Influence of heat treatment on fracture and magnetic properties of radially oriented Sm2Co17 permanent magnets

The quenching, fracture and aging treatment of radially oriented Sm2Co17 ring magnets were investigated. The results indicate that the ring magnets have obvious anisotropy of thermal expansion, which easily leads to the splits of the magnets during quenching. The fracture is brittle cleavage fracture. The difference （Aa） of the expansion coefficient reaches the maximum value at 800-850 ℃. So, various quenching processes at different steps are adopted in order to reduce the splits. When the magnets are aged, 1：5 phase precipitates from the 2：17 matrix phase and forms a cellular microstructure with 2：17 phase. BHmax and JHc reach the maximum value 226 kJ/m^3 and 2 170 kA/m after being aged at 850 ℃ for 4 h and 8 h, respectively. The aging treatment at 850 ℃ has little influence on remanence（Br）, which can always keep a high value （≥1.0 T）. Through appropriate heat treatment, the ring magnets have uniform cellular microstructure and excellent magnetic properties： Br ≥ 1.0T, JHc ≥2 100 kA/m, BHmax ≥ 220 kJ/m^3.     

预焙铝电解槽阳极钢爪自焙保护环优化技术

就目前预焙铝电解槽所用的自焙保护环的制作进行了研究．提出了优化方案，通过工业试验认为．自焙保护环的制作技术优化后．可以给企业创造显著的经济效益。     

柴油机活塞环耐磨性探讨

通过分析活塞环的基体组织、径向弹力与气缸套的匹配以及对其施行表面处理，以提高活塞环的耐磨性。对活塞环进行调质或渗氮处理，可显著提高其使用寿命。     

GCr15钢轴承套圈的磨削开裂失效分析

通过金相分析及断口观察，对GCr15钢轴承套圈的磨削开裂进行了系统分析。结果表明．淬火裂纹是套圈失效的根本原因，而原材料中Cr的带状偏析、套圈表面的应力集中、淬火加热时的氧化脱碳以及不当的磨削工序则共同加剧了淬火裂纹的萌生和扩展。     

聚醚多元醇中环状齐聚物的去除(续)

(接上期第 2 3页 )3　膜分离Doraietal[16] 通过超滤除去低相对分子质量级份 ,使聚醚多元醇 ,尤其是聚四氢呋喃多元醇 ,具有较窄的分布 (Mw∶Mn=1 .2～ 1 .8)。该方法通过对多分散的熔融聚合物实施物理分级 ,达到降低相对分子质量分布的目的 ,可使最终产物的相对分子质量为 40 0～ 40 0 0 ,分散度为 1 .2～ 1 .8。该方法首先需要准备 1套交叉流动的膜分离系统 ,采用渗透膜或半渗透膜 ,膜的一边是滞留物 ,另一边是超滤液。然后 ,在起始聚合物的熔点以上 ,分解温度以下 ,且温度不大于膜的熔融和分解温度 ,将起始聚合物熔融 ,并流入该系统中…     

Turbulent flow field comparison and related suitability for fish passage of a standard and a simplified low‐gradient vertical slot fishway

Fishways are hydraulic structures that allow passage of fish across obstructions in rivers. Vertical slot fishways—VSFs—are considered the most efficient and least selective type of technical fishway solutions, especially due to their ability to remain effective even when significant upstream and/or downstream water level fluctuations occur. The scope of the present study is to perform numerical simulations in order to investigate and compare the hydraulic turbulent flow field in a standard and a simplified version of the most common VSF design. Implications in relation to fish swimming behaviour and fish passage performance are discussed. Different water depths (as well as discharges) were investigated, using a bed slope of 5%, as a reference for low‐gradient VSFs with a very limited selectivity that can be used in multispecies rivers in grayling‐barbel regions. Results show that maximum values of velocity, turbulent kinetic energy, and Reynolds stresses are higher in the standard design. However, corresponding to slot geometry and orientation, the direction of the main jet in the simplified design is more inclined towards the left side of the pool. This causes the eddy to split into 2 smaller ones; the minimum eddy dimension is reduced from 0.4–0.5 to 0.2–0.3 m. These dimensions are detrimental for fish passage efficiency, being more comparable with fish length (0.15–0.40 m), thus affecting migrating fish stability and orientation. Furthermore, the standard design provides a more straightforward upstream path and wider areas of low flow velocities and turbulence, useful for fish resting. Therefore, it is recommended that the standard design should be preferred over its simplified version, even if its construction costs are around 10–15% higher than the simplified one.     

Studies on film potentiometric stripping analysis: effects of electrochemical parameters

Film potentiometric stripping analysis (PSA) is a novel method for concentrating the test ion directly on a glassy carbon electrode with subsequent stripping by a chemical oxidant, the redissolution step being followed by a chronopotentiometric sequence. The electrochemical parameters governing both preconcentration and redissolution steps are studied on a rotating disk electrode: experimental results are compared with the theoretical developments recently published. Except for the influence of rde rotation rates on each step and on analytical parameters, experiments and theory are in agreement. Discrepancies concerning the rotation rate effects are studied by potentiostatic coulometry and voltammetry measurements in regard to the preconcentration step: the rotation rate effects are based on the physical behaviour of the rde. Routine analysis is carried out using film PSA, Pb(II) as the test ion and Fe(III) as oxidizing agent, in perchlorate medium.     

一种应用层组播可靠性技术

组播是一种高效的多点通信方式,IP组播效率高,但需专门的组播路由器,代价大,至今未能大规模部署.应用层组播数据的复制转发功能由终端主机完成,不涉及现有网络基础设施的更新,在Internet上容易实现,但终端主机的稳定性和安全性不如组播路由器,容易导致单点失效,且数据恢复困难.为解决应用层组播存在的可靠性问题,提出了一种树环结构的应用层组播方案,通过环结构来增加数据传输的可靠性,并采用主动随机转发技术来解决树环结构的多点失效问题.该方案既有效解决了应用层组播可靠传输问题,又降低了恢复时延和系统开销.     

2-乙基-2- 唑啉的阳离子开环聚合及聚合物的表征

以对甲苯磺酸甲酯为引发剂进行２乙基２唑啉阳离子开环聚合研究，主要考察了不同的单体／引发剂配比、聚合温度和聚合时间对聚合转化率和聚合物分子量的影响。聚合物通过ＩＲ、１Ｈ核磁共振、ＤＳＣ进行表征，并考察了聚（２乙基２唑啉）与部分聚合物和共聚物的共混性能。     

气化炉锥底砖、激冷环与下降筒的损毁与解决对策

针对国产化大氮肥水煤浆气化炉中锥底砖、激冷环和下降筒使用过程中出现的问题,分析了损毁原因,分别从技术改进、工艺操作和设备管理等方面提出了相应的解决对策,可以不同程度地延长锥底砖、激冷环、下降筒的寿命。