棉铃宝高效液相色谱分析方法研究

本法采用同一色谱条件反相高效液相色谱法测定棉铃宝中甲基对硫磷和辛硫磷的含量，方法简单易行，具有较高的精密度和准确度，其回收率分析为甲基对硫磷９９．５９％，辛硫磷１０１．０％。     

结晶器液面自动控制系统在唐钢板坯连铸机的应用

介绍了涡流法和同位素法2种结晶器钢水液面自动控制检测方式,及其在唐钢板坯连铸机的应用.     

板坯连铸涡流检测钢水液位系统的应用

介绍了新一代RAM型涡流传感钢水液位控制仪在莱钢板坯连铸机上的应用及其效果。     

The concept of an endurance limit for adhesive joints

The effect of cyclic stressing on the strength of single lap adhesive joints has been studied and a considerable reduction in strength observed when the maximum stress exceeds about 40% of the ultimate tensile strength, but whether or not a true endurance limit exists is not proven. Fallacies are shown in some of the techniques which have been proposed for studying the fatigue behaviour of adhesive joints.     

Development of a Magnetic Suspension Densimeter and Measurement of the Density of Toluene

The development of a magnetic suspension densimeter that has been built for measurement of the density of compressed liquid at pressures up to 30 MPa in the temperature range 20 to 150°C is described. The densimeter was first built by the author and his coworkers at NIST. We describe here further improvements made on a second system built at NMIJ based on the same principle. The densimeter uses a small coil suspended from an electronic balance. Within the coil is placed a sample cell in which the pressurized sample and a buoy, which is a permanent magnet, are enclosed. For measurement of density, balance readings are recorded (1) with the buoy at rest and (2) with the buoy in magnetic suspension. The measurement procedure is basically a hydrostatic weighing, which is simpler than those of conventional magnetic densimetry. As an example, measurements of toluene density performed as part of an inter-laboratory comparison are presented. The data agreed with reliable literature values to within a few hundredths of a per cent.     

Limit Cycles in a Class of Hybrid Dynamical Systems

This paper deals with qualitative analysis of the so-called switched fluid networks. Such networks are used to model communication, computer, and flexible manufacturing systems. We prove that for any deterministic network from a specific class, there exists a finite number of limit cycles attracting all the trajectories of the system. Furthermore, we determine this number. Date received: March 11, 2000. Date revised: January 19, 2001.     

Lower bound limit analysis using non‐linear programming

This paper describes a new formulation, based on linear finite elements and non‐linear programming, for computing rigorous lower bounds in 1, 2 and 3 dimensions. The resulting optimization problem is typically very large and highly sparse and is solved using a fast quasi‐Newton method whose iteration count is largely independent of the mesh refinement. For two‐dimensional applications, the new formulation is shown to be vastly superior to an equivalent formulation that is based on a linearized yield surface and linear programming. Although it has been developed primarily for geotechnical applications, the method can be used for a wide range of plasticity problems including those with inhomogeneous materials, complex loading, and complicated geometry. Copyright © 2002 John Wiley & Sons, Ltd.     

竖直狭缝通道中液氮沸腾强化换热的实验研究

实验表明，狭缝间隙对液氮自然对流核态沸腾换热有明显的影响，在低热流密度下，间隙小的狭缝沸腾换热比间隙大的狭缝明显增强，当狭缝间隙小于实验压力下气泡的脱离直径时，对于同样的热流密度，传热温差减小一个数量级以上，沸腾换热系数提高十几倍到二十倍以上，当热流密度增加一定程度（＞4W/cm^2)时，间隙小的狭缝沸腾换热比间隙大的狭缝有所减弱。     

刚性棒状全芳香液晶聚酯的合成及性质的研究

以溴和苯基取代的对苯二甲酰氯及2，2′-二甲基联苯-4，4′-二甲酰氯作为单体，分别与甲基、叔丁基、苯基取代的对苯二酚经熔融缩聚反应，合成一类具有刚性棒状结构的全芳香液晶聚酯。聚酯的热性质以TGA、DSC，热台偏光显微镜研究。所有的聚酯均为热致性液晶，它们具有相对较低的转变温度，在普通的有机溶剂中具有较好的溶解性质。     

A limit analysis of nonlinear elastic lateral displacements of thin-walled reinforced and prestressed beams

An incremental iterative process based on direct energy minimization is presented for a limit analysis of nonlinear elastic lateral displacements and twists of reinforced and prestressed beams. Problems encountered with the constitutive relations are discussed and two possible material models are presented.