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101.
Effect of Particle Size on Monometallic and Bimetallic (Au,Pd)/C
on the Liquid Phase Oxidation of Glycerol 总被引:2,自引:0,他引:2
Nikolaos Dimitratos Jose Antonio Lopez-Sanchez David Lennon Francesca Porta Laura Prati Alberto Villa 《Catalysis Letters》2006,108(3-4):147-153
The influence of metal particle size of monometallic and bimetallic supported catalysts (Au, Pd, Au–Pd)/C was studied using
as a model reaction the liquid phase oxidation of glycerol. By tuning the metal particle size from 2 to 16 nm a progressive
decrease of activity and simultaneously an increase in the selectivity to sodium glycerate was observed. Moreover, the influence
of the temperature was studied and it was found that by increasing the temperature, only with a large particle size the formed
glycerate was retained and not over-oxidized to tartronate. 相似文献
102.
103.
激光粒度分析仪测定氢氧化铝细颗粒方法的探讨 总被引:1,自引:0,他引:1
针对马尔文2000型激光粒度分析仪在氢氧化铝分析中对25μm粒径以下细颗粒的分析不太敏感,难以满足氧化铝生产分解过程对粒度控制的要求,对试验样品采用一些非常规的特殊处理方法,以提高细小颗粒在处理过样品中所占的体积百分比;研究了不同的样品处理方式对分析结果的影响。试验结果表明,只有对洗涤、过滤后的湿样进行分析,才能对分解料浆样品中的细颗粒的粒度分布进行准确地分析,得到满足试验和生产过程控制精度的结果。 相似文献
104.
The paper presents a computational approach and numerical data which facilitate the use of the smeared-tip method for cohesive fracture in large enough structures. In the recently developed K-version of the smeared tip method, the large-size asymptotic profile of the stress intensity factor density along a cohesive crack is considered as a material characteristic, which is uniquely related to the softening stress-displacement law of the cohesive crack. After reviewing the K-version, an accurate and efficient numerical algorithm for the computation of this asymptotic profile is presented. The algorithm is based on solving a singular Abel's integral equation. The profiles corresponding to various typical softening stress-displacement laws of the cohesive crack model are computed, tabulated and plotted. The profiles for a certain range of other typical softening laws can be approximately obtained by interpolation from the tables. Knowing the profile, one can obtain with the smeared-tip method an analytical expression for the large-size solution to fracture problems, including the first two asymptotic terms of the size effect law. Consequently, numerical solutions of the integral equations of the cohesive crack model as well as finite element simulations of the cohesive crack are made superfluous. However, when the fracture process zone is attached to a notch or to the body surface and the cohesive zone ends with a stress jump, the solution is expected to be accurate only for large-enough structures. 相似文献
105.
106.
本文描述了醋酸纤维素-纤维素大孔增强超滤膜的结构特征一分离性能之间的关系。详细论述了膜材料含量和粘连剂含量及其分子量对膜结构和性能的影响。论述了不同配方铸膜液的膜,其孔径,水通量和截留率随操作压力的变化规律。实验证明这种高强度的CAC膜经多次重复使用后,其结构性能保持完好。 相似文献
107.
本文提出了一种广义最小均方(GLMS)算法,分析了GLMS算法的性能,并根据GLMS算法,导出一种自适应递归滤波(ARF)算法。在推导中,ARF算法避开了超稳定定理,从而考虑自适应系统的严格正实条件和Popov不等式是不必要的。计算机模拟表明ARF算法具有很高的收敛速度。 相似文献
108.
Microstructure evolution during metal forming processes 总被引:8,自引:0,他引:8
Recrystallization and grain growth evolutions during metal forming processes are considered. Coupling between the thermo-mechanical and microstructure processes is realized. Die forging of a rear-axle flange is simulated numerically on the base of the finite element method. Material parameters of the models are obtained experimentally. The influence of interpass and holding times on grain size distributions in the end product is shown. 相似文献
109.
关于正整数的k次根的整部 总被引:1,自引:0,他引:1
徐哲峰 《纺织高校基础科学学报》2003,16(3):208-209
对于给定的自然数m,令口α(m)为m的是的次根的整部。即:α(m)=[m^1/k]。研究了α(m)的渐近性质,并给出了一个有趣的渐近公式。 相似文献
110.
Multi-User MIMO Mobile CDMA Uplink System Employing Turbo Coding and Joint Detection Through a Multipath Rayleigh Fading Channel 总被引:1,自引:1,他引:0
Yasmine A. Fahmy Hebat-Allah M. Mourad Emad K. Al-Hussaini 《Wireless Personal Communications》2006,38(3):325-341
In this paper, a generalized multiple-input multiple-output (MIMO) antenna system that can be fitted to the uplink of a wireless communication system is considered for the general case of multi-user. At the transmitter, the information bits are Turbo coded, then interleaved and passed through a serial-to-parallel converter. The channel is assumed bad urban suffering from multipath Rayleigh fading resulting in inter-symbol and multiple access interferences (ISI and MAI). At the front-end of the receiver, a number of receiving antennas are used followed by a joint multi-user estimator based on the Minimum Mean Square Error Block Linear Equalizer (MMSE-BLE).Computer simulations demonstrate a significant performance improvement in both single user and multi-user cases.This paper depends in parts on that presented at the 11th European Wireless Conference, Cyprus, Nicosia, pp. 187–192, April 2005.
Yasmine A. Fahmy was born in Guiza, Egypt, on June 4, 1976. She received the B.Sc., M.Sc. and Ph.D. degrees in Communication and Electronics engineering from Cairo University, Egypt on 1999, 2001 and 2005 respectively. She is presently an assistant professor at Cairo University, Egypt. Her current field of interest is wireless communication and channel estimation.
Hebat-Allah M. Mourad received her B.Sc., M. Sc. and Ph.D. degrees in electrical communication engineering from Cairo University, Egypt, in 1983, 1987 and 1994 respectively. Since 1983, she has been with the Department of Electronics and Communications, Faculty of Engineering, Cairo University, and is currently associate professor there. Her research interests include optical fiber communications, mobile and satellite communications.
Emad K. Al-Hussaini received his B.Sc degree in Electrical Communication Engineering from Ain-Shams University, Cairo, Egypt, in 1964 and his M.Sc and Ph.D. degrees from Cairo University, Giza, Egypt, in 1974 and 1977, respectively. From 1964 to 1970, he was with the General Egyptian Aeroorganization. Since 1970, he has been with the Department of Electronics and Communications, Faculty of Engineering, Cairo University, and is currently professor there. He was a research fellow at Imperial College, London, UK, and at the Moore School of Electrical Engineering, University of Pennsylvania, Philadelphia, PA, USA, in the academic years 1976/1977 and 1981/1982, respectively. In 1990, he received the Egyptian national encouragement award for outstanding engineering research. He has written several papers for technical international journals and conferences. His research interests include signal processing, fading channel communication, modulation, and cellular mobile radio systems. Dr Al-Hussaini is a senior member of IEEE. He is listed in Marquis Whos Who in the World and in the IBC (International Biographical Center, Cambridge) for outstanding people of the 20th century. 相似文献