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991.
Linear oligosiloxanes functionalized with bulky side chain tris(trimethylsilyl)hexyl (TTSH) substituents were transformed into cross-linked materials by UV 193 nm excimer pulsed laser ablation. The process occurred without any catalyst, by reactions of radicals formed in UV laser induced photolysis of side tris(trimethylsilyl)hexyl groups. Chemical changes were monitored by FTIR, LC/UV, GC/MS and solubility tests. 相似文献
992.
A tertiary amine functionalized 4-nitro-4′-alkoxy azobenzene mesogen with a 10 or 12 carbon spacer (azo-nN) was synthesized and complexed in equimolar proportions with poly(acrylic acid) (PA-H) and poly(sulfonic acid) (PSS-H), and investigated by thermogravimetric analysis, differential scanning calorimetry, polarizing optical microscopy, Fourier transform infrared spectroscopy and X-ray diffraction. The neat azo-nN is characterized by a partial bilayer SA mesophase at higher temperatures, and a highly ordered phase, in which the molecules are stacked orthogonally in bilayers, at lower temperatures. As supported by infrared analysis, for the azo-nN/PA-H mixture, the complexation is partial while for the same azo-nN/PSS-H mixture, complete proton transfer occurs. When the azo-nN is blended with the PA-H, regarded as a weak acid, a biphasic system is generated and the thermotropic behavior of neat mesogen is not significantly affected. In contrast, by mixing the same mesogen with a PSS-H (regarded as a strong acid), the thermotropic behavior is significantly influenced: the complexation generated a partial or interdigitated smectic A or tilted smectic C lamellar phase. 相似文献
993.
管线油电损耗的灰色模型及预测 总被引:11,自引:2,他引:9
对于管道运输来说,影响输油成本变化的因素有很多,但是对总成本影响最大的是油电损耗费用。由于来自现场的输量和相关参数样本数据不足,只知道连续几年的流量、油电损耗,要预测将来每年的油电损耗,经典经济数学不能满足这样的研究。然而灰色系统理论要求的研究样本较少,只要知道连续几年的流量、油电损耗,就能预测将来每年的油电损耗,估算其输油成本,且模型精度较高。利用灰色系统理论,以输油管线每年的输量、相应的电耗和油耗为时间序列,建立了三元素非等间距GM(1,1)模型,该模型为预测管线年输油成本提供了可靠的依据。 相似文献
994.
The Mean Opinion Scale (MOS) is a questionnaire used to obtain listeners' subjective assessments of synthetic speech. This paper documents the motivation, method, and results of six experiments conducted from 1999 to 2002 that investigated the psychometric properties of the MOS and expanded the range of speech characteristics it evaluates. Our initial experiments documented the reliability, validity, sensitivity, and factor structure of the P.L. Salza et al. (Acta Acustica, Vol. 82, pp. 650–656, 1996) MOS and used psychometric principles to revise and improve the scale. This work resulted in the MOS-Revised (MOS-R). Four subsequent experiments expanded the MOS-R beyond its previous focus on Intelligibility and Naturalness, to include measurement of the Prosody and Social Impression of synthetic voices. As a result of this work, we created the MOS-Expanded (MOS-X), a rating scale shown to be reliable, valid, and sensitive for high-quality evaluation of synthetic speech in applied industrial settings. 相似文献
995.
扫描式X光机及DDS在其运动控制中的应用 总被引:2,自引:0,他引:2
扫描式X光机是一种高精度,高性能的新型医疗设备,其显著优点在于大大降低了患者所受X光辐射剂量,可直接得到患者清晰的X光数字图像,缩短出片时间,X光片资料存储方便,便于实现远程诊断,该设备对运动控制部分的匀速性,平稳性和多次扫描的位置重复性的要求均很高。本文主要针对其运动控制部分的结构特点,分析了影响运动性能的主要原因,并将直接数字频率合成器应用于调速,从而实现了对其运动控制部分的要求。 相似文献
996.
Hu Kai Yang Xianjin Cai Yanli Cui Zhenduo Wei Qiang 《Frontiers of Materials Science in China》2007,1(3):229-236
A hydroxyapatite (HA)/collagen (COL) composite coating on NiTi shape memory alloy (SMA) was prepared by eletrochemical deposition
(ELD) in modified simulated body fluid (MSBF). To draw comparisons of physical characteristics and bioactivity of the composite
coating, the HA/COL composite coating was also prepared by chemically biomimetic growth (BG) and the ELD coating was re-soaked
in MSBF again for further biomimetic growth (called EBG method in this paper). It was indicated that the c-axis of HA crystals
was oriented parallel to the longitudinal direction of the COL fibril in BG and EBG coating, which could not found in ELD
coating. The EBG method could induce a denser, thicker and better crystallized HA/COL coating. The cell culture test indicated
that the BG coating presented better cell biocompatibility. 相似文献
997.
GIS数据库中的数据挖掘 总被引:6,自引:0,他引:6
首先探讨了DM在GIS中应用的必要性和可能性,然后讨论了GIS数据库中的DM可以发现的知识类型、可以使用的方法,可以采用的DM系统原型,最后简单介绍了DM对GIS的贡献。 相似文献
998.
利用自行研制的“光电阴极多信息量测试系统”首次对国产三代微光管中的GaAs光电阴极的均匀性进行了光谱响应测试 ,结果表明该国产三代微光管存在明显的非均匀性。利用曲线拟合方法估算了GaAs光电阴极的材料性能参数 ,发现表面逸出概率不一致是非均匀性的主要原因 ,GaAs材料的少子扩散长度 (1 1 2~ 1 82 ) μm ,与阴极厚度相当 ,后界面复合速率在 (1× 1 0 5~ 1× 1 0 6 )cm/s之间 ,它限制了阴极灵敏度的提高 相似文献
999.
1000.
We present the fabrication and short circuit test results of a 14 kV single-phase resistive superconducting fault current limiter (SFCL) based on YBa2Cu3O7 (YBCO) films. Individual components were processed using the 4″ YBCO films and have the rated voltage and current of 600 V and 35 A at 77 K, respectively. Twenty four components, eight components in series and three lines in parallel, make a module having the rated voltage and current of 4.8 kV and 105 A, respectively. Three modules were assembled in series to produce the SFCL working at 77 K, a 14 kV single-phase machine for the 22.9 kV Y-Y grid. short circuit tests were successfully conducted in an accredited test facility with the maximum fault currents up to 14.1 kAP. All components quenched together upon faults and shared the rated voltage evenly without any supplementary device between the modules. This proves that the SFCL based on YBCO films may not only work reliably at 22.9 kV, but also provide technical feasibility for higher voltage application including the transmission grids. 相似文献