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101.
Meng Wai Woo 《Drying Technology》2008,26(1):15-26
Current methods in alleviating the wall deposition problem in spray drying emphasize mainly controlling the stickiness of the drying particles and less attention is placed on the properties of the dryer wall. In this experimental study, the effect of wall surface properties on the deposition mechanism has been investigated. Properties considered in classifying different wall materials were surface energy, roughness, and dielectric properties. The model solution contained sucrose, representing low-molecular-weight sugars commonly encountered in spray drying of fruit and vegetable juices. The effect of wall properties on deposition was explored at different drying rates producing particles of different surface rigidity. Larger surface roughness produced higher deposition fluxes for particles with high impact velocity and moisture. Surface energy and surface roughness were found to have no significant effect for dry rigid particles at the middle and bottom elevation of the drying chamber. However, material with lower surface energy (Teflon) exhibited less deposition for rubbery particles at such elevations. Analysis shows that dielectric wall material (Teflon) tends to enhance deposition of dry particles because of attrition at the surface. Higher wall temperature was found to produce slightly more deposition. The results of this work give a general indication of the effect of wall material on the deposition problem and provide the fundamental understanding for further studies along this line. Proper selection of dryer wall material will provide potential alternatives for reducing the deposition problem. 相似文献
102.
Qingzhao Yao Yuming Zhou Yanqing Sun Xiaoyun Ye 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(4):477-484
TiO2 hybrid molecular imprinted polymer (MIP) for ethofumesate using methacrylic acid (MAA) as the functional monomer and silane
coupling agent 3-(trimethoxysilyl) propylmethacrylate (KH570) as organic–inorganic connective bridge was synthesized via photo-excitation
method. Hydrogen bond was proved to act between MAA and ethofumesate for pre- and post-polymerization binding properties as
testified by UV spectrometric method. KH570 modified TiO2 nanoparticles were prepared via sonochemical reaction, which can accelerate hydrolysis, increase collision chance for the
reactive system and improve the dispersion of the nanoparticles. Scanning electron microscope (SEM), transmission electron
microscope (TEM), binding and the adsorption kinetics experiments as well as thermogravimetric analysis (TGA) were employed
for characterization. The results indicated that the hybrid MIP revealed a larger surface area and more ordered imprinting
cavities with improved thermal stability compared to organic-only MIP. Furthermore, faster adsorption kinetics and enhancive
adsorption capacity were achieved, which made it promising in chemical sensor applications. 相似文献
103.
溶胶凝胶法聚合物/无机复合材料的研究与应用 总被引:2,自引:0,他引:2
介绍了制备聚合物/无机复合材料的溶胶凝胶原理,基本过程及制备途径,简要阐述了其在光学材料、电子材料、生物材料、涂层材料、纳米材料等领域的研究及应用进展,指出了其进一步研究的发展方向和重点。 相似文献
104.
《稀有金属材料与工程》2006,23(4):12-16
透过性能对用于过滤分离、流体混合、布气分流等方面的多孔材料是一项十分关键的质量指标。主要介绍了多孔材料透过性能的表征方式,包括流体流动的基本概念、层流条件下流体的透过性能表征、多孔材料透过性能的综合表征、气体透过多孔材料时渗透系数的具体表征等方面。 相似文献
105.
106.
Gomatofu (sesame tofu) is one of the traditional Japanese healthy foods and is representative of all shojin (vegetarian) dishes. Gomatofu, one of the mixed gels consisting of kudzu (arrowroot) starch and sesame, possesses an extremely unusual textural characteristic which is soft, smooth, and springy. The textural properties are greatly influenced by preparation, ingredients and roasting conditions of sesame seeds. Hence there are many kinds of sesame materials which can be used to prepare gomatofu such as white, black, huskless or not and roasted or unroasted sesame materials, in this study, the effects of these materials on the physical properties of gomatofu were studied. The sample of Ra-W prepared with unroasted huskless sesame seed had the least hardness, but mouthfeel of this sample were the highest. The samples of Ro-B and Ro-W prepared with roasted husk (black and white) sesame seed were evaluated to have the best palatability because of their superior springiness. It was clarified that different kinds of sesame materials affected the forming of structure and physical properties of gomatofu, because the chemical components were different from varieties of sesame materials. 相似文献
107.
A systematic investigation of the magnetic and transport properties of Ti doped La0.67Ca0.33MnO3 was reported. The Ti substitution for Mn ions results in a reduction in ferromagnetism and conductivity. The metal-insulator transition temperature is close to Curie temperature which decreases from 274 to 82 K as x increases from 0 to 0.17. The most important effect of Ti doping is to introduce spin clusters in the samples due to the distortion of local lattice and the inhomogeneous magnetic structure induced primarily by the random distribution of Mn ions. A maximum magnetoresistance ratio as large as 90% in 1 T at 122 K was obtained for the sample with x =0. 055, which is four times larger than that obtained for LCMO sample at 272 K. There is a remarkable field-history dependent MR in the cooling process for the doped samples while such phenomenon disappears in the warming run. The resistivity follows well the variable range hopping behavior in paramagnetic state. Both the size effect and spin dependent hopping of carriers between the spin clusters should be considered in this system. 相似文献
108.
CHENG Xiang 《半导体光子学与技术》2004,(4)
Amorphous carbon (a-C) films and amorphous carbon films incorporating with the nitrogen (a-C∶N) were deposited on silicon substrates in a radio-frequency driven plasma enhanced chemical vapour deposition system, while the surface electrical properties of films were investigated by electrochemical capacitance-voltage measurements. It was examined the effect of the interface defects on the properties and deduced that the conducting type of a-C∶N films was n-type. Subsequently, a comparative studies of a-C and a-C∶N films were performed by photoluminescence spectra depending on the temperature. With the decrease of the temperature, the main band with peak energy of 2.48 eV in the a-C∶N films was more intense compared with the other three bands caused by amorphous C in the a-C films. 相似文献
109.
Mingzai Wu 《Materials Research Bulletin》2004,39(12):1875-1880
Magnetite/silica nanocomposite was synthesized by a facile solvothermal processing at 150 °C for about 10 h. X-ray diffraction (XRD) analysis revealed the effect of annealing on the crystallinity of silica. Transmission electron microscopy (TEM) images showed the good dispersion of magnetite in the silica matrix. Magnetic properties of the nanocomposite were characterized by vibration sample magnetometer (VSM), and the enhanced coercivity was explained by the intrinsic anisotropy of the particles enhanced by the interparticle dipolar fields. 相似文献
110.
John E. Sohn 《The Journal of Adhesion》1985,19(1):15-27
Enhanced matrix-filler adhesion is realized after filler treatment with a surface treatment process. The hydrosol/coupling agent treatment was applied to a wide range of inorganic and organic fillers, and adhesion to a variety of matrix resins was improved. Scanning Electron Microscopy (SEM) was used to determine the locus of failure in the filled systems. The locus of failure shows the relative degree of adhesion between the filler and the polymer matrix. Significant improvement in adhesion in humid environments is also observed. 相似文献