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91.
1,3,5‐Triglyceratetriazine [first tier (G1)] and tri(1,3,5‐triglycerate) triazine [second tier (G2)] dendrimers were prepared with 1,3,5‐trichlorotriazine and sodium glycerate in a 1 : 3 mass ratio in an ethanolic medium.G1 and G2 were amorphous, white, solid substances. Their structures were elucidated with IR, 1H‐NMR, and 13C‐NMR, and their thermal stability was studied with thermogravimetric analysis. The activation energy was calculated with the Freeman–Carroll model. Densities, viscosities, and surface tensions for 0.01–0.08 mol/kg aqueous solutions increased at 0.01 mol/kg for sodium glycerate, 1,3,5‐trichlorotriazine, 1,3,5‐triazine triglycerate chloride, G1, and G2. These values were measured at 298.15 K. The apparent molal volume, reduced viscosity, and inherent viscosity were calculated from the densities and viscosities, respectively. The data were regressed for the limiting densities, limiting apparent molal volumes, intrinsic viscosities, limiting inherent viscosities, and limiting surface tensions for solute–solvent interactions. The positive limiting apparent molal volume values were noted in the order of G2 > 1,3,5‐triazine triglycerate chloride > G1 > 1,3,5‐trichlorotriazine > sodium glycerate, with weaker hydrophilic intermolecular interactions of G2. The higher intrinsic viscosity and limiting inherent viscosity values for G2 implied stronger G2–H2O hydrophilic interactions, and the higher limiting apparent molal volume of G2 indicated slightly higher dynamic conformational changes in comparison with G1, with stronger structural activities. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
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93.
炉顶红外摄像装置在新钢6号高炉上的安装及应用 总被引:2,自引:0,他引:2
阐述了高炉炉顶红外摄像装置的安装及应用。该装置对及时了解和掌握高炉炉喉的料面情况、煤气流的分布状况,对指导高炉操作、维护炉况顺行和稳定,改善各项技经指标,发挥了重要作用。 相似文献
94.
95.
本文简述了红外热成像技术用于厚膜混合集成电路热设计中的理论与实验方法,并讨论了结果。 相似文献
96.
本文介绍了用αβ谱仪系统同时测量αβ谱、实现Rn/Th子体补偿、确定超铀α核素气溶胶体积活度及人工放射性气溶胶总β体积活度的技术途径。利用RaA、RaC′a峰的二段时间计数可确定空气中RaA、RaB、RaC的气溶胶体积活度,相应的,也能给出RaB、RaC对总β计数的贡献。根据一般环境条件下的平衡比,用ThC′的。计数修正Th子体对αβ测量的影响。 ̄[239]pu或/和 ̄[241]Am人工核素的α计数,可通过两段时间分别扣除RaA、RaC′拖尾的方法确定;β计数分别扣除Rn/Th子体β贡献即可确定。在本文规定的测量条件下,对室内天然Rn子体水平在15Bq/m ̄3以下,超铀α核素气溶胶体积活度的测量下限可达到0.1Bq/m ̄3;即使在75Bq/m ̄3环境下,人工核素总β的测量下限也可达lBq/m ̄3以下。 相似文献
97.
A spatially resolved infrared (IR) imaging technique to monitor the linear adsorbed CO coverage on supported catalyst surface combining an IR bandpass filter and an IR thermography camera has been developed. Images acquired during the CO adsorption/desorption and ignition indicate that the technique provides an excellent method to image the change of surface coverage with a spatial resolution. It is expected that the combination of infrared thermography with spatially resolved imaging of surface coverage will provide a deeper insight in the dynamics of spatio-temporal patterns on heterogeneous catalysts. 相似文献
98.
David Lloyd Suzie Morrell Helle N. Carlsen Hans Degn Phillip E. James Christopher C. Rowlands 《Yeast (Chichester, England)》1993,9(8):825-833
Saccharomyces cerevisiae HSc was grown with ethanol at concentrations up to 10% (v/v). The immediate effects of additions of externally added ethanol on CO2 production and O2 consumption of washed organisms were studied by stopped-flow membrane inlet quadrupole mass spectrometry. Fermentative activities of organisms grown with ethanol (0–5% v/v) showed similar sensitivities to inhibition by ethanol, whereas those grown with 10% (v/v) ethanol had become protected and were markedly less sensitive. The fluidity of subcellular membrane fractions was measured by determination of the temperature dependence of the rotational order parameter of the spin label 5-doxyl stearic acid (free radical) by electron spin resonance. Mitochondria prepared from yeasts grown with 0, 7 and 9% (v/v) ethanol showed similar overall fluidity, although differences in temperature-dependent behaviour indicate altered lipid composition or lateral phase separations. On the other hand the microsomal fraction from organisms grown with 9% ethanol showed a remarkable increase in fluidity. These data suggest that the protective effects of growth with ethanol near the limit of tolerance on fermentative activities may arise from altered plasma membrane fluidity properties. 相似文献
99.
Research presented in this paper deals with the systematic examination, development, and evaluation of a novel multimodal registration approach that can perform accurately and robustly for relatively close range surveillance applications. An analysis of multimodal image registration gives insight into the limitations of assumptions made in current approaches and motivates the methodology of the developed algorithm. Using calibrated stereo imagery, we employ maximization of mutual information in sliding correspondence windows that inform a disparity voting algorithm to demonstrate successful registration of objects in color and thermal imagery. Extensive evaluation of scenes with multiple objects at different depths and levels of occlusion shows high rates of successful registration. Ground truth experiments demonstrate the utility of the disparity voting techniques for multimodal registration by yielding qualitative and quantitative results that outperform approaches that do not consider occlusions. A basic framework for multimodal stereo tracking is investigated and promising experimental studies show the viability of using registration disparity estimates as a tracking feature. 相似文献
100.
金属表面柴油机油沉积物的反射红外光谱法研究 总被引:1,自引:1,他引:0
利用镜反射红外光谱法研究了CC级柴油机油中添加剂对成漆板板面漆膜组成的影响:考察了成漆板漆膜组成与Cat.1H2活塞环台漆膜组成的相关性。试验结果对柴油机油的研制和应用有一定指导作用。 相似文献