The effect of sparger geometry on gas holdup and regime transition points in a bubble column equipped with perforated plate spargers

This paper investigates the effect of sparger geometry on flow regime of a bubble column. The experiments presented in this study were performed under atmospheric pressure with water/air in a cylindrical Plexiglas^® column of 33.0 cm i.d. and 3.0 m height. Three different perforated plate spargers were employed. Hole diameter was varied in the range of 1–3 mm, while the free area was 1.0%.The theory of linear stability is used for the prediction of regime transitions in the bubble column and a comparison has been presented between the predictions and the experimental observations. A good agreement between the predictions and the experimental values of transition gas holdup has been obtained.In addition, the data from the literature has been analyzed. Experimental values of transition gas holdups and predictions by the theory of linear stability have been compared with those of literature.A correlation based on dimensionless numbers (Archimedes, Froude, Eötvös and Weber) and the group (d_o/D_C) for the prediction of gas holdup in homogeneous regime is proposed. The average error between the correlation predictions and experimental values remains under ±10%.The proposed correlation is compared with the published data and found to be in fairly good agreement.     

Characterization of dynamic behavior of a spout-fluid bed with Shannon entropy analysis

Differential pressure fluctuation time series were obtained at different locations in a two-dimensional spout-fluid bed with a cross section of 300 × 30 mm and height 2000 mm. Shannon entropy analysis of differential pressure fluctuations was developed to characterize the dynamic behavior. Effects of two important operating parameters (spouting gas velocity and fluidizing gas flow rate) on the Shannon entropy were examined. It was demonstrated that a spout-fluid bed at a high spouting gas velocity or fluidizing gas flow rate was a deterministic chaos system since the Shannon entropies at all bed locations increased sharply and asymmetric unstable flows occurred. Shannon entropies were found to be significantly different at various bed locations. Shannon entropies of different flow regimes were distinct, so they were used to identify the flow regimes. The results show that the Shannon entropy helps to grasp the complex characteristics of dynamic behavior in spout-fluid beds.     

Hydrodynamics of three-phase fluidized bed systems examined by statistical, fractal, chaos and wavelet analysis methods

Hydrodynamic studies were conducted in gas-liquid-solid systems (0.1 m ID, 2 m high) of 3.0 mm glass beads and of 2.1 mm polypropylene low-density particles, with particles densities of 2471 and 1290 kg/m³, respectively. Simultaneous measurement of differential pressure and bubble conductivity probe signals sampled at 500 Hz for 60 s enabled the investigation of the change in flow structure in relation to the flow regime transitions. Superficial gas velocities ranged between 0.010 and 0.052 m/s for polypropylene particles, and extended to 0.12 m/s for glass beads, while the superficial liquid velocities covered the ranges of 0.0007-0.045 m/s for polypropylene particles, and ranged up to 0.056 m/s for glass beads.Spectral analysis of the pressure fluctuations revealed a transition from dispersed to coalesced bubbling flow with decreasing liquid velocity for a given superficial gas velocity. The use of a conductivity probe facilitated characterization of the local flow structure in terms of bubble movement. The measurements were extensively analyzed using fractals and chaos, power spectra frequency analysis and wavelet decomposition in addition to the standard statistical analyses. The coefficient of variation of the bubble probe signals was found to be the most effective in deducing the transition velocity between coalesced and dispersed bubbling flow regimes, while wavelet energy confirmed the similarity in the distribution between two axial positions once operated in the dispersed flow regime. Comparison of the flow structure between glass beads and polypropylene particles showed that both the minimum liquid fluidization velocity and the transition velocity between the bubble flow regimes were much higher for the glass beads than for the lighter polypropylene particles. Furthermore, the standard deviations of the decomposed bubble probe signals through wavelet transformation successfully highlighted the difference between the two systems of particles.     

Fluidization with hot compressed water in micro-reactors

In this paper the concept of micro-fluidized beds is introduced. A cylindrical quartz reactor with an internal diameter of only 1 mm is used for process conditions up to and 244 bar. In this way, fast, safe, and inherently cheap experimentation is provided. The process that prompted the present work on miniaturization is gasification of biomass and waste streams in hot compressed water (SCWG). Therefore, water is used as fluidizing agent. Properties of the micro-fluid bed such as the minimum fluidization velocity (U_mf), the minimum bubbling velocity (U_mb), bed expansion, and identification of the fluidization regime are investigated by visual inspection. It is shown that the micro-fluid bed requires a minimum of twelve particles per reactor diameter in order to mimic homogeneous fluidization at large scale. It is not possible to create bubbling fluidization in the cylindrical micro-fluid beds used. Instead, slugging fluidization is observed for aggregative conditions. Conical shaped micro-reactors are proposed for improved simulation of the bubbling regime. Measured values of U_mf and U_mb are compared with predictions of dedicated 2D and 3D discrete particle models (DPM) and (semi)-empirical relations. The agreement between the measurements and the model predictions is good and the model supports the concept and development of micro-fluid beds.     

