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31.
The transitions and reactions involved in the thermal treatment of several commercial azodicarbonamides (ADC) in an inert atmosphere have been studied by dynamic thermogravimetry analysis (TGA), mass spectrometry and Fourier transform infrared (FTIR) spectroscopy. A pseudo‐mechanistic model, involving several competitive and non‐competitive reactions, has been suggested and applied to the correlation of the weight loss data. The model applied is capable of accurately representing the different processes involved, and can be of great interest in the understanding and quantification of such phenomena, including the simulation of the instantaneous amount of gases evolved in a foaming process. In addition, a brief discussion on the methodology related to the mathematical modeling of TGA data is presented, taking into account the complex thermal behaviour of the ADC. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
32.
基于带传动在稳定工作时的受力平衡,从理论上导出了摆架式自动张紧装置所产生的张紧力的计算公式。结果表明:只要合理选择计算安装参数,其张紧力总能满足张紧条件的要求,以对张紧装置进行设计计算;并指出该装置产生的张紧力,具有随外载荷变化而自动调节的性能,使传力零件部分卸载。 相似文献
33.
34.
生烃化学动力学在川东北普光气田的应用 总被引:9,自引:2,他引:7
普光气田是四川盆地近期发现的规模最大、埋藏最深、资源丰度最高的气田。通过认识普光气田各个烃源岩层的贡献量、生烃关键期与构造演化的关系、油气成藏具体模式等,建立生烃化学动力学模型、标定参数,结合地区烃源岩参数和地史、热史资料,定量描述该地区的生烃过程及油裂解成气过程。认为:普光地区的主力烃源岩为下志留统泥岩;主要干酪根生油期为早二叠世末到早三叠世末期(距今286Ma至240Ma);主要干酪根生气期为中三叠世(距今240Ma至230Ma);主要气源是原油后期热裂解气,原油裂解成气的时间比较晚,主要油裂解成气期为早白垩世(距今144Ma至97.5Ma),从而决定了普光气田的成藏模式为“多期成藏,油气转化,晚期定位”。图2表3参33 相似文献
35.
The objective of this study is to determine the chemical kinetics of desulphurization of Thai limestone in an atmospheric fluidized bed combustor (AFBC). The experiments, which employed the batch technique using the limestone samples from six major sources in Thailand, were performed in a laboratory‐scale AFBC. The results obtained were analysed and correlated in the form of apparent reaction rate and deactivation rate constants as a function of operating conditions of the furnace and their properties, respectively. The formulae derived from these correlations were kept as general as possible in order that they could be used as input parameters for the selected mathematical model of desulphurization in an AFBC that is suitable for practical use. The predicted results were in good agreement with the experimental data reported in the literature. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
36.
为提高抽油机减速器齿轮铸件的机械性能,提出以Sn代替Mo作为合金元素,并通过试验确定了合理的Si、Cu、Sn的加入量。指出Si加入量应控制在1.9%-2.1%范围内,同时加入0.36%~0.9%的Cu和0.025%~0.07%的Sn,可保证球铁的强度和延伸率都满足QT700-2的要求。鉴于试件与实际铸件的表面硬度有一定的差值,为提高铸件表面硬度,进行了余热正火试验,并给出了铸件在铸型内的时间-冷却温度曲线。最后根据球铁化学成分的选择结果,进行了齿轮生产试验。 相似文献
37.
A numerical study of the transport phenomena arising in a single-screw extruder channel is carried out. A non-Newtonian fluid
is considered, using a power law model for the variable viscosity. Chemical reaction kinetics are also included. Finite difference
computations are carried out to solve the governing set of partial differential equations for the velocity, temperature and
species concentration fields, over a wide range of governing parameters for the case of a tapered screw channel.
The numerical treatment for this combined heat and mass transfer problem is outlined. A marching procedure in the down-channel
direction is adopted and the validity of the scheme for practical problems discussed. For large viscous dissipation, the material
heats up considerably due to the prevailing shear field, affecting the viscosity significantly, and results in large changes
in the pressure development at the end of the channel. The rate of reaction controls the mass diffusion rate which in turn
affects viscosity and the flow significantly. The dimensionless throughput,q
v
, is one of the most important parameters in the numerical solution. The dimensionless pressure variation is very sensitive
toq
v
, and orders of magnitude changes are possible for small variations inq
v
. Schemes for dealing with other important effects such as back flow, heat transfer by conduction in the barrel, and the effect
of the die are also outlined.
A list of symbols is given at the end of the paper
This is publication No. F-10544-4-91 of the New Jersey Agricultural Experiment Station supported by State Funds and the Center
for Advanced Food Technology (CAFT). The Center for Advanced Food Technology is a New Jersey Commission on Science and Technology Center. This work was also
supported in part by the US Army Research Office. 相似文献
38.
R. Niebuhr K. H. Bachem U. Kaufmann M. Maier C. Merz B. Santic P. Schlotter H. Jürgensen 《Journal of Electronic Materials》1997,26(10):1127-1130
Oxygen doped GaN has been grown by metalorganic chemical vapor deposition using N2O as oxygen dopant source. The layers were deposited on 2″ sapphire substrates from trimethylgallium and especially dried
ammonia using nitrogen (N2) as carrier gas. Prior to the growth of the films, an AIN nucleation layer with a thickness of about 300? was grown using
trimethylaluminum. The films were deposited at 1085°C at a growth rate of 1.0 μm/h and showed a specular, mirrorlike surface.
Not intentionally doped layers have high resistivity (>20 kW/square). The gas phase concentration of the N2O was varied between 25 and 400 ppm with respect to the total gas volume. The doped layers were n-type with carrier concentrations
in the range of 4×1016 cm−3 to 4×1018 cm−3 as measured by Hall effect. The observed carrier concentration increased with increasing N2O concentration. Low temperature photoluminescence experiments performed on the doped layers revealed besides free A and B
exciton emission an exciton bound to a shallow donor. With increasing N2O concentration in the gas phase, the intensity of the donor bound exciton increased relative to that of the free excitons.
These observations indicate that oxygen behaves as a shallow donor in GaN. This interpretation is supported by covalent radius
and electronegativity arguments. 相似文献
39.
40.