Asymmetric alumina membranes electrochemically formed in oxalic acid solution

Alumina membranes were fabricated by anodizing aluminium metal in 0.15 M oxalic acid. The growth kinetics of the porous layer were investigated in the temperature range –1 to 16 °C using linear potential scans up to 70 V. The faradaic efficiencies of metal oxidation and of porous layer formation, determined by applying Faraday's law, were found to be independent of both temperature and electrical charge. SEM analysis of the metal-side and solution-side surfaces revealed different morphologies. After dissolution of the barrier layer in phosphoric acid, the metal-side surface showed circular pores whose size of about 90 nm was found to be uniform and independent of temperature. The pore population was also practically independent of temperature and a value of about 4 × 10¹³ pores m^–2 was determined. On the solution-side surface the presence of a deposit partially occluding the mouths of pores was observed. This coating could be removed by chemical etching in NaOH or thermal treatment at 870 °C, where decomposition of oxalate occurs. This supports the hypothesis that the deposit consists of an aluminium salt containing oxalate anions precipitated from the solution. The results show that it is possible to control the morphological characteristics of the anodic alumina membranes by careful choice of experimental conditions.     

Advances in Microporous and Mesoporous Solids—Highlights of Recent Progress

This report highlights developments in the fields of microporous and mesoporous materials that were published mostly during the year 2002. Selected examples are provided to illustrate new zeolite structures, porous coordination materials, mesoporous solids with new compositions, controlled morphologies, and increased hydrothermal and thermal stabilities, as well as porous solids with tunable pore openings or other structural features that can be dynamically modified. A number of applications are discussed, including stabilization of reactive guests, separations, electronic materials, and sensors.     

部分可渗透直立圆柱的消波作用研究

本文导出了线性波浪作用于上部可渗透的直立刚性圆柱体上的水动力的解析解。在线性有势流的假定下，用特征函数展开方法求出了内部和外部流场的解。给出了不同波浪要素及结构尺寸参数下的数值结果。由结果可知，提高可渗透性可以有效消减波幅。     

变异函数在进间砂体预测中的应用

应用变异函数探讨了砂体的定量预测问题。通过对北二东密井网试验区不同类型砂体，不同井网密和岩厚度的预测，检验了此方法的精度（为70％左右），在原方法的基础上，通过对预报精度的分析并结合精度地质研究进一步完善了该方法，提出二次建模法并应用于北二东西块聚驱井的砂岩厚度预测中，预测精度可提高5％以上，从而说明应用变异函数研究砂体的定量预测问题具有可借鉴性，可以为今后新井调整厚度的预测及砂体描述提供依据。     

求解复杂形状旋转体拉延毛坯直径的新方法--计算机作图查询法

提出了基于AutoCAD软件的确定复杂形状旋转体拉延毛坯直径的方法－计算机作图查询法，这种方法操作严谨，结果准确，比原有的3种方法简捷、快速，是一种值得推广的好方法。     

发电机用DJL350磁极钢板的开发与应用

本文论述了高强度冷轧磁极板的试制性研究，应用性研究及在开生桥机组上的实施。通过与国外材料的对比，研究了材料的化学成分、力学性能、磁性能、金相组织及其与性能的关系。并对其实际应用效果进行了分析总结。     

单片机在监控同步电动机运行功率因数中的应用

介绍如何利用单片机自动控制同步电动机运行时的功率因数。     

微絮凝接触过滤处理低浊度含藻水的研究

通过现场试验，对微絮凝过滤处理生活用水所带来的一系列问题进行了详细、科学的分析，在大量试验数据基础上对产生问题的原因进行了研究并取得了初步结论。在此基础上，提出了改进措施，取得了实效。     

软体排在长江江新洲堤岸加固工程中的应用

介绍了长江江新洲堤段应用软体排护岸新型技术的情况，结合长江江新洲护岸工程对软体排施工、工艺、设备作简要叙述。