Phase Composition of Oxide Scales during Reheating in Hot Rolling of Low Carbon Steel

Low carbon steel was oxidized over the temperature range 1000‐1250°C in O₂‐CO₂‐H₂O‐N₂, O₂‐H₂O‐N₂, and O₂‐CO₂‐N₂ gas mixtures. Oxidation times were 12‐120 min. and the scales were 50‐2000 μm thick. The variations of these parameters were chosen to elucidate the phase composition of oxide scales under conditions similar to those of reheating furnaces in hot strip mills, using either thin slab casting or conventional casting and rolling technology. Two types of scales have been observed which are influenced by the furnace atmosphere, oxidation time, and temperature. The first type is a crystalline scale with an irregular outer surface, composed mostly of wustite (FeO), and a negligible amount of magnetite (Fe₃O₄). The second type is the classical three‐layer scale, composed of wustite (FeO), magnetite (Fe₃O₄), and hematite (Fe₂O₃). In general, the experiments showed that an increase in oxidation time decreased the percentage of wustite while the percentages of magnetite and hematite increased. A rise in oxygen concentration in the gas mixture increased the percentages of magnetite and hematite, confirming earlier experimental findings. In water vapour‐free atmospheres O₂‐CO₂‐N₂, the oxide scales had a low percentage of wustite, and high percentage of magnetite and hematite. Carbon dioxide showed a small influence at 1100°C, and a negligible one at 1250°C.     

重油催化裂化装置高温烟气冷却器的改造

对重油催化裂化装置原有的高温烟气冷却器进行改造的情况和改造后的烟冷器的优点进行了详细论述，并对烟冷器改造后带来的经济效益作了简要介绍。     

多量程数据采集记录装置的设计

通常的数据采集与记录装置不易实现多量程测量。通过对标度方程进行分析得知,要改变量程只须改变两个参数——标度因子和量程下限。我们设计了一个使用单片机的多量程数据采集和记录装置,能处理多达256种量程。本文叙述了算法分析、硬件和软件的设计以及该装置的性能指标。     

Effect of temperature on methyl radical generation over Sr/La2O3 catalysts

The role of gas phase CH₃ radicals in the oxidative coupling of CH₄ over 1 wt% Sr/La₂O₃ is supported by the observations that (i) this is a very effective catalyst for the generation of CH₃ · radicals and (ii) the concentration of CH₃ · radicals increases with temperature over the range of 450 °C–800 °C.     

DS18S20在单总线多点测温系统中的应用技巧

DS18S2 0是一种新型的单总线数字温度传感器。该器件在实际应用中 ,如果使用不当不但无法发挥其优势 ,反而会引入不必要的误差 ,文章重点阐述了它的使用技巧和方法     

紫金山金矿低品位资源开发的地质技术研究

介绍了紫金山金矿床赋存的基本特征；重点阐述了生产探矿增加储量．扩大矿床规模，建立低品位矿开发蛭济模型和责源评价软件系统研制等系列地质技术研究与创新成果：强调了加大经济与科技投入．对矿山的发展有重大意义。     

中原高温高盐油藏疏水缔合聚合物凝胶调剖剂研究

针对中原油田高温(>80℃)、高盐度(>50 g/L)、高硬度(>1 g/L)砂岩油藏,研制了地下成胶的高热稳定性聚合物凝胶调剖剂。所用聚合物为疏水缔合聚合物AP-P4,M=9.0×106,HD=27%,疏水基摩尔分数0.2%;交联剂为可生成酚醛树脂的3种化合物;调剖剂胶液用矿化度160 g/L的马寨油田污水配制;实验温度95℃。根据形成的凝胶黏度(95℃,1.1 s-1)确定交联剂各组分用量为:MZ-YL 0.429%,MZ-BE 0.060%,MZ-XS 0.012%;酸度调整剂用量0.12%;成胶时间10~15小时。2.5、3.0、3.5 g/L AP-P4的凝胶在95℃老化100天后黏度保持在~40 Pa.s及以上。初配制胶液在3000 r/min下剪切15分钟后黏度降低87.5%~89.0%,但成胶后和老化过程中凝胶黏度只比未剪切样降低17.1%~6.6%。3.5 g/L AP-P4的调剖剂对~1μm2的6支储层岩心的堵塞率在88.1%~95.8%范围,平均93.3%,造成的残余阻力系数在15.2~28.6范围,平均19.8,使渗透率级差2.3~8.0的4组双人造岩心的注水流量比发生不同程度的反转。认为该凝胶调剖剂高温下稳定性好的原因,是强化学交联密度低,因而凝胶脱水收缩作用弱。图2表5参5。     

幕帘涂布工艺

本文主要介绍涂布与塞孔工艺,并对此工艺进行特征描述与释疑。     

DCS在30m~3聚合釜控制中的应用

介绍了电化厂聚合技改后的聚合釜温度控制方案,CS3000DCS在控制中的应用。实现了从进料、升温、恒温、直至反应结束的全过程自动控制,在操作站实现了动态工程流程图、控制分组、历史趋势等显示功能,可变参数在权限范围内的下载及报表打印等功能。     

Increasing Raffinate Dewaxing Efficiency

The efficiency of dewaxing of wide and narrow distillation raffinates using different mixed solvents: acetone and methyl–tert–butyl ether (MTBE), acetone and toluene, methyl ethyl ketone (MEK) and toluene, is compared. Decreasing the cutpoints from 100–140 to 50–70°C increases the filtration rate by 2 and more times and the yield of dewaxed lube oil by 2.5–5% as a function of the solvent used.