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51.
52.
This paper investigates the catalytic ignition of the H2/O2/CO2 mixture on platinum in a stagnation flow at atmospheric pressure experimentally and numerically. We measure the ignition temperatures of the gas mixtures flowing towards resistively heated platinum with various composition ratios and various diluent gases of N2, Ar and CO2. Compared with N2 or Ar, the CO2 dilution shows higher ignition temperature by about 50 K, even at the same composition ratio. The ignition temperature increase is proportional to the dilution ratio. Through the numerical simulation, it is illustrated that higher ignition temperature is caused by the adsorption of CO2 and following dissociation on platinum surface, which was to date considered negligible in catalytic combustion. 相似文献
53.
Investigation into polishing process of CVD diamond films 总被引:1,自引:0,他引:1
A new technique used for polishing chemical vapor deposition (CVD) diamond films has been investigated, by which rough polishing of the CVD diamond films can be achieved efficiently. A CVD diamond film is coated with a thin layer of electrically conductive material in advance, and then electro-discharge machining (EDM) is used to machine the coated surface. As a result, peaks on the surface of the diamond film are removed rapidly. During machining, graphitization of diamond enables the EDM process to continue. The single pulse discharge shows that the material of the coated layer evidently affects removal behavior of the CVD diamond films. Compared with the machining of ordinary metal materials, the process of EDM CVD diamond films possesses a quite different characteristic. The removal mechanism of the CVD diamond films is discussed. 相似文献
54.
使用金相显微镜、扫描电镜及X射线能谱和波谱观察并分析了NdFeB烧结材料中夹杂物的形态、数量和组成。磁粉制备后立即烧结的NdFeB磁体中的夹杂物是氧化钕;而在不同环境条件下放置后的NdFeB粉再烧结的材料中发现,除了氧化钕的夹杂物外,还有钕的氮化物及钕的氮氧复合夹杂物。同时还论讨了这些夹杂物对于NdFeB材料磁性能的影响。 相似文献
55.
Daniela M. Nevskaia Maria Luisa Rojas Cervantes Antonio Guerrero Ruíz Juan de Dios Lpez Gonzlez 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1995,63(3):249-256
Adsorption of Triton X-100 on various silica substrates has been investigated. A number of solids, including a natural quartz, this quartz washed with HCl acid and subsequently heated at 1273 K; two aerosils and one Kieselgel silicas were studied. These solids exhibit surface areas in the range of 5 to 430 m2 g?1. All the Triton adsorption isotherms display an S-shape at the adsorption temperatures studied (298 and 308 K). It has been found that the pretreatments of natural quartz (by water washing, impurities removed by acid and/or high temperature calcination) affect considerably the amounts of TX-100 adsorbed. Measurements of surface composition have been made by X-ray photoelectron spectroscopy (XPS) with particular emphasis on the presence of impurities and on the number of OH groups at the surface of the samples. The nature of the surface hydroxyl has also been studied by infrared spectroscopy. Furthermore, the specific number of hydroxyl groups on the surface of the silica samples has been determined by thermogravimetric analysis. Finally an attempt to correlate solid surface characteristics with adsorption isotherms has been developed. 相似文献
56.
本文在液相合成(SrPb)TiO3粉的基础上,研究了升温速率、保温时间、烧结温度及降温方式对(SrPb)TiO3基陶瓷的V型PTC热敏特性的影响。实验表明:升温速率对其热敏特性影响不大,保温时间和烧结温度的作用是一致的,具有一最佳范围。而降浊方式对材料的热敏特性影响较大。综合各因素的影响,本配方中,样品的烧结制度定为:以200℃/h的速率升温,在1250℃保温1h,炉冷至950℃,保温0.5h,再 相似文献
57.
通过加入增强剂、增韧剂、抗氧剂等添国剂可改善聚丙烯力学性能。以SiO2为填料,丁苯橡胶(SBS)为增韧剂,探讨SiO2、丁苯橡胶含量对共混体系强度、韧性的影响,结果表明,在SBS含量大于5%、SiO2一小于10%的范围内,可使PP/SiO2/SBS复合的拉伸弹性模量和冲击强度明显提高,其力学性能均为均衡。 相似文献
58.
氢电弧等离子体法制备的纳米镍铈粒子的催化特性 总被引:3,自引:0,他引:3
利用氢电弧等离子法制备具有储氢特性纳米镍铈粒子,并在气相苯加氢反应中研究了其催化特性,发现其催化活性与储氢特性及表面层中NiCe合金存在有关,且具有高的选择性和热稳定性,这与纳米粒子独特的结构及铈的加入有关。 相似文献
59.
María P. Albano Liliana B. Garrido 《Journal of Materials Synthesis and Processing》2002,10(4):211-218
Si3N4powders coated with 6 wt% Y2O3and 4 wt% Al2O3were prepared by coprecipitation. The resulting powders were dispersed in water at different pH values and with addition of various amounts of ammonium polyacrylate (NH4PA) to produce 32 vol% slips. The influence of the amount of NH4PA solution added and pH on the rheological properties of 32 vol% coated Si3N4slips were studied. In addition, the sintered density of cast samples was determined and related to the degree of slip dispersion. The adsorption of the NH4PA on the coated particle surface was rather high and the surface became saturated near 0.86 mg/m2at pH 9.2. High NH4PA concentrations (1.7–3 wt%) were necessary to obtain well dispersed 32 vol% coated Si3N4slips at pH 9.2. The best stabilization was obtained with the addition of 2.3 wt% NH4PA; in this condition, the viscosity reached a minimum value of 35 mPa.s at 100 s–1. The slip viscosity increased with increasing pH from 9.2 to 10.2. Slips with low viscosities gave a more dense packing of cast samples and consequently higher sintered density values. 相似文献
60.