Cr17Ni2钢焊接接头抗刀状腐蚀性能的研究

采用二次稳定化退火处理,解决了Cr17Ni2钢异质焊接接头刀状腐蚀的问题。提高了用Cr17Ni2钢制造的焊接叶轮的使用寿命,取得了明显的经济效益。     

Ammonia synthesis: The bellwether reaction in heterogeneous catalysis

This is a personal account of the Havreholm Conference with a choice of topics dealing with catalytic ammonia synthesis. Among the general concepts that were retained are: the rate determining step with rates of adsorption and desorption of nitrogen; the direct activated dissociative adsorption of N₂; the surface crystalline anisotropy of iron; the role of promoters in industrial iron based catalysts; and the atomic structure of the metallic surface on the industrial multiply promoted catalyst. Finally, a new isotope jump technique to measure an upper limit to the real turnover frequency is discussed.     

Properties of radiation stable, low viscosity impregnating resin for cryogenic insulation system

Impregnating resins in fusion magnet technology are required to be radiation stable, low viscosity, long usable life and high toughness. To meet these objectives, we developed a new epoxy based composite which consists of triglycidyl-p-aminophenol (TGPAP) epoxy resin and isopropylidenebisphenol bis[(2-glycidyloxy-3-n-butoxy)-1-propylether] (IPBE). The ratio of TGPAP to IPBE can be varied to achieve desired viscosity and working time. The boron-free glass fiber reinforced composites were prepared by vacuum pressure impregnation. The radiation resistance was evaluated by ⁶⁰Co γ-ray irradiation of 1 MGy at ambient temperature. The mechanical properties of the composites have been measured at room temperature and at 77 K.     

三芳基甲烷树脂的磁性行为

介绍了ＢＡ／Ｐｙ，ＢＡ／Ｐｈ和ＰＨＢＡ三种具有三芳基甲烷结构Ｂ阶树脂的合成方法及分子链的单元结构形式。对用紫外光和激光照射法进行脱氢反应的实验条件及脱氢化后树脂的磁性能（磁滞现象，矫顽力和磁化强度）进行考查。     

Electrosynthesis of dimethylsulfone from dimethylsulfoxide at a dimensionally stable anode

Galvanostatic electrochemical oxidation of dimethylsulphoxide (DMSO) to dimethylsulfone (DMSO₂) has been effected at a dimensionally stable anode (DSA) under different conditions of current density and reaction media, in both a batch and a flow reactor (membrane cell with an ion-exchange membrane between the two working electrodes) functioning in batch recirculation mode. Excellent yields of the sulfone have been obtained under both conditions. The product has been characterized by various physicochemical techniques. The operational conditions giving maximum yield of the product have been established. The electrochemical oxidation of DMSO has also been studied by cyclic voltammetry at a glassy carbon (GC) electrode. The mechanism of electrochemical oxidation and the advantages of the present methods over existing ones, are discussed.     

块H-矩阵的简捷判据

Feingold与Varga引入了块对角占优的概念,基于它的优美性质,引起了许多学者的浓厚兴趣本文研究块H-矩阵(广义块对角占优矩阵)的实用判定,给出了块H-矩阵的两个新的简捷判据,并应用十矩阵正稳定性和亚正定性的判定。