HPLC法测定新益肾蠲痹丸中延胡索乙素含量

建立HPLC法测定益肾蠲痹丸中延胡索乙素的含量。采用Kromasil色谱注,流动相为甲醇-乙腈-1%醋酸铵缓冲液（pH=5.0±0.02）（10∶30∶60）,流速1.0ml/min,检测波长283nm。延胡索乙素在0.07776～1.5552ug（r=0.9999）范围内线性关系良好,平均回收率为99.6%。     

关于大学生行为学建构的几点思考

研究与探索大学生的行为及其规律,对于造就与培养社会主义事业建设者和接班人,完成高等教育任务,意义重大。本文主要就大学生行为学逻辑起点、学科基础、研究对象与任务等问题进行探讨,并就如何建构大学生行为学,提出了初步构想。     

贺力氏Multi-Lab Hvdris定氢系统使用探讨及影响因素

本文主要介绍贺力氏Multi-Lab Hvdris定氢系统使用探讨及影响因素。     

Monitoring Moisture Uptake and Delamination in CFRP-Reinforced Concrete Structures with Electrochemical Impedance Sensors

Electrochemical impedance spectroscopy (EIS) sensors have been used to inspect carbon fiber reinforced polymer (CFRP) -reinforced concrete structures exposed to a variety of test conditions. Similar specimens were also used to investigate the detection of delamination between the CFRP and the concrete using a modified wedge test configuration. The use of external electrodes attached to the CFRP surface, coupled with the embedded rebar, provided the best results. Equivalent circuit modeling was used to analyze the impedance spectra. Several circuit parameters, especially the capacitance and constant phase element (CPE) magnitude, correlated very well with both bonded area/delamination and moisture. Both parameters exhibit a linear relationship with delamination area. The capacitance also showed a linear relationship with moisture content while the CPE was more strongly dependent on moisture. Differences in the response of the specimens subjected to the different exposure conditions were seen and explained based on the moisture uptake of the various specimens.     

Sensitivity of spectral reflectance to variation in live fuel moisture content at leaf and canopy level

Wildland fires burn large areas of the earth's land surface annually, causing significant environmental damage and danger to human health. In order to mitigate the effects, and to better manage the incidence of such fires, fire behaviour models are used to predict, among other things, the likelihood of ignition, the rate of spread, and the intensity and duration of burning. A key input parameter to these models is the amount of water in the vegetation, described as the fuel moisture content (FMC). A number of studies have shown that vegetation indices (VI) calculated from red and NIR reflectances may be used to map spatial and temporal variation in FMC in a range of fire-prone environments, with varying degrees of success. Strong empirical relationships may be established between VI and FMC over grasslands, yet over shrublands and forests, the relationships are weaker. If FMC is to be estimated with greater accuracy and consistency than is currently achieved, it is necessary to fully understand the relative contribution that spatial and temporal variation in the various biophysical and geometrical variables make to reflectance variability at the leaf and canopy level.This paper uses a modelling approach to investigate the sensitivity of reflectance data at leaf and canopy level to variation in the biophysical variables that are used to compute FMC. At the leaf level, the results show that the sensitivity of reflectance to variation in leaf water and dry matter content, used to compute FMC, is greatest in the SWIR and NIR, respectively. Variation in FMC has no effect in the visible wavelengths. At the canopy level, the results show that the sensitivity of reflectance to variation in leaf water and dry matter content is heavily dependent upon the type of model used and the range of variation over which the variables are tested. In the longer wavelengths of the SWIR, the competing influence of variable leaf area index, fractional vegetation cover, and solar zenith angle is shown to be greater than that at the shorter wavelengths of the SWIR and NIR. Empirical relationships between the normalised difference water index (NDWI) and FMC are shown to be weaker than that with canopy water content. However, when the range of the variables under study is more limited, useful empirical relationships between FMC and remotely sensed VI may be established.     

基于数学解析法的油纸绝缘参数辨识研究

现阶段变压器油纸绝缘等效弛豫机构参数辨识多采用拓扑支路数任意假定、粒子群等智能算法对 N组非线性方程组寻优迭代计算。其计算往往具有收敛性差、结果不唯一等问题,且难以从介质响应函数特性分析真实的油纸绝缘弛豫过程,影响后续弛豫参数对老化评估的准确性。基于此,提出一种应用数学解析法的变压器油纸绝缘弛豫机构参数辨识新方法。首先,从介质响应函数特性出发,深入挖掘弛豫项数信息,辨识油纸绝缘等效弛豫机构的拓扑结构;其次,公式推演得到参数辨识的数学计算公式,避免了智能算法对非线性方程组的寻优误差与不唯一性;最后,通过实例验证该方法的有效性与可行性,提出的数学解析法可为变压器油纸绝缘介质内部弛豫响应特性提供可靠的数学分析模型。     

损失气求取方法研究

当逸散时间较长时，用直线回归法采取损失气结果偏低，而逸散时间较短取点数少时，结果偏高。曲线拟合法是比较实用的一种方法，但计算工作量较大。经过模拟实验证明，在变围压条件下，甲烷的解吸规律也服从经验方程Ｑ＝ＷＪ［１－ｅｘｐ（１－ｍ＿１￣ｍ２／ｍ＿２］，并推导出迭代法求取损失量的计算公式。     

Can computers carry content ‘inexplicitly’?

