Investigation of the stability of tablets prepared from sucrose and citric acid anhydride utilizing response surface methodology

Inversion of sucrose is a stability problem particularly of candies with acidic taste that contain sucrose and small amounts of organic acids such as citric acid, since the free d-fructose produced by hydrolysis is hygroscopic. The following possibilities were investigated for preventing the hydrolysis of sucrose in tablets containing sucrose and citric acid: Adding various amounts of tri-sodium citrate to the formulation to neutralize the citric acid, (Hot) melt coating of citric acid and tri-sodium citrate with a vegetable fat at different coating ratios, variation of the ratio of coated citric acid and tri-sodium citrate in formulations, and compressing the formulations with different compression forces. After tablet processing and storage of tablets, the concentration of d-fructose was determined on the basis of enzymatic reactions. A response surface central composite design was used. The above-mentioned variations were chosen as independent variables and the amount of d-fructose was chosen as response variable. The lowest rates of inversion could be achieved by increasing the content of tri-sodium citrate and the ratio of coating material and decreasing the ratio of coated citric acid and tri-sodium citrate in the tablet formulations. The compression force had no significant effect on the inversion of sucrose.     

灰熔聚粉煤气化炉存在的问题及改进

对灰熔聚粉煤气化炉运行中存在的问题进行了分析、讨论，并提出了解决方案和建议。     

塔河油田三叠系水平井地质导向技术研究

针对塔河油田三叠系碎屑岩油气藏油层薄、储集层非均质性较强、泥质和低渗致密夹层纵横向变化大的地质特点，在分析、研究不同区块多口水平井资料的基础上，探讨了水平井不同地质情况下斜井段及目的层砂顶的预测和判别技术，以实例阐述了井眼轨迹调整方法，首次形成了一套适合于该地区碎屑岩非均质薄层油气藏水平井录井地质导向技术，在塔河油田水平井钻探开发中取得了显著的成效。     

Kinetics of phenol oxidation in a trickle bed reactor over active carbon catalyst

The wet air oxidation of phenol over a commercial active carbon catalyst was studied in a trickle bed reactor (TBR) in the temperature and oxygen partial pressure ranges of 120–160 °C and 0.1–0.2 MPa, respectively. The performance of the active carbon was compared in terms of phenol and COD destruction. The weight change of active carbon due to reaction was also measured. Finally, oxic phenol adsorption isotherms were assessed in batch conditions at 25, 125 and 160 °C. In order to use the conversion data obtained from the TBR for a kinetic study, special care was taken to check the kinetic control in the TBR experiments. Several kinetic models including power law or Langmuir–Hinshelwood expressions were considered to describe the catalytic oxidation of phenol over active carbon. The simple power law model with first order dependence on both phenol and oxygen concentration predicted satisfactorily the experimental data not only over the entire range of operating conditions studied, but also outside its validity range. Copyright © 2005 Society of Chemical Industry     

一种新型卷绕方式CPW介绍及应用

主要介绍了德国ＮＥＵＭＡＧ公司开发的新型高速卷统方式ＣＰＷ（致密精密卷绕）的工艺技术特点，并对引进和应用该设备技术的生产情况及其产品质量做了对比分析．     

高水位地基处理实例

介绍高水位(距槽底300)条件下,地基处理的方法、检测及效果验证。为在此条件下进行施工作业提供依据。     

南方沙地开发利用途径的探讨

根据南方风沙化地自然及气候的特点，提出并讨论了在风沙化土地区营造防风固沙林；建立沙地果业基地；发展沙区畜牧水产业；搞好沙地蔬菜生产；完善农防林体系建设，发展沙区工业等开发利用模式。     

气固流化床中非线性特性的多尺度分析

Deterministic chaos theory offers useful quantitative tools to characterize the non-linear dynamic behavior of a fluidized bed and the developed complexity theory presents a new approach to evaluate finite sequences. In this paper,the non-linear,hydrodynamic behavior of the pressure flutuation signals in a reactor was discussed by chaos parameters and complexity measures.Coherent results were achieved by our multi-scale analysis,which further exposed the behavior in a gas-solid two-phase system.     

低压组合床重整工艺工业试验

介绍了国产500kt／a低压组合床催化重整装置首次在中国石化股份有限公司长岭分公司的工业试验情况。近两年的运转及标定结果表明试验是成功的，该技术达到了国外连续重整技术第一代与第二代之间的水平，并且投资小，适于小型固定床重整装置的改造。