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91.
高密度钨合金热静液挤压流动粘度的数值计算 总被引:1,自引:0,他引:1
采用粘性流体的运动微分方程分析工作介质在锥模中的挤压流动,通过分析工作介质的粘度对热静液挤压的影响,指出了合理的选择工作介质的成分使得粘度适宜,可以使热静液挤压力最小,而且能够避免挤压件缺陷的产生。挤压介质的粘度是关系到坯料变形流动的润滑性能及挤压变形流动性能的关键。在此基础上,给出了挤压介质的粘度的数学关系式,为热静液挤压工艺奠定重要的理论基础。 相似文献
92.
紫外光快速固化的树枝状丙烯酸酯齐聚物的制备和性能 总被引:2,自引:0,他引:2
通过乙二胺(EDA)和三羟甲基丙烷三丙烯酸酯(TMPTA),以甲醇为催化剂,在30℃进行6小时Michael加成反应,可制得含多个双键的树枝状丙烯酸酯齐聚物(DAO).与相似分子量的线性丙烯酸酯齐聚物相比,DAO粘度低,用作紫外光固化树脂,其固化速度快,且固化产物硬度好,耐溶剂性好. 相似文献
93.
94.
探讨了影响连续固相增粘产品活性的因素,提出了控制主反应器的温度、氮气流量、基础切片的端羧基、氮气露点等主要因素,实现生产的平稳控制,从而保证产品黏度的稳定。 相似文献
95.
Viscosity data over a temperature range of 37-115°C and a pressure range of 0-10 MPa gauge are presented for a Cold Lake bitumen sample. These data show that the compression of Cold Lake bitumen results in a significant increase in its viscosity. Results are compared with those from a similar study on an Athabasca bitumen sample. Also presented are two correlations for the effects of pressure and temperature on the viscosity of Cold Lake bitumen. 相似文献
96.
4‐(4‐dimethylaminophenyl)‐1,2,4‐triazolidine‐3,5‐dione ( DAPTD ) was prepared from 4‐dimethylaminobenzoic acid in five steps. The compound DAPTD was reacted with excess acetyl chloride in N,N‐dimethylacetamide (DMAc) solution and gave 1,2‐bisacetyl‐4‐[4‐(dimethylaminophenyl)]‐1,2,4‐triazolidine‐3,5‐dione as a model compound. Solution polycondensation reactions of monomer with succinyl chloride (SucC), suberoyl chloride (SubC), and sebacoyl chloride (SebC) were performed under conventional solution polymerization techniques in the presence of triethylamine and pyridine as a catalyst in N‐methylpyrrolidone (NMP) and led to the formation of novel aliphatic polyamides. These novel polyamides have inherent viscosities in the range of 0.09–0.21 dL/g in N,N‐dimethylformamide (DMF) at 25°C. Fluorimetric studies of the model compound as well as polymers were performed. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 947–954, 2007 相似文献
97.
98.
Portland cement pastes modified by 20% weight (polymer/cement ratio) of poly(ethylene-co-vinyl acetate) (EVA) were prepared, cured, and immersed in water for 11 days. The effects of water saturation and drying on the EVA polymeric film formed in cement pastes were observed using environmental scanning electron microscopy (ESEM). This technique allowed the imaging of the EVA film even in saturated samples. The decrease of the relative humidity inside the ESEM chamber did not cause any visual modification of the polymeric film during its drying. 相似文献
99.
Calcium silicate hydrate is a porous hydrate that is sensitive to temperature and readily loses strength at elevated temperatures. Mechanical and chemical changes in the microstructure, due to escaping water, can significantly affect the mechanical properties, but these changes occur over different temperature ranges. By measuring Young's modulus as a function of temperature using the dynamic mechanical analyzer, the temperature range in which the greatest change in stiffness occurs can be identified. Additional mineralogy, pore size distribution, and composition analysis from high temperature X-ray diffraction, nitrogen sorption, and thermogravimetric analysis will demonstrate the changes in the microstructure. The results demonstrate that over 90% of the loss in stiffness occurs below 120 °C. Therefore, the damage is due to microcracking caused by pore water expansion and evaporation and not the change in mineralogy or composition. More damage, as indicated by greater loss in stiffness, occurs in stiffer and less permeable samples where higher stresses can develop. 相似文献
100.
A comprehensive experimental investigation was performed to understand the pullout behavior of polypropylene fibers from a cementitious matrix. The effect of embedded length on the pullout characteristics, the development of the interfacial bond with age of curing of matrix and the effect of exposure to degrading environments, like seawater and salt water, on the interfacial bond between the fibers and cementitious matrix were studied. The aim of these experiments was to understand the properties of fiber/matrix interface, which are of primary significance in predicting the overall behavior of fiber-reinforced cement-based composites. Polypropylene fibers have a weak bond with cementitious matrix because of smooth surface of fibers, which does not allow for sufficient friction to develop between the two. In this study a new method to improve the frictional bond by means of mechanical indentations of fibers was also proposed. The bonding performance was characterized by means of pullout tests of the plain and modified fibers from a cementitious matrix. An optimum level of fiber modification for maximization of bond efficiency was determined experimentally. 相似文献