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141.
142.
Development of nano indium tin oxide (ITO) grains by alkaline hydrolysis of In(III) and Sn(IV) salts
Indium tin oxide (ITO) nano powders of different compositions (In: Sn = 90: 10, 70: 30 and 50: 50) were prepared by heat treatment
(300-450°C) of mixed hydroxides of In(III) and Sn(IV). The hydroxides were obtained by the reaction of aq. NH3 with mixed aq. solutions of In(NO3)3 and SnCl4. FTIR and TG/DTA studies revealed that powders existed as In(OH)3H2O—SnO3H2H2O in the solid state and then they transformed to In2O3—SnO2 via some metastable intermediates after 300°C. Cubic phase of In2O3 was identified by XRD for the oxides up to 30% of Sn. Particle size measurements of the solid dispersed in acetone and SEM
study for microstructure showed that the oxides were in the nano range (55-75 nm) whereas the size range determined from Debye-Scherrer
equation were 11–24 nm. 相似文献
143.
144.
Yaping KeLU 《材料科学技术学报》2002,18(6):492-496
In this paper,glass transition and thermal stability of the Zr-Al-Cu-Ni metallic glasses were investigated by using electrical resistance measurement(ERM),DSC and X-ray diffraction techniques.The experimental results show that the ERM is capable of detecting the glass transition of the amorphous alloys and can help to distinguish the crystallization products of the Zr-Al-Cu-Ni metallic glasses owing to the difference of the electrical resistivity between the precipitation phases. 相似文献
145.
The objective of the present study is to develop multi-functioned coating to the components, which are made of copper with electroplated Ni and are widely used for steel making industry. In this paper, we report the mechanical and thermal properties of Ni based superalloys with carbide sprayed by high velocity oxygen fuel (HVOF), and the detailed effects of sprayed material, spraying conditions, and initial powder structure on these properties. It was found that, among commercial Ni self-fluxing alloys (without fusing treatment), coating with a carbon content of 0.58 mass% had the most preferable properties, with a good balance of the hardness, strength, and thermal shock resistance. The thermal shock resistance depended not only on the strength of the coating but also on the volume contraction when tested at high temperatures. For the several developed Ni based superalloys with carbide, Ni20Cr8Mo5Fe–WC and Ni16Cr15Mo3–WC demonstrated the prominent adhesion strength and thermal shock resistance with high Galvanic corrosion resistance through optimized spraying condition. Also, 20 mass% NiCr–Cr3C2 coating sprayed by using employed relatively small primary particle succeeded in achieving the multi-superior properties; high adhesion strength, high corrosion resistance and thermal shock resistance. 相似文献
146.
147.
The gelatinisation temperatures, pasting characteristics and enzymic susceptibilities in the temperature range 48–72°C of normal, high amylose, low amylose and zero amylose barley starches were determined. Normal starches had the lowest gelatinisation temperatures, but low and zero amylose starches had the lowest pasting temperatures. Normal starches were the most readily soluble in water at 48–60°C in the presence of a mixture of α‐amylase, β‐amylase and limit dextrinase and were most readily broken down to reducing sugars by these enzymes. High amylose starch was the most resistant to enzymic hydrolysis in the temperature range 48–72°C and, hence, produced the lowest level of reducing sugars. 相似文献
148.
钢铁表面黑色转化膜处理技术 总被引:1,自引:1,他引:0
黑色转化膜技术是目前较为先进的钢铁表面处理技术 ,本文试验研究了一种新工艺 ,提出了TB值的概念 ,通过控制TB值即可控制处理液的质量 ,获得性能优良的转化膜。此工艺性能可靠 ,可操作性强 ,并可应用于激光热处理前的预处理。 相似文献
149.
Tatsuro Kijima Kouji Ohshima Hideo Kise 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1994,59(1):61-65
Racemic amino acid esters were optically resolved via hydrolysis in organic solvents by the catalysis of an industrial alkaline protease, “Alcalase”. The products which were composed mainly of L-amino acids were insoluble and easily separated by filtration. The activity of the enzyme and enantiomeric excess of the products were significantly dependent on the nature of solvent and the water content in the reaction media. Generally, high values of enantiomeric excess were obtained at low water contents. Many natural and unnatural amino acids were resolved by this method. 相似文献
150.
本文描述用离子束透过钽金属膜进行混合和快速热处理方法来形成钽的硅化物.用溅射方法在P型硅衬底上淀积一层金属钽,然后用砷离子束透过钽金属模进行混合,采用快速热处理后形成了平整的硅化钽薄层.使用厚度为500埃的钽金属膜,得到钽的硅化物薄层电阻为5.5Ω/□.研究了砷离子能量、剂量及钽膜厚度对钽的硅化物薄层电阻的影响.用透射电镜和台阶仪对所形成的硅化钽进行了分析和厚度测量. 相似文献