全文获取类型
收费全文 | 11243篇 |
免费 | 1315篇 |
国内免费 | 577篇 |
专业分类
电工技术 | 993篇 |
综合类 | 750篇 |
化学工业 | 2893篇 |
金属工艺 | 216篇 |
机械仪表 | 302篇 |
建筑科学 | 572篇 |
矿业工程 | 300篇 |
能源动力 | 619篇 |
轻工业 | 820篇 |
水利工程 | 207篇 |
石油天然气 | 323篇 |
武器工业 | 145篇 |
无线电 | 1972篇 |
一般工业技术 | 2010篇 |
冶金工业 | 147篇 |
原子能技术 | 202篇 |
自动化技术 | 664篇 |
出版年
2024年 | 44篇 |
2023年 | 189篇 |
2022年 | 325篇 |
2021年 | 477篇 |
2020年 | 410篇 |
2019年 | 418篇 |
2018年 | 393篇 |
2017年 | 478篇 |
2016年 | 465篇 |
2015年 | 458篇 |
2014年 | 728篇 |
2013年 | 1059篇 |
2012年 | 850篇 |
2011年 | 812篇 |
2010年 | 672篇 |
2009年 | 589篇 |
2008年 | 573篇 |
2007年 | 676篇 |
2006年 | 593篇 |
2005年 | 518篇 |
2004年 | 402篇 |
2003年 | 348篇 |
2002年 | 319篇 |
2001年 | 235篇 |
2000年 | 211篇 |
1999年 | 134篇 |
1998年 | 117篇 |
1997年 | 122篇 |
1996年 | 79篇 |
1995年 | 77篇 |
1994年 | 64篇 |
1993年 | 69篇 |
1992年 | 41篇 |
1991年 | 26篇 |
1990年 | 34篇 |
1989年 | 28篇 |
1988年 | 17篇 |
1987年 | 18篇 |
1986年 | 10篇 |
1985年 | 8篇 |
1984年 | 12篇 |
1983年 | 7篇 |
1982年 | 3篇 |
1981年 | 5篇 |
1980年 | 9篇 |
1978年 | 3篇 |
1974年 | 1篇 |
1965年 | 1篇 |
1958年 | 1篇 |
1951年 | 3篇 |
排序方式: 共有10000条查询结果,搜索用时 625 毫秒
101.
102.
选择有应用价值的CuO/ZrO2体系,通过大量试验寻找到了一种以ZrO2为载体的高比表面催化剂的制备方法。 相似文献
103.
A piezoelectric sprayer for dispensing semiochemicals was developed and used for a field test of bark beetle semiochemicals. The sprayer consists of a geared pump that pushes a syringe slowly to dispense semiochemicals in solvents through a microtube to a glass micropipet fixed to a piezoelectric high-frequency vibrator. The frequency is adjusted via a function generator to about 120 kHz until the harmonic properties of the glass micropipet, drawn by an electrophysiological pipet puller, cause vibrations that atomize the solvent from the micropipet tip. The sprayer, syringe, pump, function generator, and power supply were hung on one arm of a rotating trap pair (traps 6 m apart) that was slowly rotated at 2 revolutions per hour (rph) to even out the position effects on trap catches. The aggregation pheromone components of Pityogenes bidentatus, grandisol and cis-verbenol, were released by standard tube dispensers in one trap and compared to the release of similar amounts by the sprayer in the other trap. No significant differences in catch were observed. No effect of the solvent hexane on aggregation could be observed. The trap pair also caught approximately equal numbers of bark beetles when the baits were identical. The release of (+)and (–)--pinene, (+)-3-carene, and terpinolene, monoterpenes of host Scotch pine, Pinus sylvestris, at increasing rates from 0.01 to 10 log-equivalents in decadic steps (each at 0.1–100 g/min) resulted in decreasing responses to aggregation pheromone (only 9% at highest rate). Inhibition by the individual monoterpenes tested at the 100 g/min rate was significant for (+)and (–)--pinene and terpinolene (12, 13, and 15% of control, respectively). The inhibition by the host Scotch pine monoterpenes may allow P. bidentatus to avoid resistant trees that release large amounts of toxic monoterpenes in their resin and instead colonize dying and diseased limbs or slash, the usual host substrate. The piezoelectric sprayer should prove generally useful to dispense precise amounts of semiochemicals in field and laboratory experiments. 相似文献
104.
105.
