碳化硅陶瓷的熔盐腐蚀

系统总结了碳化硅陶瓷的高温熔盐腐蚀行为,包括熔盐的化学性、腐蚀动力学、材料在腐蚀过程中的性能变化,并提出了今后提高碳化硅陶瓷耐熔盐腐蚀的研究方向.     

高温固相催化剂在铝灰热法处理过程中的应用研究

选取三种类型铝灰和三种高温固相催化剂作为试验原料,通过温度、时间和催化剂对高温条件下铝灰中复合盐脱除效率影响的探讨,得出高效脱除铝灰中复合盐的最佳条件。结果表明,A型催化剂更适合高铝质铝灰中复合盐的脱除;B型催化剂更适合高铝质铝灰和高镁质铝灰中复合盐的脱除;C型催化剂更适合高硅质铝灰和高镁质铝灰中复合盐的脱除。在最优条件下,煅烧后的铝灰中复合盐脱除率高、含量低,可满足大多数氧化铝材料工业使用要求,有望作为工业原料或替代原料使用。     

采卤对接井施工工艺的工程实践

以江西九二盐业403-404采卤对接井组的施工工程为案例,系统介绍了井区地质情况、钻探施工情况;总结了大口径取心工具的优点,螺杆定向钻进施工工艺及攻克技术难点。     

Extraction and on-line concentration of flavonoids in Brassica oleracea by capillary electrophoresis using large volume sample stacking

Flavonoids are bioactive compounds found in plants. Studies indicate consumption of food containing these compounds may reduce the incidences of cancer and cardiovascular diseases. In broccoli, the flavonoids are present at variable concentrations and so far have mainly been determined using high performance liquid chromatography (HPLC). This paper describes a rapid capillary electrophoresis method, involving large volume sample stacking (LVSS), suitable for the analysis of flavonoids in broccoli. Following acid hydrolysis, the two key flavonoids (kaempferol and quercetin) in a broccoli extract were concentrated on-line by LVSS prior to separation by capillary zone electrophoresis (CZE). Using an optimised method, the extract was injected for 50 s into a 50 μm (internal diameter) × 85 cm (total length) capillary followed by stacking/matrix removal at −5 kV for 83 s. The two analytes were then separated in less than 8 min by CZE using a 10 mM sodium borate buffer (pH 8.40) and a separation voltage of +30 kV at 30 °C. A linear relationship in the range 1–20 ppm was observed for the method (r² = 0.9991–0.9995) with detection limits of 0.9 and 0.6 mg/kg of broccoli for kaempferol and quercetin, respectively. This method demonstrated good repeatability for the standard and extract with relative standard deviations of less than 5% for both peak area and migration time measured over five different days (n = 5). The method was successfully applied to quantitatively determine kaempferol and quercetin contents in a commercial broccoli sample as 11.8 and 14.6 mg/kg fresh weight, respectively. This result was validated by HPLC analysis and is within the ranges reported in the literature.     

Effect of fermented rice culture on the microbiological,biochemical and sensory characteristics of low‐salt douchi,a traditional Chinese fermented soybean condiment

A low‐salt (4% NaCl, w/w) douchi supplemented with different concentration of fermented rice culture (FRC) of 0%, 5%, 10%, 15% and 20% (v/w) was produced, and the effect of FRC on microbiology, biochemistry and sensory quantity was investigated. Results indicated that FRC had a significant effect on low‐salt douchi. Compared with the control (added 0% FRC), in the other treatments, the counts of yeast and lactic acid bacteria increased by about 50%, whereas the moulds decreased by about 30%; the pH reduction was close to 4.7; total acid increased to about 1.300 g per 100 g; reducing sugar maintained a decrease to 21.07 mg per g; amino nitrogen increased to about 0.900 g per 100 g, but not above the control (1.013 g per 100 g). In general terms, total free amino acid contents and three organic acids were higher in low‐salt products than four commercial products. Sensory evaluation of products supplemented with 10% and 15% FRC revealed better overall acceptability compared with other treatments and a commercial product.     

减盐防控高血压的科学证据和实践

大量动物实验和流行病学研究表明,过量的食盐摄入是导致血压升高的主要因素之一。人群干预研究和发达国家的减盐行动表明,人群中减盐是预防高血压最具成本效益的措施。本文总结了减盐防控高血压的科学证据和国际减盐行动,指出了我国开展减盐防控高血压工作的必要性。     

从岱山惨案看民国浙江地区的盐政

1936年7月13日,岱山爆发了以盐民集体反对盐斤归堆为导火线的岱山惨案,致使百余人伤亡。这次渔、盐民集体反抗当地盐税警的冲突,其原因是多方面的,而由南京政府推行的渔盐变色和盐斤归堆的盐政改革措施中存在的弊端实为其中不可忽视的因素。此次惨案对财政部的盐政改革造成了巨大冲击,促使财政部对浙江盐政改革中的弊病做出了适当的调整。     

试论《四库全书》的编纂及其盐文献

《四库全书》采进书多来自盐区藏书家,大量的盐文化圈学者也参与了该书的编纂,它应该最能反映当时的盐文化成果。《四库全书总目》的“提要”对《四库全书》收录的盐政、盐史等盐文献的介绍。该书“阐明性学治法”的编纂宗旨,价值尺度的保守和思维方式的滞后使得其中的盐业科技、管理等文献不如想象中丰富。盐业科技、物质文化的发达并未能将整个社会文化推进到以实证为基础的现代文明的新时代。     

精制卤水中含盐泥问题初探

针对精制卤水中含有盐泥的问题,从反应时间、絮凝剂添加、转料及过滤等几方面进行深入探讨,分析了盐泥可能存在的原因,并提出了切实可行的改造方案,对生产运行进行了优化,取得了很好的效果.