Studies on the interactions of metal oxides and Na2 SO4 at 1100 and 1200 K in oxygen

The interaction of different metal oxides such as Co₃O₄, NiO, Al₂O₃, Cr₂O₃, Fe₂O₃ and SiO₂ with Na₂SO₄ at a temperature of 1100 and 1200 K in flowing oxygen has been studied. The thermogravimetric studies for each system were carried out as a function of Na₂SO₄ in the mixture. The presence of different constituents in the reaction products were identified by X-ray diffraction analysis and the morphologies of the reaction products were characterized using metallography and scanning electron microscopy (SEM). The formation of products was also investigated by thermodynamic computation of free energies of the reactions and the study of relevant equilibrium phase diagrams. The soluble species in the aqueous solutions of the reaction products were determined quantitatively using atomic absorption spectrophotometry. The high temperature interaction products usually contain a 3-phase structure namely, Na₂O·M₂O _x , M₂O _x and metal sulphide and/or metal sulphate. The formation of Na₂O·M₂O _x depends upon the solid state solubility of metal oxide in the molten salt at high temperatures. Under limited solubility conditions Na₂O·M₂O _x is invariably formed, but as soon as this condition is relaxed the oxide. M₂O _x , precipitates and forms a separate phase.     

Recrystallization/precipitation behaviour in microalloyed steels

Microalloyed high-strength low-alloy (HSLA) steels contain additions of Nb, V, Ti, or in combination, in amounts of 0.01 to 0.1 weight percent to improve mechanical properties, which are strongly dependent on the thermomechanical interaction taking place in the course of rolling mill processes. The recrystallizatian of hat-twisted austenite has been investigated in a cylindrical specimen (f 6×50 mm) machined from hat rolled plates of 0,052 wt % Niobium microalloyed steel. Continuous and interrupted torsion test were carried out in the temperature range 1123 K to 1173 K after a solution treatment of 1.5 minutes at 1423 K and torque-twist data were analysed. The various methods were discussed for obtaining results from torsion tests. The effect of precipitation kinetics was appreciated by way of connection t_p/t_p(red), where t_p is the experimental measured time for the peak stress and t_p(red) is the newly defined reduced time. The softening ratio X and time t_0.05R for start of static recrystallization were established.

The correlation between precipitation and recrystallization is presented as a graphs for chosen requirements (temperature of austenitization, carbon and niobium content and strain rate). If temperature goes below 850°C, the restoration processes are hardly suppressed, both are limited by diffusion and Nb(CN) precipitation, which are extended dynamically in the range of strains rates 10⁻² to 1 s⁻¹.

In the present paper, an attempt is made to derive the PRTT diagram and to define all mathematical equations for describing recrystallization times t_0.05R, t_0.5R, t_0.95R and t_0.05P for the start of precipitation. In real metal forming processes such as the hot rolling of plates or strips the knowledge of these parameters and results is extremely important for the the correct microstructure and sheet quality to be obtained.     

Strain analysis of moving objects using a Fourier transform grid method

There is no good method to measure the shape and the strain distributions of a structure changing with time. We have previously proposed the Fourier transform grid method (FTGM) to measure the three-dimensional shape and surface strain distributions of stationary objects by analysing the two-dimensional grating images recorded with two cameras. In the stereoscopic method, it is very important to determine the accurate geometric parameters of the camera system. In this paper, the positions and the directions of cameras are accurately determined using the FTGM applied to images of a reference object on which a two-dimensional grating is drawn. Applications for analysing shape and strain distributions of vibrating rubber plates and a moving human skin are shown.     

一种简便的评定引战配合效率方法

在导弹近炸引信起爆延时具有随机性基础上，本文建立了一种用延时及其数学特征表示的评定引战配合效率的简便方法，并对有关应用问题进行了讨论。     

长输管道建设物流管理新模式——物资配送

长输管道工程是以线路管道与沿途站场为主要内容的建设工程,其物资配送有着不同于一般物流管理的特点,点多线长,且交通不便.文章结合西南成品油管道建设工程的物资配送实践,总结出长输管道物资配送的类型,并从机构设置、计划编制、台账和报表管理等方面介绍了物资配送的管理内容及经验,实践证明,这种物资配送方法不但使业主的物资管理人员大为减少,而且使长输管道工程的物资供应更加及时有序.     

压裂泵往复密封性能及机理研究

根据流体动压润滑理论，对压裂泵柱塞密封摩擦副的润滑机理进行了理论分析。在排出和吸入行程，柱塞密封摩擦副均能满足流体动压润滑的条件，即在柱塞与密封界面上能形成并保持一定厚度的油膜润滑密封，从而达到减小摩擦提高寿命的目的；建立了摩擦界面油膜厚度和泄漏量的计算公式。利用有限元法理论，对密封圈的压力沿轴向的分布规律、泄漏量与压力变化关系进行了模拟计算。对往复密封圈沿轴向压力分布、泄漏量随压力变化进行了测试；试验结果表明，建立的计算模型具有较高的计算精度，揭示了压裂泵的密封机理。     

新疆重质混合原油研制高等级道路沥青

对利用新疆重质混合原油生产的减压渣油作为基质沥青制备高等级道路沥青进行了研究。考察了低硫石蜡基原油（A）和含硫环烷-中间基原油（B）的掺炼比对基质沥青四组分组成的影响，减压渣油软化点与基质沥青四组分组成的关系，以及添加剂对改进沥青性质的作用。由此得出原油（B）的合适掺炼量，减压渣油软化点的控制范围和优化的生产工艺条件，调合出了符合GB／T18150—2000和JTGF40—2004要求的高等级道路沥青。     

准噶尔盆地腹部超压层分布研究

准噶尔盆地腹部普遍发育深层（大于4000m）超压系统，很多钻井都钻遇超压。通过对超压段钻井、地质、测井、地震特征系统研究发现，超压段泥浆密度大幅增加，具有高声波时差、低电阻率以及地震低速的超压响应特征。利用Dix公式计算地震层速度和利用Fillippone公式计算地层压力，得到超压数据体。准噶尔盆地腹部超压在白垩系及其以下沉积地层中均有分布，超压层的深度范围不同。分1井西凹陷边缘以及昌吉凹陷西南有空层现象。超压顶面分布的层位由北往南、从东到西逐渐变浅，从三叠系顶部到白垩系底部。深部超压对油气分布和富集有着重要的控制作用，准噶尔盆地腹部超压层分布的研究将对本区油气勘探起积极的推动作用。