Apparatus and procedure for measuring release rates from formulations of lepidopteran semiochemicals
John H. Cross James H. Tumlinson Robert E. Heath Donald E. Burnett 《Journal of chemical ecology》1980,6(4):759-770
An apparatus was developed wherein a vacuum source was used to pull air across a controlled-release-formulation dispenser or a planchet containing a known quantity of a semiochemical and into a collector filled with a polymeric adsorbent. After a set time, the semiochemical was eluted with solvent and was quantified by gas-liquid chromatography (GLC). High percentages of known quantities of the lepidopteran semiochemicals (Z)-7-dodecen-l -ol acetate (Z7DDA), boiling point (bp) 275 ° C/1 atm, (Z)-9-tetradecen-1-ol formate (Z9TDF), bp 289 °C/1 atm, and (Z,Z)-3,13-octadecadien-1-ol acetate (ZZODDA), bp 490 °C/1 atm, were recovered. The semiochemicals did not oxidize and were recovered quantitatively from the adsorbent. The release rates of Z9TDF from a controlled-release dispenser were found to be directly proportional to the airflow rates. Release rate measurements on the Z9TDF dispensers were made for the purpose of estimating the method's precision. The method was shown to give internally consistent results by measurements on another Z9TDF formulation. The accuracy of the method is discussed.Mention of a commercial or proprietary product in this paper does not constitute an endorsement by the USDA. 相似文献
106.
介绍了目前广泛使用的耐久压烫整理剂的DMDHEU在低醛化方面的研究进展这影响甲醛释放的因素。 相似文献
107.
Ralph Schreiber Britta ReinkeCarsten Vogt Joachim WertherGerd Brunner 《Powder Technology》2003,138(1):31-38
Various particles with sizes between 100 and 200 μm were encapsulated with waxes commonly used in technical coating applications. For this, a homogeneous mixture of molten paraffin and supercritical carbon dioxide was prepared in an autoclave and injected into the high-pressure fluidized bed through a nozzle from the bottom. Due to the different conditions in the mixing autoclave and the fluidized bed, the paraffin precipitated in the vicinity of the nozzle and adhered to the solid particles. A complete, thin, uniform, and solvent-free coating was produced. The use of two paraffins with different alkane compositions resulted in dissimilar spreads on glass beads due to their different glass transition temperatures. A smaller pressure drop across the nozzle led to more uniform and even coatings. Glass beads, ceramic spheres, potassium chloride, and lactose showed similar coating results, whereas different morphologies were observed with a plastic material, characterized by a rougher surface and a lower surface energy. The high quality of the coating was confirmed by standard dissolution tests with coated potassium chloride crystals and lactose agglomerates. 相似文献
108.
复杂环境下的多普勒频移变化及信号功率衰减均会对载波准确跟踪造成影响. 在研究北斗卫星B1 频点信号结构的基础上, 建立以环路中相关积分值为观测量的非线性EKF 模型和UKF模型, 并提出利用滤波估计状态量进行状态反馈控制的方法, 从而解决了载波跟踪环路在高动态及弱信号环境中难以高性能工作的问题. 实验结果表明,状态反馈控制的EKF 模型和UKF滤波模型能准确地跟踪弱信号及高动态下的信号变化, 从而有效控制跟踪误差, 为实现快速准确的载波跟踪奠定了基础.
相似文献109.
主要研究了酸活化剂、填充剂、pH载体等因素对固载二氧化氯释放特性的影响,得到了不同情况下的释放峰值和峰值时间及几种常见菌种达到杀菌率100%所需固载二氧化氯释放剂量。 相似文献
110.
A laboratory scale spray dryer was used to encapsulate vildagliptin (VLG), an antihyperglycemic drug, into different polymers such as poly(dl-lactide) (PDLA), poly(dl-lactide-glycolide)-50:50 (PLGA 50:50), and poly(dl-lactide-glycolide)-75:25 (PLGA 75:25). Response surface methodology (RSM) was employed to evaluate the effects of process and formulation factors on the encapsulation efficiency (EE). The physicochemical properties of the drug-loaded micro-/nanoparticles, mainly the drug loading (DL), particle size distribution, surface morphology, drug–polymer compatibility, and release rate were investigated. % EE of drug-loaded micro-/nanoparticles were in the range of 57.10% to 76.44%. PLGA50:50 micro-/nanoparticles showed highest EE as compared to PDLA and PLGA75:25 micro-/nanoparticles. The mean particle size of the micro-/nanoparticles containing PLGA 50:50, PLGA 75:25, and PDLA polymers were 428?nm, 640?nm, and 1.22 µm, respectively. Surface morphology study revealed smooth, spherical and nonporous surface structures of the micro-/nanoparticles. Fourier transform infrared spectroscopy studies confirmed the drug–polymer compatibility. Powder X-ray diffraction analysis of micro-/nanoparticles revealed that VLG was present in the amorphous form within the micro-/nanoparticles formulations. In vitro release study demonstrated that VLG is slowly released from micro-/nanoparticles for 12?h and the drug release rate was influenced by type and viscosity of polymers used. This work suggests that PDLA, PLGA 50:50, and PLGA75:25 polymers are able to sustain the VLG release rates from micro-/nanoparticles. 相似文献