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The present status of Cs-corrected TEM/STEM is described from the viewpoint of the observation of nanomaterials. Characteristic features in TEM and STEM are explained using the experimental data obtained by our group and other research groups. Cs correction up to the 3rd-order aberration of an objective lens has already been established and research interest is focused on correcting the 5th-order spherical aberration and the chromatic aberration in combination with the development of a monochromator below an electron gun for smaller point-to-point resolution in optics. Another fundamental area of interest is the limitation of TEM and STEM resolution from the viewpoint of the scattering of electrons in crystals. The minimum size of the exit-wave function below samples undergoing TEM imaging is determined from the calculation of scattering around related atomic columns in the crystals. STEM does not have this limitation because the resolution is, in principle, determined by the probe size. One of the future prospects of Cs-corrected TEM/STEM is the possibility of extending the space around the sample holder by correcting the chromatic and spherical aberrations. This wider space will contribute to the ease of performing in situ experiments and various combinations of TEM and other analysis methods. High-resolution, in situ dynamic and 3D observations/analysis are the most important keywords in the next decade of high-resolution electron microscopy. 相似文献
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Syed S. Amin Shu-you Li Xiaoxia Wu Weiqiang Ding Terry T. Xu 《Nanoscale research letters》2010,5(2):338-343
High-yield synthesis of TiO2 one-dimensional (1D) nanostructures was realized by a simple annealing of Ni-coated Ti grids in an argon atmosphere at 950 °C
and 760 torr. The as-synthesized 1D nanostructures were single crystalline rutile TiO2 with the preferred growth direction close to [210]. The growth of these nanostructures was enhanced by using catalytic materials,
higher reaction temperature, and longer reaction time. Nanoscale tensile testing performed on individual 1D nanostructures
showed that the nanostructures appeared to fracture in a brittle manner. The measured Young’s modulus and fracture strength
are ~56.3 and 1.4 GPa, respectively. 相似文献
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Muhammad Hanafiah Nurmawati Parayil Kumaran Ajikumar Ravindranath Renu Suresh Valiyaveettil 《Advanced functional materials》2008,18(20):3213-3218
Fabrication of two and three‐dimensional nanostructures requires the development of new methodologies for the assembly of molecular/macromolecular objects on substrates in predetermined arrangements. Templated self‐assembly approach is a powerful strategy for the creation of materials from assembly of molecular components or nanoparticles. The present study describes the development of a facile, template directed self‐assembly of (metal/organic) nanomaterials into periodic micro‐ and nanostructures. The positioning and the organization of nanomaterials into spatially well‐defined arrays were achieved using an amphiphilic conjugated polymer‐aided, self‐organization process. Arrays of honeycomb patterns formed from conjugated C12PPPOH film with homogenous distribution of metal/organic nanomaterials. Our approach offers a straightforward and inexpensive method of preparation for hybrid thin films without environmentally controlled chambers or sophisticated instruments as compared to multistep micro‐fabrication techniques. 相似文献
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对贵金属纳米材料的种类、用途、产业化方法和发展趋势等内容进行了综合评述。贵金属纳米材料包括贵金属单质和化合物纳米粉体材料、贵金属新型大分子纳米材料和贵金属膜材料等几大类,随着国家对黄金和白银专控政策的放开和纳米技术与传统的贵金属深加工产业的结合,贵金属纳米材料作为一类在工业生产中起着重要作用的新材料,具有良好的发展前景。非负载型贵金属纳米粉末常用化学还原法、光化学合成法、电化学沉积法以及热物理法等方法进行生产,负载型贵金属纳米粉体材料则一般采取化学法(浸渍法)、离子交换法和吸附法等)生产,这两类贵金属粉体材料是目前获得工业应用最多的贵金属纳米材料,贵金属纳米材料的产业化过程有其特殊性,其发展趋势可以概括为改造、隆本、集约化和多功能化。 相似文献
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《Ceramics International》2015,41(8):9615-9621
Dairy effluent (DE) is environmentally toxic and needs special attention. Photocatalytic degradation of DE was studied using novel polyurethane (PU)-based membranes. Typically, silver–titanium dioxide nanofibers (AgTiO2 NFs) and silver–titanium dioxide nanoparticles (AgTiO2 NPs) were individually incorporated in PU electrospun nanofibers to overcome the mandatory sophisticated separation of the nanocatalysts, which can create a secondary pollution, after the treatment process. These nanomembranes were characterized in SEM, TEM, XRD and UV studies. The polymeric electrospun nanofibers were smooth and continuous, with an average diameter of about 550 nm, and held their nanofibrous morphology even after more than 2 h of photocatalytic degradation of DE, due to the good stability of PU in the aqueous solutions, which indicates good imprisoning of the functional photocatalysts. The PU–AgTiO2 NPs and PU–AgTiO2 NFs were effective materials for degradation of DE, even after two successive cycles. PU–AgTiO2 NPs and PU–AgTiO2 NFs showed a maximum degradation of 75% and 95%, respectively after 2 h. The significant enhancement of degradation in the PU–Ag–TiO2 NPs and PU–Ag–TiO2 NFs is attributed to the photoactivity of Ag–TiO2 material under visible light irradiation. 相似文献