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101.
The maleic anhydride functionalized graphene oxide (GO-MA) is fabricated by an efficient and solvent-free Diels–Alder reaction. Polyethylene terephthalate (PET)/thermotropic liquid crystal polyester (TLCP), PET/TLCP/GO-MA, PET/TLCP/aminated multi-walled carbon nanotubes (MWCNTs-NH2), and PET/TLCP/GO-MA/MWCNTs-NH2 composite fibers are systematically melt-spun. The structure and compatibilizing effects of GO-MA and MWCNTs-NH2 on the mechanical, thermal, and crystallization properties of the composite fibers are indicated. The non-isothermal crystallization kinetics and X-ray diffraction (XRD) data show that TLCP and nanofillers can change the crystalline morphology of PET. The mechanical properties of the fibers rise with increasing TLCP content. The tensile strength 929 MPa and modulus 17.5 GPa of the fibers with 7 wt% TLCP and 0.25 wt% nanofillers (0.1 wt% GO-MA and 0.15 wt% MWCNTs-NH2) are significantly higher than those with 7 wt% TLCP (tensile strength 622 MPa and modulus 16.1 GPa) and even higher than those with 15% TLCP (tensile strength 836 MPa, and modulus 18.0 GPa). When the GO-MA and MWCNTs-NH2 co-exist, the anti-dripping phenomenon is improved. Therefore, the TLCP, GO, and MWCNTs synergistically strengthens the mechanical properties. This is promising for the industrial fabrication of high-strength fibers. 相似文献
102.
Weiyan He Xia Guo Xiaobing Zhao Jinrong Liu 《International Journal of Applied Ceramic Technology》2021,18(3):880-888
Nanopowders of pure zirconia have been synthesized using citric acid (CA)-assisted lamellar liquid crystal template method. The microstructure of the zirconia powder prepared at the different mole ratios of CA to zirconium oxynitrate (ZN) was characterized by FT-IR, X-ray diffraction (XRD), laser particle size analyzer, Raman spectroscopy, and scanning electron microscope (SEM) methods. The phase structure of the sodium dodecyl sulfate (SDS)/C10H21OH/H2O system before and after adding mixing solution CA and ZN was determined by POM (Polarizing Optical Microscope). The results show that lamellar structure of the SDS/C10H21OH/H2O system after adding mixing solution CA and ZN is stable. The presence of CA inhibits agglomeration and growth of zirconia particle. The crystallite size of zirconia powders decreases and agglomerates lowly with addition of CA. Fourier transform infrared spectrometry (FI-IR) analyses reveal that the structure of chelating organic complex is maintained in zirconia structure at high-temperature calcination to cause oxygen vacancies which stabilizes the tetragonal phase of zirconia. The zirconia powders remained the single metastable tetragonal phase at the molar ratios of CA to ZN ranging from 1:3 to 5:1. The crystallite size of zirconia with spherical morphology varied from 32.2 to 20.1 nm with the increase of the molar ratio of CA to ZN in the range of 1:3 to 5:1. 相似文献
103.
SiCFIBER/ALUMINIUMPREFORMWIRESFABRICATEDBYULTRASONICLIQUIDINFILTRATIONPROCESSZhangChenge;WangLingsen(CentralSouthUniversityof... 相似文献
104.
研究了Ce对Al—16%Si合金熔体粘滞性的影响。结果表明:Ce的加入增加了合金熔体的粘度,且随着Ce含量的增加粘度值也增加。结合加入Ce的Al—16%Si合金氢含量的变化、凝固组织和DSC曲线研究了熔体结构的变化,分析了粘度与液态结构变化之间的关系。 相似文献
105.
液膜法分离富集,测定水中微量锶 总被引:1,自引:0,他引:1
用乳状液膜体系对锶进行分离富集,该体系包括协同流动载体(PMBP,TBP),表面活性剂(SPAN80)增强剂(丙三醇)溶剂(正己烷)和内相(1.2mol/L的盐酸溶液),实验表明,在适宜的条件下,锶的富集效率可达99.5%以上,而在此条件下许多共存离子,如Fe^3+,Al^3+,Ca^2+,Mg^2+,Ba^2+,Cr^3+,CO^2+,Ni^2+,Zr^4+,Cu^2+,Zn^2+,Pb^2+和 相似文献
106.
1 INTRODUCTIONTransientliquidphase (TLP)bondingtechniquehasbeensuccessfullyusedinjoiningheatresistantal loys ,likeHastelloyX ,Inconel713C ,In10 0 ,Udimet5 0 0 ,70 0 ,MarM 2 0 0 ,0 0 7,2 4 7,30 2 ,Rene′80 ,TD NiCr ,MA75 4,6 0 0 0 ,PWA14 2 2 ,CSMX 2etc ,whicharesusceptibletohotcrackingor post weldheat treatmentcrackingproblemsduringfusionweld ing[14 ] .Inaddition ,therewerereportsofjoiningNiAlandTiAlintermetallicsbyTLPbondingmethod[510 ] .Forexample ,Galehadinvestigatedthemic… 相似文献
107.
108.
F. Sommer 《Journal of Alloys and Compounds》1995,220(1-2):174-178
Trends in the dependences on temperature and concentration of experimentally determined heat capacities of liquid and undercooled liquid metals and alloys are discussed. A new adiabatic calorimeter for determining the heat capacity of liquid alloys up to 1500 K is described. The ability of several approximations and models to describe the different characteristics of the heat capacity of liquid and supercooled liquid metals and alloys is demonstrated. 相似文献
109.
T. Nguyen I. Zarudi L.C. Zhang 《International Journal of Machine Tools and Manufacture》2007,47(1):97-106
This paper studies an innovative development of a steel grinding–hardening technology using an inert cryogen—liquid nitrogen. It was found that phase transformations took place during grinding with the application of liquid nitrogen and resulted in hardened surface layer in a ground component. The layer had a fine laths martensite structure which gave rise to a remarkably high hardness. It was also shown that the treatment can produce superior surface integrity, with compressive surface residual stresses and without surface oxidation. Due to the inert nature of the liquid nitrogen, the grinding process becomes environmentally conscious. 相似文献
110.
液锻连挤硅线石粒子/铝复合材料的摩擦磨损行为 总被引:2,自引:0,他引:2
采用液锻连挤成形工艺获得了一种新型硅线石颗粒增强LY12铝基复合材料,其性能可与常规热挤压件媲美.摩擦磨损性能测试表明:硅线石颗粒增强铝基复合材料具有优良的摩擦磨损性能,且其耐磨性能随粒子体积分数增加而增加.材料经液锻连挤后,硅线石粒子在强大三向压应力作用下嵌镶于基体内,粒子很难拉脱,承受摩擦力的作用时,硅线石粒子起支承作用,粒子硬度高,故使复合材料整体耐磨性能提高. 相似文献