I examine whether it is possible for content relevant to a computer's behavior to be carried without an explicit internal representation. I consider three approaches. First, an example of a chess playing computer carrying emergent content is offered from Dennett. Next I examine Cummins response to this example. Cummins says Dennett's computer executes a rule which is inexplicitly represented. Cummins describes a process wherein a computer interprets explicit rules in its program, implements them to form a chess-playing device, then this device executes the rules in a way that exhibits them inexplicitly. Though this approach is intriguing, I argue that the chess-playing device cannot exist as imagined. The processes of interpretation and implementation produce explicit representations of the content claimed to be inexplicit. Finally, the Chinese Room argument is examined and shown not to save the notion of inexplicit information. This means the strategy of attributing inexplicit content to a computer which is executing a rule, fails.I wish to thank Fred Dretske, JOhn Perry, and an anonymous reviewer for helpful comments and suggestions. Earlier versions of this paper were read at the American Philosophical Association Pacific Division Meeting in San Francisco in March, 1993, and at the 7th International Conference on Computing and Philosophy in Orlando in August, 1992.     

A changing society and problems of method: a politically committed research type

This essay examines a politically engaged research genre, which follows the biography of the author who founded two journals: one on mathematical models published in English (Quality and Quantity) and one on politically committed social and economic research published in Italian (Inchiesta). The research considered focuses on Italy in the 1950s, the research by Lazarsfeld in Vienna in the 1920s and in the United States in the 1950s and 1960s, and post-1968 politically committed research in Italy. The analysis of such politically committed types of research (all very different from one another in terms of the interpretative model of reality, the methods used and the relations with the tendering party and the people observed) allows one to understand how this kind of research can be performed with very different methods—all of which do, however, seek to modify reality on the grounds of the research results. The metaphor of the crystal and the flame presented by Italo Calvino in order to classify facts and ideas and styles and feelings can also be used to visualise the polarity (and the difficulty/impossibility of contact) that has always been present in sociology between two different tendencies: towards a discipline that offers the most abstract and objective interpretative model of reality possible with the use of mathematical models (the crystal), and, instead, towards a discipline in which an interpretative model of reality is central, one that produces a social change and in which the qualitative and quantitative methods utilised are at the service of this change (the flame). This polarity thus allows us to separate first and foremost all the politically committed research performed by others for different purposes (market research, research to verify some theoretical hypotheses, etc.) but the same polarity also lies within the politically committed research. We can, indeed, identify a type of politically committed research in an area that has, at one extreme, research tending towards the utmost objectivity and scientific quality of the results and where the co-ordinators try to have all the information on the subjects maintaining the greatest possible distance (the subjects must not know they are being observed); at the other extreme, there is a type of research in which the coordinator completely involves the subjects in the gathering of information that will serve to realise a piece of research whose political aims are explicitly shared. For the identification of a sufficiently articulated typology it has been important to consider five dimensions of politically committed research: (a) the characteristics of the research coordinator (his/her belonging to the type and the academic/non-academic professional status) and his/her interpretative model of reality (b) some general characteristics of the research (the tender and funding, the topic choice, the aims, the contributions to the sociological theory, the duration); (c) the research coordinators relations with the political actors (the intensity of the relations, the political use of the research); (d) the relations of the research co-ordinator with the research subjects; (e) the methodological choices (the basic strategies, the methods used, the use of mathematical procedures). The research that exemplifies this typology is all politically committed to the left and was realised in different times and contexts. I start by considering a kind of politically engaged research (co-research) that appeared in Italy in the 1950s; I then analyse two types of politically engaged research realised in Austria at the end of the 1920s and one in the United States in the 1950s; there then follow two kinds of research realised in the 1960s and 1970s in the United States and a further two kinds realised in Italy in the 1970s and early 1980s. In order to have other kinds of research please refer to the two Journals of which I am the editor: one is an English language journal of mathematical models (Quality and Quantity, International Journal of Methodology, founded in 1966 and published today by Kluwer of Amsterdam), and a politically engaged review (Inchiesta, founded in 1971 and still published today by Dedalo of Bari).