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121.
《Information Processing Letters》2014,114(6):317-321
We propose an output-sensitive algorithm for the enumeration of all maximal bicliques in a bipartite graph, tailored to the case when the degree distribution in one partite set is very skewed. We accomplish a worst-case bound better than previously known general bounds if, e.g., the degree sequence follows a power law. 相似文献
122.
本方法以150×3.9mm(i.d)NovapakC184μm不锈钢柱为色谱柱,二氯甲烷+甲醇+异丙醇+水为流动相,在检测波长为252nm下对60%硫·三环可湿性粉剂进行液相色谱分析。三环唑和硫磺的标准偏差分别为0.12%和0.15%;变异系数分别为0.39%和0.31%;线性相关系数分别为0.9999和0.9997;平均回收率分别为99.63%和99.26%。 相似文献
123.
Controlling the linear alkylbenzene sulfonate (LAS) sulfonation process is a critical part of the LAS manufacturing process;
this process can be monitored by assaying for LAS content, unsulfonated linear alkylbenzene (LAB), and LAB sulfones. Traditionally,
assaying the LAB and LAB sulfone contents has been time consuming and not straightforward. A simple and rapid procedure is
described for the isolation and simultaneous capillary gas chromatographic (GC) quantification of LAB and LAB sulfones in
LAS. The procedure involves extraction of the unsulfonated LAB and the LAB sulfones into n-heptane; sodium linear alkylbenzenesulfonate or linear alkylbenzenesulfonic acid (reacted to form sodium linear alkylbenzenesulfonate)
remains in the aqueous extraction solvent layer. High-temperature capillary GC using a specialty metal capillary column enables
both LAB and high molecular weight LAB sulfones to be quantified. 相似文献
124.
125.
N-甲基乙酰氧基乙酰苯胺的液谱分析 总被引:1,自引:0,他引:1
本文研究了高效液相色谱测定N-甲基乙酰氧基乙酰苯胺的方法。采用Hypersil C18柱,以甲醇:水=60:40(V/V)为流动相。该方法的变异系数为0.43%,回收率为98.9%-100.6%。 相似文献
126.
《Advanced Engineering Informatics》2014,28(4):381-394
The dangers of the construction industry due to the risk of fatal hazards, such as falling from extreme heights, being struck by heavy equipment or materials, and the possibility of electrocution, are well known. The concept of Job Hazard Analysis is commonly used to mitigate and control these occupational hazards. This technique analyzes the major tasks in a construction activity, identifies all potential task-related hazards, and suggests safe approaches to reduce or avoid each of these hazards. In this paper, the authors explore the possibility of leveraging existing construction safety resources to assist JHA, aiming to reduce the level of human effort required. Specifically, the authors apply ontology-based text classification (TC) to match safe approaches identified in existing resources with unsafe scenarios. These safe approaches can serve as initial references and enrich the solution space when performing JHA. Various document modification strategies are applied to existing resources in order to achieve superior TC effectiveness. The end result of this research is a construction safety domain ontology and its underlying knowledge base. A user scenario is also discussed to demonstrate how the ontology supports JHA in practice. 相似文献
127.
乙烯装置长周期运行安全风险分析与对策 总被引:2,自引:0,他引:2
分析了中国石化茂名石化公司化工事业部乙烯装置长周期运行的安全风险,讨论了风险控制措施。结果表明:乙烯装置连续运行6年,其安全风险属于可容许风险。 相似文献
128.
The indigo method developed by Bader and Hoigné for aqueous ozone analysis was modified to allow for both gaseous and aqueous ozone determination. Gas or water samples were extracted with a gas-tight syringe containing a known volume of indigo reagent. The modified procedure provided a more consistent basis for gaseous and aqueous ozone determination allowing for more accurate ozone mass balance calculations. Direct gaseous ozone UV absorbance with molar absorptivity of 3,000 M?1cm?1 at 258 nm was used as primary standard to determine the molar absorptivity of the indigo reagent. The molar absorptivity of indigo reagent, assuming a 1:1 stoichiometric ratio for the reaction between indigo and ozone, was determined to be 23,150 ± 80 M?1cm?1, or approximately 16 percent higher than that of 20,000 M?1cm?1 suggested by Bader and Hoigné. An independently calibrated membrane-electrode ozone monitor showed good correlation with indigo method results using the molar absorptivity value determined in this study. The apparent molar absorptivity of aqueous ozone at the wavelength of 258 nm measured by the modified indigo method increased from 2,400 to 3,600 M?1cm?1 in the investigated ozone concentration range of 0.4 to 11.0 mg/L. This variation might have been caused by the inherent interference of unidentified ozone byproducts, which presence was supported with scanning spectra in the wavelength range of 200 to 300 nm. 相似文献
129.
采用气相色谱法,氢火焰离子化检测器,选用3%OV-17填充柱,正十三烷为内标,气化室和检测器温度为180℃,柱温120℃,对3溴4氟苯甲醛进行定量测定。该方法简单、快速、准确、适用,标准偏差0.26%,变异系数0.27%,平均回收率100.1%。 相似文献
130.
高效液相色谱法在农药残留分析中的应用 总被引:4,自引:0,他引:4
朱正斌 《化学工业与工程技术》2004,25(6):51-53
介绍了高效液相色谱法在农药残留分析中的应用,列举了一些杀虫剂、除草剂、杀菌剂的分析方法,指出了高效液相色谱法在农药残留分析中发展方向。 相似文献