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61.
Phase separation during polymerization was studied in a model system consisting of a diepoxide based on diglycidyl ether of bisphenol A (DGEBA), variable amounts of ethylenediamine (EDA) and the mass of castor oil (CO) necessary to obtain a mass fraction equal to 0-15 in a final system where the stoichiometric ratio of amine to epoxy equivalents, r, was equal to 1. A two-step polymerization process was performed by curing first a system with r = 0-5, during variable times before phase separation, and then carrying the system to r = 1. Thermodynamic analysis of samples with different r values led to a linear relationship between the Flory-Huggins interaction parameter and r. The concentration (P) and average size (D?) of dispersed-phase particles followed opposite trends, i.e. P increased while D? decreased, when either r was increased or the time of curing in the first step of a two-step process was decreased. This was explained by assuming that the competition between nucleation and growth was determined by the viscosity at the cloud point, ηcp. Low values of ηcp favoured growth over nucleation and led to fewer but larger particles. 相似文献
62.
无间隙原子钢的微观结构特征和塑性应变比 总被引:1,自引:0,他引:1
采用X射线衍射的ODF和LP分析技术,SEM电子通道花样和蚀坑技术观测,研究了超深冲无间隙原子钢板的微观结构特征。结果表明:控制化学成分、保证基体纯净、优选工艺参数,促进强的γ-〈111〉∥N.D纤维织构的形成是获得优异成型性的关键。用CMTP方法,由ODF织构数据从理论计算了塑性应变比(r),表明rm值高达3.18。文中讨论了再结晶织构形成机制。 相似文献
63.
恢复地层剥蚀厚度方法综述 总被引:28,自引:2,他引:26
恢复地层剥蚀厚度是对盆地进行定量研究的重要基础工作。本文综述、评价了目前常用的恢复剥蚀厚度的方法,并对作者曾提出的天然气平衡浓度法作了进一步的阐述。 相似文献
64.
65.
Anionic copolymerizations of styrene (M1) with excess 1-(4-dimethyl-aminophenyl)-1-phenylethylene (M2) were conducted in benzene at 25°C for 24h, using sec-butyllithium as initiator. Narrow molecular weight distribution copolymers with M?;n = 16.1 × 103 g/mol (M?w/M?n = 1.04) and 38.2 × 103g/mol (M?w/M?n = 1.05), and 24 and 38 moles of M2 per macromolecule, respectively, were characterized by size exclusion chromatography, 1H NMR spectroscopy and DSC. The monomer reactivity ratio, r1 = 5.6, was obtained from the copolymer composition at complete consumption of M1, assuming that the rate constant k22 =0,i.e. r2 =0. The polymers exhibited Tg values of 128 and 119°C, respectively, which correspond to an estimated Tg = 217°C for the hypothetical homopolymer of M2. 相似文献
66.
Air cleaning as a means of mitigating the risks arising from exposure to indoor radon progeny has been evaluated in a single-family house in the north eastem US. using an automated, semi-continuous activity-weighted size distribution measurement system. The measurements included radon concentration, condensation nuclei count, and activity-weighted size distribution of radon decay products. Measurements were made in the house with and without an operating air filtration system and with various particle sources common to normal indoor activities operating. Aerosols were generated by running water in a shower, candle burning, cigarette smoking, vacuuming, opening doors, and cooking. Using a room model, the changes in attachment rates, average attachment diameters, and deposition rates of the unattached fraction with and without the air cleaning system were calculated. In the presence of active aerosol sources, the air filtration unit typically reduced the concentration of particles within the hour following the end of particle generation. After candle burning, cigarette smoking, and vacuuming in the bedroom, the reductions of PAEC by air filtration are about 60% with the air filtration system operating in the bedroom. During cooking in the kitchen, the reductions of PAEC in the bedroom with the air filtration system were about 40%. However, for all cases the dose reductions were smaller than the particle and PAEC reductions. For those particles that were generated within the bedroom, there was a 20% to 50% reduction in dose. In the case of cooking where the door was open and particles infiltrated from the rest of the house, the dose reduction was only 5% on average and appears to be insignificant. Thus, the dose reductions were h e r than the reductions in activity concentration, but there were no cases where the estimated dose actually increased. 相似文献
67.
首先对OFDM的发展以及应用做了简要的介绍,然后讨论了当前OFDM研究过程中的两个关键技术问题,最后展望了OFDM的未来发展。 相似文献
68.
Yukihisa Tanaka Jiro Hirano Tadashi Funada 《Journal of the American Oil Chemists' Society》1992,69(12):1210-1214
In an attempt to concentrate the content of DHA (docosahexaenoic acid) in a glyceride mixture containing triglyceride, diglyceride
and monoglyceride, fish oil was hydrolyzed with six kinds of microbial lipase. After the hydrolysis, free fatty acid was removed
and fatty acid components of the glyceride mixtures were analyzed. When the hydrolysis withCandida cylindracea lipase was 70% complete, the DHA content in the glyceride mixture was three times more than that in the original fish oil.
The EPA (eicosapentaenoic acid) content became almost 70% of the original fish oil. Hydrolysis with other lipases did not
result in an increase in the DHA content in the glyceride mixtures. Hydrolysis of DHA-rich tuna oil (DHA content is about
25%) withCandida cylindracea lipase resulted in 53% DHA in the glyceride mixture. The EPA content, however, remained close to that of the original tuna
oil. In this report, the acyl chain specificity of lipases is evaluated in terms of hydrolysis resistant value (HRV). HRV
is the ratio between the DHA contents in the glyceride mixture of hydrolyzed oil and original oil. HRV clearly indicates differences
in hydrolysis between DHA and other fatty acids (e.g., saturated and monoenoic acids). 相似文献
69.
���ƾۺ����ཬ���������Ե�;�� 总被引:5,自引:0,他引:5
本文在肯定聚合物泥浆提高钻井速度的同时,也指出了该种泥浆在井内使用较长时间以后将会出现网架结构强、包被抑制性能减弱的弊病。为此,文中强调推出新的聚合物材料,研究泥浆中聚合物剩余浓度的测定方法及控制浓度的要领,提高固控效率净化泥浆等措施以解决之。 相似文献
70.
LIHong-kun MAXiao-fiang WANGZhen ZHUHong 《国际设备工程与管理》2003,8(4):233-238
The local wave method is a very good time-frequency method for nonstationary vibration signal analysis. But the interfering noise has a big influence on the accuracy of time-frequency analysis. The wavelet packet de-noising method can eliminate the interference of noise and improve the signal-noise-ratio. This paper uses the local wave method to decompose the de-noising signal and perform a time-frequency analysis. We can get better characteristics. Finally, an example of waveletpacket denoising and a local wave time-frequency spectrum application of diesel engine surface vibration signal is put forward. 相似文献