating on the oxidative stability ofd-tocopherols were studied in relation to the production of fatty acids in oils. During microwave heating, the stability of
tocopherols decreased in the orderδ>β>γ>α. This order did not depend on the types of ethyl esters of fatty acids or oils present. But, the shorter the chainlength
and the lower the degree of unsaturation of the fatty acid ethyl esters, the greater was the reduction in amount of individual
tocopherols. A similar tendency was observed when tocopherol-stripped vegetable oils, with equimolar mixtures of tocopherols
added, were treated under the same conditions. The reduction in tocopherols became greater with increasing levels of free
fatty acids. 相似文献
63.
腐殖(植)酸(Humic Acid,以下简称HA)是天然有机化合物。在农业应用上十分广泛,主要有土壤改良剂、肥料、农药、植物生长剂、兽药、饲料添加剂、水产养殖剂等产品。从狭义的角度说,食品生产源头指土、水、肥、药、种等主要生产环节的硬条件。HA与食品生产源头诸要素之问关系密切。HA与土壤:土壤是种植业依赖的生命基础;HA是土壤有机质中的重要组成部分,也是最活跃的部分。HA与水:水是生命之源;HA在水生体系中普遍存在,是转运大多数生命必需物质甚至毒性物质的一种非常好的工具。HA与肥料:肥料是植物的粮食;HA在改良肥料、增加肥效、提高肥料利用率、协调各种营养等方面具有非常重要的作用。HA与农药:农药是植物的保护伞;HA具有提高农药药效、降低农药毒性、保护农业环境的基本条件。HA与种苗:种苗不好,作物不保;HA是孵化种苗的“保育剂”。除土、水、肥、药、种外,HA因其具有生理活性特征,而与种植业相关的诸多因素均有良好的协同作用。在此基础上,由HA开发的农用产品,涉足改土、活水、制肥、制药、种苗处理及其他衍生制剂等6大类产品,足以构筑起立体农业的防护体系,也是构筑食品源头安全的最佳选择。 相似文献
64.
Pheromone components for many lepidopteran species are produced by the use of unique chain-shortening and 9, 10, and 11 desaturase systems. Correlations in the Tortricidae indicate that the pheromone components derived from 9 and 01 desaturases are found in the more primitive species (those possessing morphological plesiomorphies). The precise blend ofZ andE acetates in a number of species is regulated in the final reduction sequence from acyl intermediates. Preliminary research has been conducted on the characterization of the various desaturase enzymes used and on the important blend regulating sequence. Initial purification work on the 11 desaturase enzyme found in the cabbage looper moth is reported. 相似文献
65.
66.
Yoshitsugu Kosugi Tsutomu Kunieda Naoki Azuma 《Journal of the American Oil Chemists' Society》1994,71(4):445-448
Rice bran oil containing 30–50% free fatty acid was continually converted to an oil containing more than 75% of triacylglycerol
(TG) by means of immobilized lipase. The reaction was carried out at 60°C for 24 h with dehydration and reactant mixing by
dry nitrogen flow under a positive nitrogen atmosphere. Enzymatic TG synthesis with evaporation by heating was not suitable
because of the increasing peroxide value of the oil.
Part of this article was presented at the annual meeting of the Japan Oil Chemists' Society at Sendai, Japan, October, 16,
1990. 相似文献
67.
68.
Sakina Khatoon Sunki Reddy Yella Reddy 《European Journal of Lipid Science and Technology》2005,107(11):786-791
Speciality plastic fats with no trans fatty acids suitable for use in bakery and as vanaspati are prepared by interesterification of blends of palm hard fraction (PSt) with mahua and mango fats at various proportions. It was found that the interesterified samples did not show significant differences in solid fat content (SFC) after 0.5 or 1 h reaction time. The blends containing PSt/mahua (1:1) showed three distinct endotherms, indicating a heterogeneity of triacylglycerols (TG), the proportions of which altered after interesterification. The SFC also showed improved plasticity after interesterification. Similar results were observed with other blends of PSt/mahua (1:2). These changes in melting behavior are due to alterations in TG composition, as the trisaturated‐type TG were reduced and the low‐melting TG increased after interesterification. The blends containing PSt/mango (1:1) showed improvement in plasticity after interesterification, whereas those containing PSt/mango (2:1) were hard and showed high solid contents at higher temperature and hence may not be suitable for bakery or as vanaspati. The blends with palm and mahua oils were softer and may be suitable for margarine‐type products. The results showed that the blends of PSt/mahua (1:1, 1:2) and PSt/mango (1:1) after interesterification for 1 h at 80 °C showed an SFC similar to those of commercial hydrogenated bakery shortenings and vanaspati. Hence, they could be used in these applications in place of hydrogenated fats as they are free from trans acids, which are reported to be risk factors involved in coronary heart disease. For softer consistency like margarine applications, the blends containing palm oil and mahua oil are suitable. 相似文献
69.
