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Silicon carbide (SiC) foam material has been applied as monolithic tray for distillation column in our previous study. A systematic understanding of the gas distribution process on the foam tray should help to the design of commercial application. In this article, local gas holdup distribution and bubble size distribution are used to measure the gas distribution. The local gas holdup is tested by the conductive probe and the number of test point is counted in different local gas holdup. The bubbles are captured by the high‐speed camera to measure the bubble size. Bubble size is calculated as ellipsoidal bubble and counted with different pore sizes. Furthermore, a three‐stage process model is put forward to explain the uneven distribution of gas phase, and verified by the experimental values. The results show that the structure and the thickness of SiC foam is the decisive factor for the gas distribution performance. © 2015 American Institute of Chemical Engineers AIChE J, 61: 4509–4516, 2015 相似文献
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In this study, we investigated the influence of the number of ethanol (EO) groups of cationic surfactants having one oleyl group on the drag-reducing effect (DR effect). Also the effect of mechanical pumping power on DR effect was experimentally investigated using two experimental setups, a circulation system (with pump) and a pressurized once-through system (without pump). The concluding remarks obtained in this study are: 1. The DR effect strongly depends on the re-formation rate of micelles disrupted mechanically. 2. When increasing the number of EO groups of the DR surfactants from 0 to 2, the available temperature range of large DR effect was shifted lower. But the DR surfactant having three EO groups (EO-3) barely exhibited the DR effect even at the low temperature. This is because the big hydrophilic head of EO groups probably delays the re-formation of micelles disrupted by pumping power. 3. The DR effect was more liable to be influenced by pumping power with a decrease in temperature. This is because it takes a long time to re-form micelles disrupted by pumping power at low temperature. 相似文献
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Erik von Harbou Markus Schmitt Christoph Großmann Hans Hasse 《American Institute of Chemical Engineers》2013,59(5):1533-1543
A simulation study of heterogeneously catalyzed reactive distillation experiments carried out with the D + R tray, a novel type of laboratory equipment, is presented. One advantage of the D + R tray is that reaction and distillation are alternating stage‐wise, in a well‐defined way that can be modeled straightforwardly. An equilibrium stage model is used to describe the distillation and a plug flow reactor model to describe the catalyst bed reactors. The model parameters are derived from a systematic experimental characterization of the D + R tray both as a reactor and as a distillation unit. A validated physicochemical fluid property model is used. The primary experimental data are reconciled. Results from the predictive simulations are in good agreement with the experimental results. The influence of errors in the input parameters on the simulation results is investigated by means of a sensitivity and error analysis. © 2012 American Institute of Chemical Engineers AIChE J, 59: 1533–1543, 2013 相似文献
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针对催化分馏塔的工艺特点,在不改变塔体的基础上,提出了ADV高效塔盘和SP规整填料的综合成组技术,并应用该技术时塔内件进行改造,实现了催化主分馏塔的扩能及综合性能的完善。与改造前相比,改造后的催化主分馏塔处理能力增大,操作弹性提高,压降减小,分离效率提高,能耗降低;消除了操作过程中的瓶颈,保证了汽油降烯烃的要求。 相似文献
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蒸馏过程进料位置优化 总被引:2,自引:1,他引:2
文章介绍了进料位置对蒸馏塔分离能力和能耗的影响,指出进料位置优化是强化分离和节省能耗的一个有效途径。并介绍了逆向蒸馏、夹点蒸馏等重要概念。对进料位置优化分别叙述了早期手算的方法和基于计算机模拟的分离因子图法、灵敏度分析法和优化器法。 相似文献