高层结构几何非线性分析的QR法

本文利用ＱＲ法分析高层建筑结构几何非线性问题，建立了新的计算格式。该法不仅未知量的数目少，精度高，而且输入简单，计算速度快，可以用微机分析复杂问题。     

软X射线光刻研究现状和发展

新的一代光刻设备朝着两个方向发展 ,一是趋向于大数值孔径、短波长 ;另一方面国际上正在寻求适应二十一世纪、小于 0 .1 5微米线宽的软 X射线投影光刻技术 ,预计成为下世纪制造千兆位以上超大规模集成电路的主要设备。软 X射线光刻及其应用研究是目前国际上非常活跃的高技术领域。把软 X射线光刻列为重要发展项目。本文摘要综述德国、美国、日本、俄罗斯等国近年来在软 X射线光刻关键单元技术及整机研究和发展方面的概况、预计下世纪初美国和日本将有软 X射线投影光刻机投入工艺生产线     

尼龙6表面金属(Ni)化膜材料的制备及性能研究

用化学还原法制得了尼龙６表面金属（Ｎｉ）化膜材料。研究了还原条件，金属盐浓度对膜材料电性能的影响，以及膜材料的电发热性能，用光电子能谱和扫描电子显微镜对其表面及形貌进行了表征。     

大泵站超驼峰水位运行压缩空气断流系统的设计方法

阐述了压缩空气断流的原理，提出了压缩空气断流装置的一般构成和设计方法，首次应用气体喷射器作为压缩空气减压增量变换器，不但及时地增加了补气量，防止断流后流道压力的下降，而且大大减小了储气罐容积，使该项技术得以满足工程实际的要求，为同类泵站的技术改造     

低渗透挥发性油藏注烃类气驱室内实验研究

通过注烃类气驱实验研究，了解文留油田低渗透挥发性油藏注气开发的一般机理和开发特点。采用PVT分析方法分析地层流体的物理性质、注入溶剂的组份；通过细管实验研究地层流体同注入溶剂在130℃时的最小混相压力；长岩心驱替实验分析气驱、水驱、水气交替注气的采收率、压力的变化规律。细管实验研究表明，最小混相压力为47．1MPa，长岩心注天然气驱替实验表现出近混相的特征。天然气驱注气压力低，采收率高，适合于文南油田低渗透挥发性油藏。     

Electrochemical noise analysis for estimation of corrosion rate of carbon steel in bicarbonate solution

We have investigated the electrochemical noise behavior of carbon steel in fully deaerated aqueous bicarbonate solutions, and discussed the optimum conditions of the noise analysis for estimating corrosion rate of the steel. Noise of the potential difference and of the short-circuit current between two identical steel coupons were successfully measured. The time-series noise patterns were transformed into frequency domain by fast Fourier transformation, and then their power spectrum densities (PSDs) at a frequency were determined to be compared with the corrosion rate. The PSDs of the potential and of the current varied with changing environmental factors of bicarbonate concentration, pH, and immersion time. The factors also controlled the corrosion rate of the steel. The PSDs were associated with the corrosion rate, and then it was found that the PSDs of the potential and of the current showed linear correlation with the corrosion rate in log-log scale. There was also linear relationship between the corrosion rate and a spectral noise resistance obtained from the PSDs of the potential and the current. The linearities of the three correlations were better at a lower analyzed frequency. Furthermore, the PSDs of the current and the noise resistance indicated more linear correlation with the corrosion rate than that of the potential. As the simplicity of the measurement system is additionally considered, it is concluded that the PSD of the current noise at an analyzed frequency of 3 mHz is the optimum conditions for estimating the corrosion rate from 10⁻² to 10⁰ A m⁻² in this study.     

一种新型图形描述算法

本文提出一种新型的图形描述算法，该算法以各种规则图形作为图形的最小处理单位。利用本算法构造的图形管理系统可广泛用于环境实时监控、采样数据动态显示等领域     

高砂比压裂技术研究

应用由美国ＮＳＩ公司引进的“ｓｔｉｍｐｌａｎ”拟三维压裂设计软件，对影响裂缝内支撑剂铺置浓度的诸因素进行了灰色关联度分析，从中找出了主要的影响因素。并以高砂比压裂的技术指标为依据，研究了在目前压裂工艺水平下，进行高砂比压裂所必须遵循的原则。文中还对国内的高砂比压裂进行了实例分析，进一步论证了文中的观点。     

特征线法分析长距离输油管道的流动瞬变过程

本文建立了基于特征线方法求充动瞬变过程的数值模型，编制了针对长距离输油管道流动瞬变过程的分析软件。在数值处理上，Ｄａｒｃｙ＝Ｗｅｉｓｂａｃｈ摩擦力项用二阶精度格式来近似，因此保证了高粘度流体在流动瞬变过程分析时的计算稳定性和精确度。模型考虑了埋管地形对沿线瞬变压力的影响，当某一泵站发生水击后其它站的反应同其上控程序确定。应用该软件，分析模拟了某一长距离输油管道在中间泵站停电或末站瞬时关阀情况下的流     

Enantioseparation of catechin and epicatechin in plant food by chiral capillary electrophoresis

The enantiomers of catechin and epicatechin were separated by chiral capillary electrophoresis using modified cyclodextrins as chiral selectors. Various conditions for the separation system were optimized, including the pH value and the concentration of the running buffer. A baseline separation of the catechin and epicatechin enantiomers could be achieved by using 0.1 mol l⁻¹ borate buffer (pH 8.5) with 12 mmol l⁻¹ (2-hydroxypropyl)-γ-cyclodextrin as chiral selector, a fused-silica capillary with 40 cm effective length (75 μm I.D.), +18 kV applied voltage, a temperature of 20 °C and direct UV detection at 280 nm. The method was applied to different plant food samples. (+)-Catechin and (−)-epicatechin could be verified as the most common flavan-3-ols. In the case of guaraná, however, we were able to identify all four enantiomers, both (+)- and (−)-catechin and (+)- and (−)-epicatechin, as naturally occurring compounds. This finding was verified by further isolation and purification of the flavan-3-ols and subsequent LC–MS analysis. This method allows for the identification of the authenticity of guaraná through the analysis of the catechin and epicatechin enantiomers, additionally to the conventional methods like HPLC.