V. Spitzer S. A. de L. Bordignon E. P. Schenkel F. Marx 《Journal of the American Oil Chemists' Society》1994,71(12):1343-1348
In addition to some usual fatty acids, the seed oil ofJodina rhombifolia (Santalaceae) contains nine acetylenic fatty acids [9-octadecynoic acid (stearolic acid) (1.1%),trans-10-heptadecen-8-ynoic acid (pyrulic acid) (20.1%), 7-hydroxy-trans-10-heptadecen-8-ynoic acid (2.3%),trans-10,16-heptadecadien-8-ynoic acid (0.7%), 7-hydroxy-trans-10,16-heptadecadien-8-ynoic acid (0.1%),trans-11-octadecen-9-ynoic acid (ximenynic acid) (20.3%), 8-hydroxy-trans-11-octadecen-9-ynoic acid (12.2%),trans-11,17-octadecadien-9-ynoic acid (1.5%), 8-hydroxy-trans-11,17-octadecadien-9-ynoic acid (1.3%), 9-hydroxystearic acid (<0.1%) and 9,10-epoxystearic acid (0.7%)]. The fatty acids
have been analyzed by gas chromatography/mass spectrometry of their methyl ester and 4,4-dimethyloxazoline derivatives. The
hydroxy fatty acid methyl esters have been examined also as trimethyl-silyl ethers. Furthermore, the fatty acid methyl esters
(FAME) have been fractionated according to their polarity (FAME-A: nonhydroxy; FAME-B: hydroxy fatty acids) and to their degree
of unsaturation (FAME-A1/A2; FAME-B1/B2) by preparative thin-layer chromatography and argentation chromatography, respectively.
All of these fractions have been analyzed by ultraviolet and infrared spectroscopy, and the fractions FAME-A and FAME-B have
been analyzed further by nuclear magnetic resonance (1H,13C, 2D H/C, attached proton test) spectroscopy and gas chromatography/mass spectrometry.
This work is dedicated to the 65th birthday of Prof. Dr. K. Pfeilsticker, Institut of Food Science, University Bonn (Germany). 相似文献
70.
Igor V. Kovalenko Glen R. Rippke Charles R. Hurburgh 《Journal of the American Oil Chemists' Society》2006,83(5):421-427
A key element of successful development of new soybean cultivars is availability of inexpensive and rapid methods for measurement
of FA in seeds. Published research demonstrated applicability of NIR spectroscopy for FA profiling in oilseeds. The objectives
of this study were to investigate the applicability of NIR spectroscopy for measurement of FA in whole soybeans and compare
performance of calibration methods. Equations were developed using partial least squares (PLS), artificial neural networks
(ANN), and support vector machines (SVM) regression methods. Validation results demonstrated that (i) equations for total
saturates had the highest predictive ability (r
2=0.91–0.94) and were usable for quality assurance applications, (ii) palmitic acid models (r
2=0.80–0.84) were usable for certain research applications, and (iii) equations for stearic (r
2=0.49–0.68), oleic (r
2=0.76–0.81), linoleic (r
2=0.73–0.76), and linolenic (r
2=0.67–0.74) acids could be used for sample screening. The SVM models produced significantly more accurate predictions than
those developed with PLS. ANN calibrations were not different from the other two methods. Reduction in the number of calibration
samples reduced predictive ability of all equations. The rate of performance degradation of SVM models with sample reduction
was the lowest. 相似文献