Synthesis and characterization of poly(ethylene aspartate)-metal complexes

Poly(ethylene aspartate) [PEA] was synthesized by the melt condensation of D,L-aspartic acid and ethylene glycol. PEA containing pendent amino and carbonyl groups in its repeating chain was used as the polymeric ligand for complexation with transition metal ions, viz. Co(II), Ni(II), Cu(II), Mn(II), Zn(II), Cd(II), Ca(II), Mg(II), Pb(II) and Hg(II). Complexation was found to be most effective in DMSO. The resulting polyester-metal complexes were solid coloured materials which have been characterized by IR spectroscopy, elemental analysis and magnetic susceptibility measurements. The thermal stability of the polyester-metal complexes was investigated by thermogravimetric analysis (TGA). On the basis of the physico-chemical studies, an oxygen and nitrogen coordinated structure for the polyester-metal complexes is proposed.     

Makespan estimation and order acceptance in batch process industries when processing times are uncertain

Batch process industries are characterized by complex precedence relationships between operations, which renders the estimation of an acceptable workload very difficult. A detailed schedule based model can be used for this purpose, but for large problems this may require a prohibitive large amount of computation time. We propose a regression based model to estimate the makespan of a set of jobs. We extend earlier work based on deterministic processing times by considering Erlang-distributed processing times in our model. This regression-based model is used to support customer order acceptance. Three order acceptance policies are compared by means of simulation experiments: a scheduling policy, a workload policy and a regression policy. The results indicate that the performance of the regression policy can compete with the performance of the scheduling policy in situations with high variety in the job mix and high uncertainty in the processing times. Correspondence to: C.V. Ivanescu     

柴油机低频排气噪声规律分析

针对柴油机（4－85）低频排气噪声，对其产生机理、规律及其影响因素等作了理论计算、分析及实验。对低频排气噪声信号进行频域分析后可知，其主要由一系列离散的谐波组成，是以柴油机点火频率为基频的一种类周期性噪声，有可能应用有源噪声控制技术。     

Cluster analysis in industrial market segmentation through artificial neural network

Market segmentation has commonly applied cluster analysis. This study intends to make the comparison of conventional two-stage method with proposed two-stage method through the simulated data. The proposed two-stage method is the combination of self-organizing feature maps and K-means method. The simulation results show that the proposed scheme is better than the conventional two-stage method based on the rate of misclassification.     

产量递减规律的诊断方法

传统的Arps产量递减分析方法要求事先选定递减规律的初始时间、初始产量及初始递减率,事实上这些参数是很难确定的。实际应用时不得不人为地加以臆断而使得此方法带有不确定性.为此提出了产量递减规律的诊断方法。应用诊断曲线很容易确定递减规律的模型参数,克服常规方法的不足。通过选用参考时间、参考产量和参考递减率,使得递减分析方法具有一定的灵活性和优越性、该方法简便、实用。     

盖层封闭能力的灰聚类评价方法

提出灰聚类评价方法，用于盖层封闭能力定量评价。所有被评价对象构成聚类对象集，所有评价指标构成评价指标集，所划分的盖层封闭能力等级构成聚类的灰类集，按照最大聚类权确定对象所属的灰类，即盖层的封闭能力级别。评价流程是：确定指标灰类模式→数据预处理→利用聚类公式计算→利用最大聚类权准则抉择。这种方法避免了加法评分法要依靠人的主观经验划定总评分值的问题，而且由于把评价对象视为“灰”的，具有处理边缘信息的能力。以琼东南盆地３个主要探区的盖层封闭性评价为例，介绍了灰聚类评价的具体应用方法。灰聚类评价方法同样可用于储集层评价、圈闭评价等地质问题的定量研究。表２参３（王孝陵摘     

起重机吊钩拖动绕线电动机他励双高调速系统

本文提出励磁电流可自动控制的他励式双高调速系统设计方案。系统在提升特别是在下放重物时，具有较硬的机械性；在负载１０－１００％的变化范围内，可实现最大偏差Δｎｍａｘ／ｎｍｉｎ１００％≤１０％，调速范围Ｄ≥１０；在满载运行条件下，可节约电能８０％以上。     

变井储系数的确定方法及其在反褶积分析中的应用

中针对变井储试井分析问题，给出了确定变井储系数及计算续流量的方法，并用反褶积分析积分析方法解释了未出现径向流的早期测压数据，给出了解决早期试井资料分析问题的有效方法。     

苯基荧光酮类试剂在金属及合金光度分析中应用新进展

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