胍基聚合物的合成及抗菌性能

采用熔融缩聚的方法合成了聚亚己基胍盐酸盐（PHGC）及聚亚己基双胍盐酸盐（PHBG）。应用气相渗透压法（VPO）及粘度法测定了其分子质量，应用元素分析，FT－IR，XPS分析了聚合物的化学组成，抗菌活性的研究结果表明所合成的胍基聚合物具有较强的而且广谱的抗菌性能。     

ˮ�ཬ������������Ƽ�����Ľ�������о�

解决注水泥作业的防气窜问题，是提高固井质量，保护油气层的关键技术。现有预测和防止水泥浆气管理的方法虽然较多，但应用于现场却有一定困难，主要表现在所考虑的因素比较单一，有些高温、高压下的水泥浆性能参数难以测定。文章在分析国内外预测和防止气窜方法的基础上，应用水泥浆浆体在环空的组成，GFP系数、水泥浆稠度阻力系数（A）及多凝水泥和环空加压等措施，拟定出一套提高水泥浆顶替效率，保证水泥浆动态和静态过程压力平衡关系的具体设计方法。     

Drying of Probiotics: Optimization of Formulation and Process to Enhance Storage Survival

This work describes how probiotic bacteria can be dried at low temperature in two steps, combining spray drying and vacuum drying, in order to enhance their survival during storage. A sufficient number of dried probiotics survived storage for more than 3 months at 30°C, if an appropriate combination of protein and carbohydrate was selected as carrier and storage conditions were maintained optimal. The use of soy protein and maltodextrin or skim milk and arabic gum resulted in the best survival rates of probiotics during storage. No evident difference was found between different spray dryer configurations, although a cocurrent flow was preferred.     

V. Yeast sequencing reports. Identification of a gene encoding a new Ypt/Rab-like monomeric G-protein in Saccharomyces cerevisiae

A Saccharomyces cerevisiae sequence cloned by serendipity was found to encode a protein that is a new member of the Ypt/Rab monomeric G-protein family. This sequence shows high homology to the yeast genes SEC4 and YPT1 and, like SEC4 and YPT1, is essential for viability. The sequence was localized to chromosome V based upon hybridization to pulse-field gel-separated yeast chromosomes. The sequence has been deposited in the GenBank data library under Accession Number L17070.     

Properties of Edible Films from Total Milk Protein

The mechanical properties and water vapor permeability of edible films made from various total milk proteins (TMPs) were investigated. Two TMPs obtained from nonfat dry milk (NDM) by removing lactose and three TMPs obtained from a commercial source were studied. Lactose was extracted from NDM by ultrafiltration or suspension in ethanol followed by filtration. TMP concentrate obtained by ultrafiltration (UF) produced films with the lowest water vapor permeability (WVP) and the highest tensile strength at break. Commercial TMP concentrates produced films more ductile than those from the UF-TMP or retentate from ethanol extraction. Further research is needed to improve mechanical properties of UF-TMP films without increasing the WVP.     

The effect of cooking on proteins from acha (Digitaria exilis) and durum wheat

The effect of cooking on proteins from acha and durum wheat was assessed from an analysis of protein extractability, gel electrophoretic profiles, in-vitro protein digestibility (IVPD) and the amino acid compositions of wholemeal flour and residue proteins. Heating wholemeal flour samples at 100–140°C (t = 10–40 min) resulted in 0–30% and 45–55% decreases in acha and durum protein solubility, respectively. In general, high molecular weight (30–70 k Da) protein subunits were more susceptible to heat damage. For both cereals, sodium dodecyl sulphate (SDS; 10 g litre^?1) and/or dithiothrcitol (DTT; 10 mM ) increased protein solubility in unheated and heated samples. The IVPD index was 90–91% and was not significantly altered by cooking (100–120°C, t = 40 min). Cooking at extreme temperatures (140°C, t = 40 min) reduced the IVPD by 8% (P = 0.05). Osborne fractionation resulted in a durum or acha residue level of 7.8% or 55.2%. Treatment with solvent containing propanol, SDS and/or DTT at room temperature followed by SDS-polyacrylamide gel electrophoresis of non-solubilised proteins showed that the glutelin fraction of acha, with the exception of a 65 kDa subunit, was insoluble owing to strong inter-subunit hydrophobic and disulphide interactions. Wholemeal acha flour and residue protein showed a significantly greater level of hydrophobic and sulphur amino acids as well as glutamine which is associated with H-bonding. The possibility that cereal protein solubility is also dependent on protein-carbohydrate links is discussed.     

康山金矿地质地球化学特征及其成因

康山金矿产在豫西熊耳山古隆起区的结晶基底太华群和盖层中元古界熊耳群地层接触界面附近，矿体严格受构造破碎蚀变带控制。流体包裹体，稳定同位素等研究表明，成矿物质来自太华群变质岩，成矿流体的性质与变质热液截然不同，而与花岗岩浆热液相近似。该矿床的形成与燕山期发生的同构造－花岗岩浆期热液活动有关，金沉淀成矿阶段有大气水的混入。     

合成彩色立方氧化锆的宝石学特征

市场上出现的紫色、浅紫色、浅黄色、粉红色、酒黄色、黄褐色、红色人造立方氧化锆均为亚金刚光泽, 火彩明显; 密度为5.99～6.34 g/cm3, 相对硬度为8～9; 除粉红色者表现出非均质性和弱多色性且内含大量定向排列的白色脱溶物外, 其余的为均质性, 内部洁净; 不同颜色的立方氧化锆的吸收光谱、紫外荧光以及滤色镜下的变色情况均存在差异; 浅紫色立方氧化锆的吸收光谱特征表明它是Nd致色. 能谱分析结果表明: 彩色立方氧化锆的常见元素有Zr, Y, P, Hf, Ca等; Er, Ce, Fe分别是粉红色、红色、酒黄色立方氧化锆的致色元素; 当Y2O3的摩尔分数大于或近于7%时, 立方氧化锆为立方面心结构且内部洁净; 当Y2O3的摩尔分数小于5%时, 立方氧化锆表现为非均质性且内含大量定向分布的白色脱溶物. 用拉尔森改写的格拉斯顿-代尔公式计算其近似折射率为2.12～2.19.     

一种新型针刺延期药的研制及其应用

本文介绍了一种新型的针刺延期药的配方设计和制备工艺，这种低猛度高热量的针刺延期药具有较高的发火感度，可满足一定的延期时间和相容性要求。文中还介绍了它在几种小型针刺延期雷管中的应用。