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191.
本文用气相色谱技术研究氯化聚乙烯(CPE)-接枝(g)-氯乙烯(VC)聚合动力学,对不同引发剂体系分析热负荷分布,并对7 m~3聚合釜传热面进行校核。 相似文献
192.
大压差减温减压是能的严重贬值。根据公司供热现状,分析了热电联产的可行性,利用蒸汽余压发电后,再供生产系统各热用户,这样既节约了能源又缓解了集团公司用电紧张的局面,而且有相当可观的经济效益。 相似文献
193.
In this paper, we develop the Contoured Robust Controller Bode (CRCBode) plot and demonstrate its use in the design of robust controllers for nonlinear single‐input single‐output (SISO) systems. The CRCBode plot shows contours (level sets) of a robust performance quantity on the Bode magnitude and phase plots of the controller. An iterative frequency domain loop‐shaping design approach is employed to eliminate all intersections of the controller frequency response with certain ‘forbidden regions,’ indicating that a standard SISO robust stability and performance criterion is satisfied. Nonlinearities are accounted for by avoiding the maximum forbidden regions over a structured uncertainty set consisting of linearizations of the system dynamics about several operating points. We demonstrate this technique by designing and experimentally verifying a flow‐rate controller for a butterfly‐valve based liquid cooling system, which is robust to valve nonlinearities and flow disturbances. Finally, we compare this compensator with one generated using an automated H ∞ synthesis algorithm and discuss the advantages of the CRCBode approach. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
194.
Behavioral evidence indicates that (Z)-9-hexadecenal (Z9-16ALD) is a trail pheromone component ofIridomyrmex humilis, and that the true trail pheromone may be multicomponent. Trail-following responses ofI. humilis workers to several concentrations of syntheticZ9-16ALD, a constituent of the Pavan's gland, were found to be comparable to responses to gaster extract trails containing ca. 100 times lessZ9-16ALD. Of the five aldehyde analogs tested, only (Z)-7-hexadecenal (Z7-16ALD) elicited significant trail-following. However, following responses to severalZ9-16ALD-Z7-16ALD combinations were lower than responses toZ9-16ALD alone. Trails on filter paper of biologically relevant concentrations ofZ9-16ALD lose activity within 2 hr in the laboratory. The release rate ofZ9-16ALD measured from filter paper trails was 0.25 ± 0.10 pg/cm-sec. This was used to estimate the trail-following threshold for this compound of Argentine ant workers. 相似文献
195.
A novel and simple growth mark method was developed to make marks during the growth process of carbon nanotube arrays. These marks can be read out under scanning electron microscope or optical microscope. Based on this method, the growth rates at different temperatures and under different acetylene partial pressures were measured, from which the activation energy and the order of reaction were determined. Based on our experimental results, the growth of carbon nanotube arrays in our experimental condition could not be diffusion-limited. The measured activation energy could possibly be attributed to the heterogeneous decomposition of acetylene over the catalyst particle. Furthermore the marked array with special segmental structure may be found some applications in the future. 相似文献
196.
Emulsion polymer isocyanate (
), polyvinyl acetate (
) and resorcinol-formaldehyde (
) adhesives were used to produce single lap shear specimens using resinous and non-resinous apitong (Dipterocarpus spp.) timbers. Tests showed that joints made with highly resinous apitong were about 40% weaker than similar joints made with non-resinous apitong. The resinous apitong was treated with different solvents to yield five different extractives which were characterized by infra-red analysis. Apitong extractives were then added to
and
adhesives and joints made with buna (Fagus crenata), a timber known to be low in extractives and easy to bond. Joints prepared using extractive-containing adhesives were generally weaker than those made with the unmodified adhesives. RF adhesives containing extractives cured more slowly than unmodified
. It is thought that the acidic nature of the extractives changes the pH of the system sufficiently to affect the curing mechanism 相似文献
197.
The structure of benzoxazines is similar to that of phenolic resin through thermal self‐curing of the heterocyclic ring opening reaction that neither requires catalyst nor releases any condensation byproduct. These polybenzoxazine resins have several outstanding properties such as high thermal stability and high glass transition temperature. To better understand the curing kinetics of this copolybenzoxazine thermosetting resin, dynamic and isothermal differential scanning calorimetry measurements were performed. Three models, the Kissinger method, the Flynn–Wall–Osawa method, and the Kamal method, were used to describe the curing process. Dynamic kinetic activation energies based on Kissinger and Flynn–Wall–Osawa methods are 72.11 and 84.06 KJ/mol, respectively. The Kamal method based on an autocatalytic model results in a total order of reaction between 2.66 and 3.03, depending on curing temperature. Its activation energy and Arrhenius preexponential are 50.3 KJ/mol and 7959, respectively. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 95: 730–737, 2005 相似文献
198.
An optimization strategy has been applied to describe the chemical composition at the furnace bottom in the Kraft recovery boiler of a pulp production process. The concentrations of each involved chemical species were calculated through an optimization approach, minimizing the Gibbs free energy of the system. Various systems were proposed and tested, assuming different chemical species and phases number. Because serious initialization problems were found at this stage for some of the proposed systems, an optimization heuristic method (PSO) was used for the first approach to the problem. Once the appropriate phases number and chemical species in the system were determined, the initialization problems disappeared and the use of a deterministic optimization method (SQP) became viable. The proposed approach has shown to be satisfactory to reproduce industrial data and also data reported in the open scientific literature. 相似文献
199.
200.