高氯酸为催化剂乙酰化法测定伯醇或仲醇

提出了以主氯酸为催化剂，分析纯乙酸乙酯为介质，乙酸化法测定伯、仲醇的实验条件，实现了对经典方法的改进，简化了操作程序。     

HPMBP与伯胺N_(1923)对希土元素(Ⅲ)的协同萃取

本文研究了HPMBP与伯胺N_(1923)的二甲苯溶液,从盐酸介质中协同萃取希土(Ⅲ)的机理。用斜率法、恒摩尔法确定了协萃配合物的组成为:RNH_3Ln(PMBP)_4。求得关于Pr(Ⅲ)协萃反应的平衡常数及协萃配合物的生成常数分别为:logK_(12)=-1.95;logβ_(12)=3.94。实验发现,协萃系数(R)随希土元素的原子序数(Z)递变而呈现“双峰效应”。还研究了协萃配合物的IR,NMR谱。     

8Li次级束的产生

在北京串列加速器次级束流线上通过2 H(7Li,8Li) 1H逆运动学反应产生了用于核天体物理研究的8Li次级束。准直后的次级束纯度达到 80 %以上 ,对于 44MeV的7Li强度约为 3 0s- 1·pnA- 1,可以用来进行逆几何转移反应的实验测量。     

用菱锌矿制取轻质氧化锌的研究

介绍了以菱锌矿为原料生产轻质氧化锌的方法，论述了反应酸浓度，煅烧温度，溶液PH值对实验的影响，并对生产工艺条件进行了研究。其工艺流程是将粉碎后的菱锌矿进行循环酸浸，净化后再直接和碳化母液反应，经沉降后再煅烧分解为轻质氧化锌，产品质量符合国家标准，视比容大，活性强，成本低，经济效益显著。     

奎宁印迹聚合物的吸附与识别特性的研究

以奎宁为模板分子 ,利用分子印迹技术合成了一种新型的类似于人工受体的印迹聚合物 ,研究了它对奎宁和其它底物的吸附特性和选择性识别能力 ,并对其固相萃取性能做了初步的研究。     

台北凹陷小草湖次凹油气成藏特点及有利区带

吐哈盆地小草湖次凹发育多套烃源岩，油源条件好，油气资源丰富，油气勘探潜力巨大，中侏罗统发育三套储盖组合，凹陷内油气藏类型主要为侏罗系三间房组，七克台组的构造－岩性复合型和侏罗系西山窑组的深盆气藏，燕山运动末期是小草湖次凹一次重要的成藏期，古构造，古构造背景和构造－岩性复合型圈闭发育是小草湖次凹成藏主控因素，根据小草湖次凹成藏主控因素评价和优选有利区带，勘探工作取得了良好效果。     

将紫外光谱用于溴指数测定方法的选择

对未知组成的样品进行紫外光谱扫描 ,根据扫描结果以及各种溴指数测定方法的适用范围 ,选择测定未知物溴指数的适宜方法 ,以提高测定准确度。     

Semiparametric Estimation in Time‐Series Regression with Long‐Range Dependence

Abstract. We consider semiparametric estimation in time‐series regression in the presence of long‐range dependence in both the errors and the stochastic regressors. A central limit theorem is established for a class of semiparametric frequency domain‐weighted least squares estimates, which includes both narrow‐band ordinary least squares and narrow‐band generalized least squares as special cases. The estimates are semiparametric in the sense that focus is on the neighbourhood of the origin, and only periodogram ordinates in a degenerating band around the origin are used. This setting differs from earlier studies on time‐series regression with long‐range dependence, where a fully parametric approach has been employed. The generalized least squares estimate is infeasible when the degree of long‐range dependence is unknown and must be estimated in an initial step. In that case, we show that a feasible estimate which has the same asymptotic properties as the infeasible estimate, exists. By Monte Carlo simulation, we evaluate the finite‐sample performance of the generalized least squares estimate and the feasible estimate.     

Original Finger Image Extraction by Morphological Technique and Finger Image Comparisons for Persons' Identification

This research uses the object extracting technique to extract the index, middle and ring fingers from the hand images. The algorithm developed in this research can find the precise locations of the different fingers' fingertips and the finger-to-finger-valleys. After finding the positions of the fingertips and finger-valleys, the index, middle and ring fingers can be extracted from the hand images by using morphological technique. The extracted index, middle and ring fingers contain many useful geometry features. One can use these features to do the person's identification. The orientations of the index, middle and ring fingers are found in this research. Image rotating, image shifting, and image interpolating techniques are used to align different persons' index, middle and ring fingers. Image subtraction is used to exam the difference of two index, middle and ring finger images. In this research so far only use the index, middle and the ring fingers as the features to identify different persons. ^★This work was supported by National Science Council under grant NSC 93-2213-E-212-011.     

马尾松木材中性脱脂工艺的研究

采用全因素试验法，对马尾松木材进行过热乙醇溶液脱脂处理，以获取马尾松木材高效脱脂工艺技术。试验结果显示：（1）脱脂温度对马尾松松脂溶出量的影响极显著，且溶出量随着脱脂温度的升高而增大；（2）脱脂时间对马尾松松脂溶出量的影响极显著，且溶出量随着脱脂时间的延长呈先增大后减小的趋势；（3）脱脂浴比对马尾松松脂溶出量的影响极显著，且溶出量随着脱脂浴比的延长呈先增大后减小的趋势；（4）利用过热乙醇溶液对马尾松木材进行脱脂，其最佳工艺是脱脂时间为130℃、脱脂时间为8h、浴比1：8。