Effect of Twin-Plane Reentrant Edge on the Coarsening Behavior of Barium Titanate Grains

When BaTiO₃ ceramics were sintered at relatively low temperatures (≤1250°C), the grains with reentrant edges caused by a (111) double twin grew exclusively. As a result, a microstructure with a bimodal grain-size distribution composed of platelike large grains and fine matrix grains was obtained. In contrast, at the usual sintering temperature between 1250° and 1350°C, grains containing a (111) double twin did not exhibit any growth advantage. In this case, a coarse and uniform microstructure was obtained. When this coarse-grained specimen was further heat-treated at 1365°C, the grains possessing a double twin were observed to grow exclusively again. The results were explained in terms of a coarsening process controlled by two-dimensional nucleation.     

A203型低温氨合成催化剂使用小结

对Ａ２０３型低温氨合成催化剂的使用进行总结，介绍了该催化剂的装填，升温还原情况及使用效果。     

Compressibility of the polymer crystal

Results for the compressibilities of a wide range of polymer crystals along the fibre- and the transverse crystal axes are presented. Good agreement is found between the theoretical and the experimental results of different authors.     

高效防腐中温磷化液LC-1的制备及性能

制备了一种含Zn2+、Mn2+、N i2+三系离子的LC-1磷化液,通过硫酸铜点滴、氯化钠浸蚀、SEM等手段对磷化膜进行了测试,测定了磷化温度、磷化时间对膜层耐蚀性的影响。结果表明,在磷化温度大于65℃,磷化时间大于10 m in的条件下,所形成的磷化膜结晶均匀、致密、黑褐色,耐蚀性良好。LC-1三系磷化液可适用于大批量钢铁工件的磷化生产。     

15%田草灵高效液相色谱分析

采用Ｎｏｖａ－Ｐａｋ Ｃ１８不锈钢色谱柱进行反相液相色谱分析，以甲醇：水＝６５：３５（Ｖ／Ｖ）为注动相，以邻苯二甲醇二乙酯为内标物，用内标法测定田草灵除草剂中苄嘧黄隆和异丙甲草胺的含量，结果表明，各有效成分与内标物色谱峰分离完全，杂质无干扰，测定结果，苄嘧黄隆和异丙甲草胺的变异系数分别为０．７４％和１．０７％，回收率分别为９９．４％￣１００．８％和９９．１％￣１０１．３％。     

Bubble temperature data for phenol-alcohol systems: Phenol-I-Amyl alcohol and phenol-n-Amyl alcohol systems

In order to supplement the literature data on VLE, isobaric bubble temperature data were collected for the binary systems phenol-i-amyl alcohol and phenol-n-amyl alcohol over the entire composition range by indirect method using a standard Swietoslawski type ebulliometer. The measurements were made at three sub-atmospheric pressures. The experimental t-x data were correlated with both equation of state method and gamma-phi methods. In the former approach, the Soave equation of state is used, whereas in the latter case Wilson, NRTL and UNIQUAC equations are used.     

高支模施工安全管理问题与对策

高支模工程安全管理不仅需要很高的技术,而且安全管理本身也具有较大的随机性,这就导致相关人员在开展安全管理工作时具有一定的难度。面对这一问题,相关监理人员必须从施工方案的审批、应急预案的落实、质量安全作业的施工技术交底和施工过程中所需要的各种原材料进场前的检验等方面加强管理。     

A New Derivation of the Cubature Kalman Filters

This paper investigates the cubature Kalman filtering (CKF) for nonlinear dynamic systems. This third‐degree rule based filter employs a spherical‐radial cubature rule to numerically compute the integrals encountered in nonlinear filtering problems, thereby removing the requirements of explicitly computing the Jacobians. The cubature rule, however, requires computing the intractable integrals over a high‐dimensional spherical region for multidimensional applications. Moreover, the cubature formula that has been used to construct the spherical cubature formula has some demerits, most notably its inconvenient properties in computation and low estimation accuracy. Aimed at these issues, a general class of CKFs that uses only cubature rules is derived in this paper. It can be shown that the conventional CKF is a special case of the proposed algorithm. The paper also includes higher‐degree CKFs, especially two representative types of the fifth‐degree CKFs. Performance of the proposed algorithms is demonstrated via two target tracking problems. The experimental results, presented herein, illustrate the superior performance of higher‐degree CKFs to conventional nonlinear filters.     

基于APIC的高精度定时器设计

在操作系统开发过程中需要一定精度的计时器支持。在Windows实时扩展改造过程中,针对原有定时精度低和波动较大的问题,提出一种基于高级可编程中断控制器(APIC)的高精度定时器设计方案。利用CPU片上结构APIC的计数寄存器编程,构建高精度时钟。运用内核驱动建立内核调度管理,通过内存映射提高用户态到内核态的数据传输速度,保证实时性能。利用DLL提供一组和内核交互的定时器接口供用户使用。实验结果表明,该方案有效解决了定时精度和稳定性问题,构造的定时器性能稳定,具有良好的实用性。     

基于模糊PID大型电力机组温度过热控制

随着高精密技术的发展,高精度、超高精度的温控系统越来越多被人们运用于大型电力机组中。传统的温度控制系统对各异的真实系统适配性较差,不能保证系统性能,适应性较差。针对这些问题,提出了一种模糊自适应PID大型电力机组温度过热控制算法,即专家-模糊PID控制器方法,根据温度偏差选择采用专家控制还是模糊PID控制,克服适应性差的问题。用专家控制避免设定值震荡,并通过模糊PID温度控制较快达到设定初始目标温度值,并稳定在该值上。最后通过仿真实验证明这种模糊PID超精度温度控制系统对于大型电力机组的温度过热控制问题具有控制精度高、响应速度快、温度波动小等优点。