Flow Regime Maps for Flow of Liquid Through Downcomer in a Turbulent Bed Contactor

The provision of a downcomer to classical turbulent bed Contactor (TBC) increases the gas treating capacity of the equipment. When the downcomer is provided, it is expected that all the liquid passes through the downcomer only without any liquid flow through the distributor. In the present study, the operational regime for the flow of liquid only through the downcomer is experimentally evaluated for various geometric parameters and particle characteristics. It is observed that the preferred operational regime without dumping and weeping increases with an increase in Archimedes number and downcomer diameter, and decreases with an increase in static bed height and downcomer weir height. Correlations are proposed to satisfactorily predict experimentally observed operational regime.     

Enhanced structural,electromagnetic and absorption features of CoSm ferrite-metamaterial absorbers through synergistic effects

Currently, materials with outstanding absorption abilities, such as thin size, better absorbing power, and light weight are the need of industry to resolve the electromagnetic issues. However, the research on optimizing the composition of the material, microstructure and the structure of the absorber are also the important factors for enhancing the absorption features. A metamaterial microwave absorber (MMA) based on nano ferrites with desirable absorption peaks is proposed and simulated. Sol-gel auto combustion route is used to prepare the nanosized Sm doped Co ferrite with Co_1+xSm_xFe_2-2xO₄ at x = 0.00, 0.03, 0.06, 0.09, respectively. XRD, VSM, FESEM, and VNA were employed to evaluate the structural, magnetic, morphological, and dielectric features. Rietveld refinement of the XRD patterns of samples was evaluated. Refined parameters show the spinel phase's emergence and the Fe₂O₃ phase. Grain size and crystallite size were increased with Sm doping in Co ferrite. Electromagnetic studies depicted that the highest dielectric constant value was found at x = 0.09 and the minimum value at x = 0.03, respectively. Sm doped Co ferrite at x = 0.09 depicted high Q values at higher frequencies. The coercivity values first decreased and then increased. All samples exhibit variations in coercivity and magneto-crystalline anisotropy constant. This variation was attributed to the super-exchange interactions and strong LS coupling of the cations. The multiple absorption peaks are attained for TE-polarization, and the absorptivity is considerably improved for x = 0.09. The proposed absorber simulated from CST depicted the absorption peaks of the S-band and C-band of the microwave regime. The synergistic effects among the metamaterial and ferrite layers may enhance the absorption feature and would be useful for satellite communication applications.     

基于反传神经网络和压差波动识别气液两相流流型

引　言研究气液两相流流型自动与客观识别具有重要的工程应用价值 ,可为相关工业中两相流动自动监测与控制提供技术保障 .因此 ,该课题一直受学术界和工业界的重视 .近年来 ,随着测量技术和信息处理技术的发展 ,为气液两相流型的客观和智能识别提供了可能[1] .目前有关流型的神经网络模式识别的研究工作正在进行 .Ｅｍｂｒｅｃｈｓ等[2 ] 采用Ｋｏｈｏｎｅｎ神经网络模型 ,分别将压差波动信号的短时Ｆｏｕｒｉｅｒ谱和正交小波变换后的小波系数作为网络的输入特征 ,对水平管内的两相流流型进行识别 .结果发现Ｆｏｕｒｉｅｒ谱作为输入特征参…     

管道内流体流动型态的简便判断方法初探

以流体流动方程为基础,以流体运动粘度和管内壁的绝对粗糙度为基本参数,导出了一组判断牛顿型流体在圆管内流动型态的简便关系式。     

液体黏度对气液固逆流三相湍动床动力学行为的影响

引　言逆流三相湍动床 (ITPTB) 仅由向上的气体来实现反应器的流化状态[1] 这类反应器因其独特的优点, 近几年受到人们极大关注并应用于催化过程、生物化工及环境工程领域[2]. 如在生物废水处Table 1　Physical properties of three phases and operation conditionsPhasesPhys     

干冰清洗技术的应用

干冰清洗是一种崭新的清洗技术,它干式、无毒、无磨损、无二次污染的清洗特点使其在目前的清洗市场中占有一定的市场份额.它在工业和民用的应用领域正在不断扩大,通过对干冰清洗的应用实例以及干冰清洗优势的阐述使人们对干冰清洗有更深的了解.