Si(111)上生长LiNbO_3薄膜的研究

利用射频磁控溅射的方法,在Si(111)衬底上制备了LiNbO3薄膜。采用X射线衍射(XRD)和扫描电子显微镜(SEM)研究了衬底温度、退火温度和溅射气体压强对LiNbO3薄膜结晶和表面形貌的影响,并用椭圆偏振仪测量了薄膜的厚度和折射率。结果表明:衬底温度为450℃时制备的薄膜,退火前后都没有LiNbO3相生成;衬底温度为500～600℃时,LiNbO3薄膜出现(012)、(104)和(116)面衍射峰,经600℃退火后3个衍射峰的强度加强;衬底温度为600℃时,经600～900℃退火得到的LiNbO3薄膜,除出现(012)、(104)和(116)面衍射峰外,还出现(006)面衍射峰;溅射气体压强从0.8 Pa增大到2.4 Pa时,经800℃退火后得到的LiNbO3薄膜表面晶粒团簇变小,而0.8 Pa制备的薄膜经800℃退火后LiNbO3相的结晶程度较其它压强下完善;900℃退火后得到的LiNbO3薄膜折射率为2.25,与LiNbO3晶体相当。     

一些常见混凝土裂缝的成因及预防

混凝土结构常因收缩变形和温度变化产生裂缝,本文分析了具体的原因,并从理论和实践上提出了防止和减少混凝土裂缝的一些措施。     

液体温度对空泡生长和溃灭过程的影响

采用光偏转测试系统研究了不同温度纯净水中激光空泡脉动过程,通过实验获得了激光空泡在靶表面膨胀和收缩全过程,确定了空泡的最大、最小泡半径、脉动周期和泡壁运动速度。实验采用0℃到70℃的纯净水,测量了空泡的泡半径和脉动周期等特征参量变化情况。实验结果表明,液体温度是影响空泡脉动的一个非常重要的因素,随着液体温度的增加空泡的最大泡半径和溃灭周期均呈增加趋势。给出了相应的理论解释。     

单光纤光栅对温度与应变的同步测量

提出了一种采用单光纤布拉格光栅(FBG)进行温度与应变同步测量的新颖设计。一根FBG被分成等长的两部分,用环氧胶水涂敷在其中一部分的表面,再套上金属套管,此时可以看成具有不同的布拉格波长的2个FBG,利用它们之间不同的杨氏模量和热膨胀系数,应变和温度能够同步测量。实验结果表明,在2700με和75℃的测量范围内,可以达到约6.1με和1.0℃的应变和温度精确度,误差主要来源于光谱仪分辨率的限制和FBG其中一部分的胶水涂抹不够均匀,通过使用高分辨率的解调仪和提高胶水涂抹工艺可得到更高的测量精确度。     

电弧喷涂马氏体不锈钢涂层残余应力分析

热喷涂涂层的残余应力对涂层与基体金属间的结合以及涂层的使用性能都有显著的影响.为了研究热喷涂工艺参数以及沉积涂层温度对涂层残余应力的影响,使用4Cr13马氏体不锈钢作为喷涂材料,分析了在喷涂过程中保持试件处于180～390℃温度范围条件下形成涂层的应力分布状况,采用电测法测定了涂层的杨氏模量和泊松比.结果表明,当沉积涂层温度保持在大约260℃时,形成的涂层到室温时有最小的残余应力.高于此温度,获得拉应力涂层;低于此温度,涂层处于压应力状态.电弧喷涂4Cr13马氏体不锈钢涂层的杨氏模量为53.1GPa,涂层的泊松比为0.1028,涂层的杨氏模量小于原始喷涂材料.     

厌氧活性污泥PCR-DGGE图谱的优化

针对特种污泥PCR-DGGE图谱的优化一直是微生物分子生态学研究的重点.在反硝化抑制硫酸盐还原菌的研究中,研究厌氧硫酸盐还原污泥和反硝化污泥DNA的提取方法,应用通用引物958F/1401R扩增16S rDNA序列,探讨不同的退火温度对DGGE指纹图谱多样性影响,同时采用时间进程法对DGGE图谱进行优化.结果表明,采用PBS洗涤污泥和超声震荡有利于硫酸盐还原污泥DNA提取;采用958F/1401R为引物时,扩增片段大约500 bp,不同的退火温度对DGGE指纹图谱的多样性影响不显著;采用时间进程法可以很好地再现不同电泳阶段对样品的分离效果,最佳变性剂梯度为40%～60%,在130 V电压下,最佳电泳时间为5 h.     

混凝土底板温度及温度应力影响参数分析

借助参数化设计语言(APDL)分析了水泥品种及标号、结构尺寸、外界约束对混凝土底板温度及温度应力的影响.结果表明:与普通硅酸盐水泥525相比,普通硅酸盐水泥425、矿渣水泥425可使底板最大拉应力分别减低约21%、37%;底板平面尺寸增大,压应力几乎保持不变,拉应力增大,发展较为平缓;底板厚度越大,出现最高温度的龄期越晚,底板降温时持续高温时间更长,且温度应力随厚度增大而增大.     

Evolution of carbides and carbon content in matrix of an ultra-high carbon sintered steel during heat treatment process

DTA, thermal expansion, XRD, and SEM were used to evaluate the effect of quenching temperature on the mechanical properties and microstructure of a novel sintered steel Fe-6Co-1Ni-5Cr-5Mo-1C. Lattice parameters and the mass fraction of carbon dissolved in the matrix of the steel quenched were investigated. It is discovered that the hardness of the steel increases with quench-ing temperature in the range of 840-900℃ and remains constant in the range of 900 to 1100℃. It decreases rapidly when the tem-perature is higher than 1100℃. The mass fraction of carbon dissolved in the matrix of the steel quenched at 840℃ is 0.38, but when the quenching temperature is increased to 1150℃, it increases to 0.98. The carbides formed during sintering are still present at grain boundaries and in the matrix of the steel quenched at low quenching temperatures, such as 840℃. When the quenching temperature is increased to 1150℃, most of the carbides at grain boundaries are dissolved with just a small amount of spherical M23C6 existing in the matrix of the quenched steel.     

Numerical simulation on the rheo-diecasting of the semi-solid A356 aluminum alloy

The effect of injection pressure, piston velocity, and the forming temperature of semisolid slurry on the filling behavior of the semi-solid A356 aluminum alloy was investigated by simulation methods. The simulation results show that these processing parameters have an important effect on the filling behavior of the semi-solid A356 aluminum alloy. The slurry flows steadily in the cavity when the injection pressure, the piston velocity, and the forming temperature are low, but it is prone to turbulent flow w...     

Effects of annealing temperature on the microstructure and properties of the 25Mn-3Si-3Al TWIP steel

Microstructures and mechanical properties of the 25Mn twinning induced plasticity (TWIP) steel at different annealing temperatures were investigated. The results indicated that when the annealing temperature was 1000°C,the 25Mn steel showed ex-cellent comprehensive mechanical properties,the tensile strength was about 640 MPa,the yield strength was higher than 255 MPa,and the elongation was above 82%. The microstructure was analyzed by optical microscopy (OM),X-ray diffraction (XRD),and transmission electron...