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21.
Thin starch coatings were deposited onto polyethylene (PE) film surfaces when PE films were immersed in 1% jet cooked starch solutions and the hot solutions were allowed to cool. Normal cornstarch, waxy cornstarch, high amylose cornstarch, and solvent‐extracted normal cornstarch (to remove native lipid) were used in these experiments. Amounts of adsorbed starch varied from about 0.03–0.05 mg per cm2 of PE, and these starch coatings imparted hydrophilic properties to film surfaces, as evidenced by contact angle measurements. Although starch could be removed by gently rubbing water‐wet PE surfaces, air‐dried coatings were more firmly attached, and did not separate from the PE surface when films were bent or flexed. SEM images of starch‐coated film surfaces showed that starch was deposited as particles less than 1 μm in diameter, and also as aggregates of these submicron particles. Despite the fact that some starch samples contained only very small amounts of amylose and native lipid, surface‐deposited starch in all experiments contained 90–100% amylose; and exhibited the same Vh X‐ray diffraction pattern, indicative of helical inclusion complex formation. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 1781–1788, 2002; DOI 10.1002/app.10589 相似文献
22.
玉米淀粉胶粘剂的改性研究 总被引:8,自引:0,他引:8
以玉米淀粉为主要原料 ,通过预糊化、氧化、加碱糊化进行化学改性 ,并加入稳定剂可制备固含量高、贮存稳定性好 ,具有一定初粘力和透明性的改性淀粉胶粘剂。本论文主要研究了改性玉米淀粉胶粘剂的主要成分配比及工艺条件对产品性能的影响。结果表明 :淀粉氧化前是否进行预糊化处理、氧化剂的用量、体系pH值、加碱糊化时碱液用量、稳定剂的种类和用量等对改性玉米淀粉胶粘剂性能影响较大。 相似文献
23.
变性淀粉取代聚乙烯醇生产Al2O3刚玉陶瓷的胶粘剂研究 总被引:4,自引:0,他引:4
论述了变性淀粉取代聚乙烯醇(PVA)生产Al2O3刚玉陶瓷的意义及聚乙烯醇结构与吸附性能的关系,并且根据胶粘机理,通过分析Al203胶粒的表面特性和变性淀粉的结构,说明了变性淀粉可以取代聚乙烯醇。 相似文献
24.
25.
This work was undertaken to discuss in depth the vital differences in the morphological development during synthesis, and properties of starch‐g‐poly‐(vinyl acetate) copolymers using two different initiators, potassium persulfate (KPS) and ceric ammonium nitrate (CAN). KPS‐initiated system gave relatively low values of grafting ratio and grafting efficiency, indicating a great tendency for the formation of poly(vinyl acetate) homopolymer (PVAc). Yet, higher values were seen for the CAN‐initiated system. Transmission electron microscope observations indicated a relatively broad distribution of latex particles for the KPS‐initiated system. The surface potential of latex particles was about ?3.5 mV, which turned out to be insufficient to maintain stability of latex particles. On the other hand, a uniform particle size distribution was found for the CAN‐initiated system, as the surface potential of latex particles was 21.5 mV. Moreover, radicals on starch molecules were generated directly through a redox reaction with positively charged ceric ion. The hydrophobic PVAc chains were thus grafted on starch, resulting in an amphiphilic graft copolymer, which provides a sufficient stabilization degree as a role of surfactant to render a relatively uniform distribution of latex particles. The synthesized starch‐g‐poly(vinyl acetate) copolymers were further converted to starch‐g‐poly(vinyl alcohol) through saponification, which were subjected to evaluations regarding the biodegradation and cell culture capability. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 3017–3027, 2006 相似文献
26.
Anisotropy of X-ray structural parameters of the three phase model proposed by Mitra and Mukherjee (ref.2), has been investigated in the case of cellulose fibres of ramie, hemp and jute. The structural parameters have been determined separately from each of the observable equatorial reflections. It has been found that the parameter degree of crystallinity as defined in the model is in fact anisotropic at least in the samples studied. The parameter degree of paracrystallinity introduced by Mitra and Mukherjee was also found to be anisotropic. Several important correlations between the structural parameters have been drawn. It has been observed, in agreement with the recent findings of Hosemann and Balta Calleja (ref.10) that the greater the paracrystalline distortion, the smaller the ‘paracrystallite size’. 相似文献
28.
热塑性淀粉/聚己内酯共混物的制备和性能的初步研究 总被引:8,自引:2,他引:8
利用热塑性淀粉(TPS)与聚己内酯(PCL)熔融共混并挤出可用来制备完全可生物降解的塑料,研究表明,组分PCL以及增塑剂水和甘油的含量对体系的力学性能和耐水性有显著的影响。 相似文献
30.